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By Bernardo Siqueira

This paper presents a unique stirred milling technology, Outotec HIGmill™, a modern, flexible and energy efficient grinding solution for fine and ultra fine grinding being tested in an industrial scale level. The test was performed at an iron ore pellet producing plant in Sweden (for confidentiality reasons, it will be referred to only as “the client”) where a pilot HIGmill™ unit (HIG25) was installed parallel to a conventional regrind circuit to compare its performance to the existing ball mill. By using a continuous test run procedure and evaluating the parameters of F80, P80, mill shaft rotation speed and power drawn it was determined its grinding capabilities, operational flexibility and energy efficiency. Outotec HIGmill™ outperformed the existing ball mill in the plant proving its capabilities to grinding finer, with steeper particle size distribution (PSD) and much higher energy efficiency. The tests performed showed that, with further refining of its operation, it is capable of consistently deliver the required PSD with up to 30% higher grinding efficiency.

Aug 16, 2017

By Wenting Zhu, Liqing Chen, Junjun Cui, Zhenye Chen

In this presentation, a low carbon high strength steel microalloyed with Nb and Ti was processed by thermo-mechanical controlled process (TMCP) containing two stages of controlled rolling. The austenite with various grain sizes was obtained by austenitizing this hot-rolled steel at different temperatures. And the effect of austenite grain size on bainitic transformation was investigated in a dilatometer to reveal microstructural change. The results showed that the microstructure of the hot-rolled steel was mainly composed of granular bainite, lath-like bainite, and martenite/austenite constituents (M-A constituents). With increasing the austenitizing temperature, or increasing the austenite grain size, the microstructure was changed from granular bainite to lath bainite. When the steel was reheated to a lower temperature of 860 ºC, a relatively higher start temperature (Bs) was measured for bainitic transformation. This was mainly caused by the formation of solute-depleted region in the austenite and the promotion of the granular bainitic nucleation. The highest reaction rate occurred at austenitizing temperature of 1000 ºC with fine grain size, while the coarse austenite grain can lead to a sharp increase in the amount of bainite. An analysis was made on the kinetics of bainite transformation which was controlled by the volume diffusion of C atom.

Oct 1, 2019

By Florian Markus Penz

The increase in Basic Oxygen Furnace (BOF) plants in steelmaking has given rise to renewed interest in a dynamic simulation of the BOF process. Material and process costs can be saved with optimized process times and targeted charging of scrap and slag formers. Beside hot metal, scrap is the main source of iron in the BOF process. Furthermore, scrap is used as a coolant during the process due to exothermal chemical reactions occurring in the BOF. In this paper, the melting and dissolution behaviour of scrap in the BOF process is discussed. A new dynamic thermodynamic and kinetic Matlab® model used to simulate scrap melting behaviour as a function of various scrap surface parameters and particle size is presented, as well as the influence of scrap properties on liquid bath temperature and final crude steel composition after a defined blowing period.

Oct 30, 2017

By Silvio Cecchini

State-of-the Art Mould Level Control Solutions for continuous casting applications face different challenges. On the one hand, technological phenomena such as clogging and unclogging, unsteady bulging or waving can create unpredicted meniscus disturbances by completely changing the casting channel geometry and the flow behaviour of liquid steel to the mould. On the other hand, from the viewpoint of caster operations, long lifetime, quick interchange-ability and integration capability into existing systems must be achieved. In the present contribution, the overall development of INTECO TBR’s mould level master – a comprehensive mould level control solution for all continuous casting applications – will be introduced. The basis for the presented system is a development over several years which includes investigations of all critical components such as shroud, stopper, stopper mechanism, servo actuator and mould level control program. These investigations finally resulted in a new-ly developed control algorithm for a highly dynamic servo actuator. The control algorithm with its basic functionality such as the prevention, identification and removal of clogging impacts with the associated automation functions to reduce their influence onto the overall mould level control performance will be presented. The scientific basis, the resulting control functions and their related automation implementation will also be illustrated. Finally, a patented control algorithm and control functionality for unsteady bulging and waving effects with the associated automation functions to reduce their influence onto the overall mould level control performance.

Aug 16, 2017

By Henara Lillian Costa

This paper aims to investigate the effects of a possible incorporation of ethanol to the lubricant during engine use on friction and lubricant film thickness, by adding small amounts of ethanol to Group I base (with and without an organic friction modifier) and to formulated oils. Film thickness was measured using ultrathin film interferometry. Friction tests were carried out using a mini-traction machine to obtain Stribeck curves. The film thickness measurements showed that in the region of low speeds, where the elastohydrodynamic film is very thin and therefore boundary lubrication may prevail, the addition of ethanol produced some boundary film, which was not present for the base oils. For the base oil with an organic friction modifier, the presence of ethanol increased the thickness of the low friction boundary film. For the formulated oil, the addition of ethanol reduced film thickness in all lubrication regimes. The friction tests showed some friction reduction due to addition of ethanol to the base oil, in particular at low speeds. For the formulated oil, the addition of ethanol reduced friction at high speeds, which was associated to a reduction in the viscosity of the lubricant, but at low speeds, the presence of ethanol reduced the formation of a boundary layer, increasing friction. For the base oil containing an organic friction modifier, the presence of ethanol increased the range of speeds for which low boundary friction occurred.

