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By Rodrigo Perito Cardoso

Low-temperature nitriding of stainless steels is applied to obtain wear resistant surfaces without losing its corrosion resistance. The treatment consists in introducing nitrogen into the steel surface avoiding chromium nitride precipitation. The corrosion resistance of martensitic stainless steels is expected to be improved if the treatment parameters are correctly selected. It can be related to ?Fe2-3N and a'N phase formation on the treated surface. In the present work the influence of the pretreatment and treatment temperature on corrosion resistance of plasma nitrided AISI 420 steel samples is studied. Annealed, as-quenched and 400ºC-tempered samples were nitrided at 300, 350, 400, 450 and 500°C, for 6 h at 600 V. The pressure was 3 Torr and the gas mixture was composed of 70%N2, 20%H2 and 10%Ar, at a gas flow rate of 3.34×106 Nm3s-1. Plasma was generated using a square-wave pulsed DC power supply and the sample temperature was controlled by the duty cycle. The modified layers were characterized by optical microscopy, X-ray diffraction and microhardness measurement. The corrosion resistance was studied by electrochemical characterization, by means of Open circuit potential and Anodic polarization curves. The maximum surface hardness was achieved at 400°C. This temperature seems to be near the limit temperature for low-temperature treatment aiming to improve or at least to keep unaltered the corrosion resistance in relation to that verified for non-treated steel samples. Results confirm that the pretreatment and treatment temperature significantly affects the corrosion resistance of the treated surface.

Aug 8, 2018

By Ananda Moreira Vaz Ourique de Avila

Ferritic stainless steels have been used in the making of high and intermediate temperature operation solid oxide fuel cells (SOFC) interconnects, replacing the ceramic materials. However, at high temperatures, on the order of 700-850 0C, these steels can present significant oxidation and degradation processes, promoting increased electrical resistivity and corrosion losses that result in contamination of the electrodes and reducing the performance and the useful life of the SOFC. Thus, the knowledge on kinetics of oxidation/corrosion of these steels and their relationship with the microstructural transformations are of great importance. In this study, samples of ferritic stainless steels AISI 430, AISI 441 and Crofer22APU® were tested for oxidation at high temperature (800 0C) for long periods of time (up to 3,600 hours) and mass gains were monitored allowing the determination of the oxidation behaviors of these steels. Additionally, the microstructural characteristics of the samples before aging (corrosion-oxidation test) and after various oxidation times were evaluated by optical (OM) and scanning electron microscopy (SEM), as well as by micro chemical elemental analysis (EDS) and X-ray diffraction (XRD) phase analysis. Electrical characterization allowed determination of electrical area-specific resistances (ASR) characteristics of the systems studied, thus relating the electrical and oxidative behaviors of steels evaluated.

Aug 7, 2018

By Lukas Pichler

The market trend of advanced high strength steel (AHSS) with demand for higher strength products is increasing continuously. The inline cooling technologies have established as the most powerful metallurgical tool to achieve these demands. However, the cooling capabilities of existing hot strip mills, plate and Steckel mills are often not adequate to generate high cooling rates and the cooling accuracy required for the production of AHSS. Hence there have been many developments for an intensive, highly flexible accurate homogeneous cooling technology. Considering the wide variety of strip and plate geometry, Primetals Technologies have developed Power Cooling Technology for strip and introduced MULPIC®4 Technology for the plate production. In this paper we shall discuss these enhanced technologies that provide the inline cooling requirement with examples from the recently commissioned machines.

Aug 17, 2017

By Eddy Dierckx

Modernization of flat rolling plants is essential to sustainably fulfill increasing market demands and to improve competitiveness. Intelligent modernizations ensure getting maximum prime yield of existing mills, even if they have gone through half a century of operation. Existing mills were designed based on former production, consumption and quality targets. Ever increasing requirements such as increase of productivity, change of product mix (e.g. new steel grades), reduction of energy consumption and improvement of product quality lead to the necessity to adapt the existing equipment to the new target. SMS group provides, besides the reliable equipment and automation solutions to successful upgrades of existing mills, also a systematic approach to develop technical and economical solutions together with our customers (conceptual engineering). This paper describes the SMS group approach to modernizations / upgrades, introduces powerful performance modules and provides a number of successful examples that have been implemented recently.