Jul 31, 2018

By Cristina Escudero Martinez

The purpose of the Basic Oxygen Steelmaking (BOS) is to refine the hot metal produced in the blast furnace into raw liquid steel, which may be subsequently refined in the secondary steelmaking shop. Appropriated fluxes for the BOF could require low melting point to reduce the energy consumption, to reduce the energy to fluidity the slag at lower temperature and to melt at lower temperature than steel. It is necessary a good Tumble test result and the fluxes do not generate fines which could obstruct the blowing plugs, so we would have a homogeneous flux. A homogeneous chemistry that allows to control the basicity (Si and MgO levels) and a high absorption characteristics to combine the flux with P, S, Si, etc. are necessary. PASEK Dunite is an ultramaphic rock exploited in the north of Spain with a basic chemical classification being olivine and serpentine its principal minerals. It is formed by orthopyroxene, clinopyroxene and olivine in variable proportion. Dunite is a very homogeneous and hard stone. The main characteristics are: High hot and cold resistance to mechanical stress (shatter / crushing / abrasion), softening and melting points of a flux, not a refractory material, large porosity which is increased more than 20% when dunite is heated at BOF process temperature, and high absorption level, and stable components with low melting points. PASEK Dunite is a good flux in BOF process and its use is recommended if the BOF process produces pig iron with low Si content, generates high levels of slag and it is necessary maintaining the basicity index and the MgO amount and with high value of hot metal ratio (high amount of phosphorus to remove).

Aug 16, 2017

By Manfred Hackl, Sergey Bragin, Alois Seilinger

The demand for hot rolled strip is growing in multiple ways. To remain competitive, new and existing mills must meet arisen challenges in the best possible way. The production of hot strip is a key element of steel production. Since close to half of all steel produced is hot-rolled to strip, mills require maximum throughput and availability combined with geometrical precision and the ability to create optimum material properties. Today there is a clear trend in developing new steel grades with high-strength and improved formability, like 3rd generation AHSS (Advanced High Strength Steels), as well as a trend to produce thinner and wider gauges. This trend challenges hot strip mills because it requires new technologies which provide more flexibility in metallurgical treatment during the rolling process. In order to meet and promote these trends Primetals Technologies is currently working on different concepts and solutions. One example is the development of a new mill stand technology Flex-HI HOT which allows to adapt the last finishing mill stands by efficiently switching from 4-high to a 6-high mode with small work roll diameter based on production needs. Another solution is to apply a permanent 6-high rolling stand at the end of the finishing train. A smaller work roll diameter allows to achieve higher specific thickness reductions and deformation rates resulting in significant thinner hot-strip gauges with valuable metallurgical benefits. The developed solution concepts with technological and metallurgical benefits will be presented in this paper.

Oct 1, 2019

By Olivier Lacroix, Dubé Mathieu, Guylaine Laforest

The reduction behavior of iron ore pellets in gas-based DR shaft processes has been studied at COREM since the late 80s. At that time, a new DR characterization test called COREM R180 was developped in collaboration with ArcelorMittal Mines Canada (former Quebec Cartier Mining) and ArcelorMittal Long Products Canada (former ISPAT Sidbec Inc.). This paper describes COREM’s approach to improve its understanding of the relations between iron ore pellet microstructure and pellet quality. The differences between the DR90 and the R180 tests are discussed. The evolution of the microstructure during reduction of both tests is also described. The reduction steps during the two tests are put forward as an important factor impacting the microstructural changes as well as the test results.

Oct 1, 2019

By John Hinton

Electromagnetic based (EM) sensor technology has been shown to detect changes in the magnetic permeability of steel strip travelling down the run out table after rolling. Measuring below the Curie temperature, these changes can be interpreted in terms of the phase transformation from austenite (paramagnetic) to ferrite (ferromagnetic). These real time measurements provide a detailed insight into the changes in the structure at high temperature providing the steel producer with feedback on quality control, product consistency and product development. However unlike mill microstructure models, the sensor measurement provides a point reading at a distance through the cooling course. To map the transformation in more detail, a sensor array is required along the length of the Run Out Table i.e. to measure points on the austenite to ferrite transformation curve. This paper describes the process and metallurgical factors that should be considered in the optimum design of a sensor array, i.e. the number and location of the sensor heads. Examples of cooling strategies for different steel grades e.g. low carbon, structural and dual phase steels are used to demonstrate the importance of sensor location. In addition, the effect of variability within typical industrial parameters e.g. cooling speed, on the sensitivity of sensor output and location will be considered.