Aug 17, 2017

By Gabriel Duarte Lott

O processo de análises físicas e químicas de amostras de minério de ferro [3] é um processo crucial para avaliação do tipo de minério que está sendo extraído, beneficiado e expedido nas operações das mineradoras. Assim, aplicar novos conceitos e equipamentos altamente tecnológicos, que irão garantir resultados cada vez mais precisos e a execução das tarefas de forma cada vez mais segura, é a chave e o desejo das empresas. No laboratório da VALE S/A, em Itabira, foi realizado um estudo de caso de um sistema automatizado de preparação de amostras capaz de realizar as etapas de divisão da amostra abaixo de 1mm, pulverização, confecção de pastilha prensada e fundida, análise de perda por calcinação (PPC), limpeza de utensílios e acessórios e descarte de resíduo de minério de ferro. Nesse estudo é abordado a avaliação dos equipamentos e tecnologias instalados e os desafios tecnológicos e de processos enfrentados durante a implantação desse projeto.

Oct 30, 2017

By Flávio Paulo Pugnal da Silva

Em 2010 foram observados elevados índices de quebra de rolamentos dos segmentos da máquina de lingotamento contínuo 3 da ArcelorMittal Tubarão. As análises iniciais, realizadas pelo fabricante, sugeriram que a causa estava relacionada principalmente a falta de proteções térmicas e desvios no sistema de lubrificação que estavam deteriorando as propriedades físico-químicas da graxa. Após o restabelecimento das condições de projeto os índices de quebra mantiveram-se elevados. O objetivo deste trabalho foi avaliar as potenciais causas ligadas as falhas de lubrificação deste equipamento. Foram estudados temperatura de trabalho do equipamento, qualidade físico-química da água, vazão e velocidade da água de refrigeração dentro dos mancais e respectivos suportes. Os resultados obtidos convergiram para uma deficiência do projeto de resfriamento dos mancais e suportes. Tais deficiências geravam baixa velocidade do fluxo de resfriamento, que associada as altas temperaturas de trabalho, proporcionavam condições adequadas a precipitação de particulados contidos na água, gerando assim a obstrução gradativa dos canais de refrigeração até total colapso do sistema.

Jul 30, 2018

By Hormando Leocadio Júnior

A otimização operacional no setor de desbaste da Linha de Tiras a Quente da Usiminas, Ipatinga, proporcionou redução do tempo de processamento dessa etapa, criando-se condições para aumento das temperaturas dos esboços na entrada do Trem Acabador (TA). Desse modo, para manutenção das temperaturas de acabamento dos laminados dentro da faixa de controle desejada, seriam necessárias menores velocidades de laminação no TA. Com a finalidade de garantir temperaturas desejadas na entrada do TA, que possibilitem adequadas velocidades, foi desenvolvido um sistema de controle de temperatura de esboço, que é acionado e desligado automaticamente na região inicial (topo), na extensão necessária do esboço. Esse sistema permitirá uma ampla exploração da nova condição de desbaste em menor tempo, com menor variabilidade da temperatura de entrada no TA, prevenindo ocorrências de estiramentos e de carepa, por temperatura alta nos topos e baixas nas bases dos laminados, maior uniformidade de propriedades mecânicas dos produtos, assim como aumento na capacidade produtiva.

Jul 30, 2018

By Luciano Almeida de Freitas

Este artigo tem como objetivo verificar os resultados da aplicação de ações que almejam a excelência no processo de carga, descarga e transporte de minério ferro de uma empresa situada na Região do Médio Piracicaba em Minas Gerais. Esta pesquisa é um estudo de caso de natureza exploratória e documental. No desenvolvimento deste estudo foram analisados os documentos da empresa, que referem-se às atas de reunião e relatórios gerenciais. As reuniões foram realizadas pelos gestores e supervisores do processo de carga, descarga e transporte de minério para identificar falhas e apresentar ações que almejassem a excelência no processo produtivo. Por fim, os resultados foram verificados e identificou um aumento no índice da utilização física dos caminhões de 11,46%, aumento da produtividade horária de 27,5% e um crescimento da movimentação total de produção dos caminhões de 23,92%. Com isso, pode-se verificar os ganhos com a aplicação das ações implementadas, que almejam a excelência nas operações.

Oct 30, 2017

By Humberto Celeste Gomes

Este trabalho irá apresentar os critérios e considerações que levaram a AMT decidir pela primarização de duas equipes de manutenção da área de Energia (equipe de manutenção mecânica das turbomáquinas e equipe de manutenção elétrica de SEP/RUG). Apresentará também os desafios de formação, treinamento e capacitação das equipes bem como abordará a avaliação dos ganhos do projeto. Ganho em produtividade: Aumento da produtividade da equipe com a redução de 11% da quantidade total de empregados e Ganho financeiro para a empresa em função de redução de custo fixo. Ganhos adicionais: Melhoria na qualidade dos serviços, com menor retrabalho e turn over; oportunidade de redução de contratação SPOT em outras atividades envolvendo equipamentos rotativos de menor porte (ex: bombas); Formação de uma base de técnicos para futuras promoções internas (inspetores, técnicos de manutenção dentre outras). Pontos de atenção: Serviços realizados fora do horário ADM pela equipe de manutenção; Formação de turno de revezamento na equipe de manutenção de Turbomáquinas em grandes paradas.

Sep 25, 2017

By Levi de Oliveira Bueno

Constant stress testing was used for characterization of creep behavior of a 1Cr0.5Mo steel plate in the ex-service condition. The tests were performed on creep machines equipped with Andrade-Chalmers type profiles, high sensitivity SLVC transducer extensometry, high stability temperature controllers, and facilities for monitoring the creep curves with an automatic data logging system. Ten creep machines of this type were used in this research, in an experimental work that lasted for one year. Three temperature levels were selected: 538, 565 and 593°C, with stress in the range from 52 to 224 MPa producing rupture times varying from 5 to about 3950h. The creep curves were all followed with great scrutiny using data logger scanning rates which enabled storing thousands of readings in each case. The experimental analysis involved measurements of minimum creep rate, rupture time and final elongation at rupture. The data were analyzed according to the classical phenomenological / physical relations (Norton, Arrhenius, Zenner-Hollomon, Monkman-Grant) and also considering five traditional parameterization methodologies (Larson-Miller, Orr-Sherby-Dorn, Goldhoff-Sherby, Manson- Haferd and Manson-Succop). Comparisons are presented among the possibilities of data extrapolation from five different methodologies. Comparison is also made with creep results obtained on a similar plate of the same material in the virgin condition.

Aug 16, 2017

By Laurent Dorel

Surface quality monitoring is primarily implemented in the last steps of steel manufacturing before shipment to the end user. However, an increasing trend for also addressing this topic in the upstream stages, such as hot rolling plant, is tackled by Primetals Technologies to give steel producers the key to a global optimized yield management, and efficient “lessons learned” processes. After the last developments of SIAS Next Gen platform, including High Resolution and Near Infra-Red, some site results will be exposed on the very specific high constraints lines such as ESP Endless Strip Production and Plate Mills, and highlights the related most interesting aspects for our customers.