Oct 1, 2019

By Rodrigo Sanchotene Silva

Currently the industries of paint have directed their efforts on cleaner production of products that provide effective performance in corrosion protection of metallic materials. This work search introduce a new alternative of organic coating, without the presence of hazardous metals and replace equipments commercials used method of anodic protection for protection of oxidized metals. From this it, was produced Smart Paint (SP), consisting of Paint Acrylic Commercial (PAC) mixed the 1 % of binder, compound by the conducting polymer, Polyaniline Emeraldine Base (PAni EB) and plasticizer 4-chloro-3-methylphenol. The SP and PAC were applied to plates of carbon steel AISI 1010, with the aid of dip coat technique and then were subjected to drying for 48 h. The SP was characterized by thermals and physicochemical analyzes in order to verify possible changes in chemical properties of the ink produced, beyond perform electrochemical tests of Open Circuit Potential and Electrochemical Impedance Spectroscopy, employing equipment Potentiostat/Galvanostat Autolab PGSTAT302 Ecochemie, and aqueous 2 mol.L-1 of H2SO4. The results obtained allow us to state that the plasticizer does not alter the electrochemical properties of PAni and application of binder PAni EB to PAC does not alter the physicochemical properties of commercial coating. The binder PAni EB adds to PAC the capacity to induce the formation or maintenance of protective oxides in oxidizable metals submitted to harsh environments, method known as anodic corrosion protection.

Aug 8, 2018

By Satish V. Kailas

For product sustainability “closing the cycle” is the first requirement. If the materials used in making the product is not replenished at the rate at which it is being extracted, the cycle is open and the product would not be sustainable. This includes the materials used in generating the energy used to make the product, the transportation, use and disposal. If the materials used in a product, that includes lubricants, is one that cannot be replenished, it has to be recycled for the product to be sustainable. The other basic condition for sustainability is the eco-friendliness of the product. It is argued that the present lubricants do not fall in this category. Using the example of cutting oil emulsions we have shown that it is possible to meet the conditions of sustainability in terms of both the material extraction-replenishment cycle and eco-toxicity. Cutting oil emulsions made from coconut oil and natural additives are shown to have superior cutting properties and are completely eco-friendly. It is concluded that products made using these conditions are possible and is a necessity for man to lead a sustainable life. Closing the cycle, with respect to the energy used in the cycle will make the product completely eco-friendly.

Jul 31, 2018

By Diego Berti Salvaro

The morphology, dimensions and chemical composition of tribolayers strongly depend on the pressures and temperatures acting on the contact. They are formed by reactions between the surfaces in contact with each other as well as with the atmosphere, lubricants and possible contaminants. In this paper the influence of test time (180, 500, 1000 and 2500 h) into the formation and characteristics of tribolayers in pairs DLC-stainless steel tested under refrigerant gas R134a atmosphere without presence of lubricating oil was analyzed. The characterization was performed using scanning electron microscopy, energy dispersive spectroscopy (SEM-EDS) (morphology and chemical composition) and white light interferometry (dimensions). The tribolayers thicknesses ranged from 100 to 500 nm and they were composed by elements originated from mutual transfers between the tribological pairs as well as oxides, being more pronounced on the stainless steel surface. The results show that the tribolayers are chemically stable (maintained the same composition over time) and the thickness remained stable after a thousand hours of testing.

Jul 31, 2018

By Hiroshi Ichikawa

In 2013, Nippon Steel & Sumikin Engineering Co., Ltd. (hereafter referred to as NSENGI), Tenova HYL and Danieli have entered into an agreement to combine ENERGION DR technology into blast furnace technology and/or with syngas technologies. This new alliance will allow the three companies to combine research and development activities with their respective expertise in ENERGIRON DR technology, Blast Furnace technology and Syngas (by-pro gas and coal gasification) technology, with the ultimate objective to develop breakthrough iron making technologies and create such EPC projects. This paper introduces the concepts and the features of our breakthrough technologies of combining of ENERGIRON DR technology, Blast Furnace technology and Syngas technology.

Aug 16, 2017

By Thierno FALL

This paper describes the study of the work-roll during the hot rolling process thanks to a 3D model built with the Finite Element Method (FEM). In terms of computational cost, that method needs high resources compared to 1D model which are mostly used. However, the 3D model is built to have a better understanding of the work-roll thermal and mechanical behavior during the hot rolling process. The thermal model shows that the highest temperature reached during rolling are within the range of 500°C and 600°C. The thermal field input used to simulate the mechanical behavior of the work-roll shows a biaxial thermal stress state, in the circumferential and axial planes. However, a peak of radial stress is observed in the backup zone. It did not generate plastic strain but could influence the fatigue behavior of the work-roll.