Aug 17, 2017

By Enif Gutiérrez Guerrero

Inclusion deposition is still a standing problem in the continuous casting of steel since the deposition of alumina inclusions inside the SEN affects the productivity and the product quality. The present work studies the factors involved in the inclusion deposition at the nozzle and the effects of inertial, gravitational, buoyant, pressure gradient, and Saffman forces on the inclusion trajectories. The results show that the inclusions reaching the nozzle, only 30% get deposited along its walls mainly at the Upper Tundish Nozzle (UTN). This area of higher deposition is identified close to a low static pressure and a high turbulent kinetic energy dissipation zones where the effects of the gravitational and buoyant forces do not promote a significant inclusion radial movement since these are aligned with the direction of the flow stream lines. In contrast, in this zone, the Saffman force shows an important effect on the deposited inclusions, slowing down the inclusions in the vertical axis and increasing their radial movement.

Aug 17, 2017

By Mühlböck Marlene

Increasingly stringent global environmental regulations are forcing steel producers to continually improve the efficiency of sinter waste gas treatment. With the Selective Waste Gas Recirculation (SWGR) system from Primetals Technologies, lower production costs can be achieved and the size of downstream waste gas cleaning units can be reduced for investment savings. SWGR features the extraction and reuse of hot sinter off gas from selected wind boxes along the sinter strand, which contributes to improved energy efficiency and off gas treatment in the sintering process. With the next generation of SWGR, Primetals Technologies can provide an energy optimized, emission optimized and environmentally friendly solution that meet customer requirements and country specific regulations. This paper demonstrates the latest developments in selective waste gas recirculation, especially results from pot grate tests and comparison from lab to real plant data. Furthermore theoretical finding and mathematical modelling is presented.

Aug 16, 2017

By Thomas Schanz

Current steel market conditions require small investments only to lower operational cost. SMS Concast has developed new products which optimize continuous casting process cost for long product steel production. This paper describes a selection of three products. All three systems are patented (patent pending for CONDRIVE). CONSAFE, a non-radioactive mould level measurement system for reliable mould level measuring on open stream casting CCM’s; CONSTIR-MWS, an improved control software for electromagnetic stirrers which lowers energy cost by 35%; CONDRIVE, a brand new oscillation drive system which provides the features of a hydraulic oscillator, however with a cost efficient electric drive.

Aug 17, 2017

By Ernst Lindemann

The SMS group has developed the ultrasound technology “HD scan” for inspection of the internal quality of as-cast products. This method of sample analysis requires less preparation work and is safer than the current, most common technique of etching and/or sulphur printing. Furthermore, this technology offers a three-dimensional view into the sample of the cast product and thus more representative information for a better quality evaluation. The internal quality evaluation can be performed automatically and objectively by software based on clear statistical methods. A quantitative centerline segregation rating can be assigned to each sample, based on the size and distribution of segregates detected by the unit. Internal crack statistic (length, position, orientation, etc.) and narrow side profile can also be measured. Grain macrostructure can also be visualized which allows for a potential optimization of casting parameters like strand cooling, soft reduction or electromagnetic stirring. The accuracy of the new method was proven by parallel metallographic investigations of more than 100 samples of different steel grades and sample shapes. Automatic defect evaluation and classification was compared against macroetching results. It was found that HD scan identified more defects and the visualization of the macro structure could be performed in more cases than with macro etching. All tests, comparisons, further developments and analyses for various steel producers and steel treatment companies have been conducted at the HD scan unit, located at the SMS group headquarters in Düsseldorf, Germany (Figure 1). Based on the results, SMS group has designed a unit which can be used in industrial scale.

Aug 17, 2017

By Francisco Morganti

The market requirements which strip processing lines have to deal with have altered significantly within the last decades. Particularly, the production has to be economical and ecological efficient and processing lines have to cover a broad product portfolio. Already existing plants either directly or indirectly are competing with new plants, which are equipped with the latest technologies. The “Special Strip Processing Equipment” is designed to be integrated easily and within small downtime phases in existing lines. All single machines can be delivered in short time “ready-to-perform” with a tested and proved automation system. Thus, the competitiveness of existing lines can be increased immediately with less effort. To find out which machines can be reasonably implemented SMS group offers an “Efficiency Check”. A special proceeding is used by experts to find out quickly which machines will have the largest effect on the efficiency of the line while demanding at the same time the smallest expense.