Oct 1, 2019

By Danilo Gonçalves de Oliveira, Rogério Martins Pereira

Chatter is a widely studied vibration phenomenon that affects most cold mills around the world and its impact on these lines are tremendous: from productivity and quality losses to mechanical equipment damage. The investigation of its origins and how to minimize the occurrences and their impact on the equipment require special instrumentation and algorithms in order to have a detection of the vibrations as soon as they start. This paper presents three methods of identification of chatter on a Tandem Cold Mill and the actions to leave the vibration frequency range before its amplitude achieve catastrophic values.

Oct 1, 2019

By Michel Rodrigo Luiz, Glaucio Augusto Polini, Leonardo de Souza Melo, Giovani Rodrigues, Giardini F. Lazzarin

ArcelorMittal's pickling and cold rolling line has been demanded to increase production since the installation of equipment in 2015. In addition to improving productivity related to these new equipment, several additional jobs were planned and executed on equipment already installed has been carried out in order to improve the efficiency of the line. The present work exposes what was done in the scale breaker (tension leveler) to improve the availability results of the section and consequently of the line.

Oct 1, 2019

By Peter Fajfa, Heinz Palkowski, Jakob Kraner, Matjaž Godec

The study of asymmetric rolling on the AA 5454 aluminium alloy plates was carried out. The plates were taken directly from the industrial hot rolled sheet. They were cold rolled on the laboratory mill with different rotation speed of the upper and the lower work roller with the strains around 33 % and 44 %. To get closer to the industrial conditions the maximal dimensions of the rolled plates for laboratory rolling mill and the special industrial lubricant were used. After deformation the plates were annealed to the soft condition. This research was focused on all possible effects of asymmetric rolling: The reduction of rolling force, the increase of strain at same set roll gap, bending of workpiece, finer microstructure, more heterogeneous textures and as a consequence of that better mechanical properties. The asymmetric rolling with favourable mechanisms in the deformation zone has created the material with the homogeneous hardness in the cross section and with lower anisotropy, which is crucial for improvement of formability properties of aluminium work hardened alloys and to get closer to properties of steels. In the presented paper the general impact and different effects of speed difference of rollers was investigated on cold rolled aluminium alloy. Obtained and analysed results explain the function of asymmetry in rolling process and the options to implement the asymmetric rolling in industrial plant.

Oct 1, 2019

By Claudio Pereira Diogo

A lot of galvalume/aluzinc steel sheet was furnished to a metallic roof manufacturer intended for tile fabrication. But, according with the roof manufacturer, that coils develops a different superficial aspect during processing. The purpose of this work was to provide an explanation for the appearance of the observed surface on one side of the coils. In order to find out the origin of the problem, mechanical and microstructural characterization tests were done at INSPEBRAS with the support of a partner laboratory. The results are described in this paper with their analysis and conclusions.

Aug 16, 2017

By Ramon Augusto Moretti, Henrique da Rocha Severino, Renato Nascimento de Castro, Fernando Cesar Sousa

Rolling stand 12 (LTx) of long steel, installed in the company A, Piracicaba - SP unit, had presented high levels of vibration, which affected its internal components, such as: shaft, gears and bearings, generating downtime. To evaluate this equipment a study was proposed by the following engineering techniques: Conventional Vibration Analysis, Operational Deflection Shape (ODS) and numerical simulation by the Finite Element Method (FEM). In the Conventional Vibration Analysis, high levels of vibration were observed during manufacturing process, especially when the material reaches the equipment. Impacts generate high values in acceleration, on average 80 m/s² peak to peak. In the moment of impact, misalignment of internal components was observed by ODS. Field results were correlated to those obtained by the Finite Element Method, which allowed to calibrate FEM model. Thus, the most effective structural modification already numerically evaluated was implemented in the system. Afterwards, new measurements by vibration and ODS techniques were performed, and attenuation of vibrational levels and operational mode, which overloaded the internal components rolling stand, were verified.

Oct 1, 2019

By Lucia Vieira

Kelvin probe force microscopy (KPFM) can be used to monitor electrostatic charges on the surfaces of materials. In this paper, we describe the use of KPFM to evaluate the electrostatic effect induced by silver nanoparticles incorporated as clusters in diamond-like carbon (DLC) films, before and after scratching. The results are compared to those obtained for DLC films without silver nanoparticles. Raman spectroscopy was used to identify the DLC signature, and energy dispersive X-ray spectroscopy (EDX) was used to confirm the presence of silver in the film. The morphology of the DLC film containing silver was investigated using scanning electron microscopy (SEM) and transmission electron microscopy (TEM). The findings suggest that the incorporation of silver nanoparticles in amorphous materials could offer new options for electrostatic energy storage on the surfaces of these materials.

Jul 31, 2018