Aug 17, 2017

By Carlos Gonzalez-Rivera

An alternative cooling curve analysis method focused on the experimental determination of the latent heat of phase changes and phase transformation kinetics is proposed in this work. The method analyses the cooling process of a metallic sample, initially liquid that is contained into a cylindrical metallic mold, both of known weight, thermally isolated at its top and bottom. The method is based on an energy balance associated with the experimental measurement of the temperature change of the sample and the mold during their cooling process. From the numerical processing of the cooling curves, are obtained approximate values of the acting global heat transfer coefficient as a function of temperature in order to describe quantitatively the energy exchange of the metal/mold system with its surroundings. These relationships and other experimental data are used to process the cooling curve of the sample and the mold during solidification, in order to obtain the latent heat of solidification.The method was applied experimentally to zinc and tin of commercial purity, initially liquids and contained into stainless steel molds in order to determine its ability to measure the latent heat of solidification. The obtained results suggests that this method shows a good potential to characterize the solidification of metals.

Oct 30, 2017

By Gerd Weyand

Gontermann-Peipers GmbH (GP) Germany developed a new, high alloyed steel grade for the manufacturing of back-up rolls. The advanced GP double pour casting processes provide highest flexibility in being quite open in rolls work layer chemistry and hence microstructure with no influence on core respectively neck properties. GP took the process advantage to provide a brand new back-up roll grade with remarkably reduced roll wear while operating with textured work rolls. In the meantime several successful trials have been made with this new roll grade on different Skin Pass Mills. As a result the performance of back-up roll and thus availability of mill will be improved while specific costs for mill will drop. This quite new back-up roll grade has recently been launched. As next step increasing the field of applications is under progress.

Aug 17, 2017

By Dilermando Nagle Travessa

High strength-light weight materials are very attractive for the transportation sector, particularly to the aerospace industry. High strength-age hardenable aluminium alloys are widely used in airframes due to their unique combination of strength, density, toughness, corrosion resistance, cost and easy processing. However, the hardening capacity of such alloys is somehow saturated due to thermodynamic issues related to the conventional processing. The production of aluminum-matrix composites is a promising strategy to overcome this limitation, resulting in strength levels that cannot be reached by actual commercial aluminum alloys. In the present work, multiwall carbon nanotubes were used to reinforce the AA6061 aluminium alloy. 1 and 2% weight percent of MWCNT were mixed to the alloy powder by high-energy ball-milling process. The blended powder was consolidated by hot extrusion. The obtained composite bars were submitted to heat treatment for the T6 condition in order to combine both CNT dispersion and precipitation hardening effects. Optical and scanning electron microscopy, as well as hardeness testing, was used to characterize the bars. Typical wrought microstructure, free of defects, was observed on the extruded bars. Hardness of the composites was observed to increase by 20, 28 and 68% for 1% MWCNT 6 h milling, 2% MWCNT 6 h milling and 2% MWCNT 10 h milling, respectively, in the as-extruded condition. The better performance for the composites blended at higher milling time was attributed to a better nanotubes dispersion. Subsequent heat treatment to the T6 condition did not result in additional hardening.

Aug 8, 2018

By Roberto Balarini Junior

Tribological behavior of Si3N4 balls sliding against Al2O3 discs in water was investigated by studying the influence of parameters such as initial surface roughness and circular axial run-out of the discs. The objective was to relate these parameters with the occurrence of the phenomenon known as ultra-low friction coefficient (ULFC), which is characterized by µ < 0.01, including the correlation with running-in duration. As a general trend, greater initial surface roughness and circular axial run-out resulted in greater running-in duration. In addition, it was verified that a mixed lubrication regime (hydrodynamic and boundary) is required to guarantee the occurrence of ULFC by comparing the calculated minimum film thickness with the composite roughness of the worn surfaces. Also, ICQ-OES analysis of the water after the tests indicated that a silicon concentration greater than 1.3 mg/l should be fundamental for the occurrence of µ < 0.01.

Jul 31, 2018