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By Ralph L. Brown

The chemical properties of the unsaturated members of the aliphatic series of hydrocarbons are such as to render them " made to order" starting points or basic . materials for the synthesis of hundreds of important organic chemicals . The tremendous quantities of these unsaturated compounds that are being produced daily in the various coal carbonization and oil refining processes , and which at present have little value other than that of fuel , render a survey of the identity and ex- tent of occurrence of these compounds important from the viewpoint of economic utilization and resource conservation The increased need of liquid fuel and the relatively early exhaustion of petroleum resources will eventually require every utilization of liquid fuel products obtainable directly or indirectly from coal . Accordingly , the Bureau of Mines took advantage of an opportunity for examining the gaseous unsaturated hydrocarbons found in the gas obtained when a mixture of water- Collection of the material gas tar and coal is distilled in a gas-making retort . for examination was made possible through the courtesy of the Trent Process Corporation , Washington , D.C. , which was at that time carrying on at the Georgetown Gas Works , distillation of " amal gams " prepared from various coals and oils by the Trent process for cleaning coals . Kanawha gas coal ( 70%) and water gas tar ( 30 % ) from the Washington Gas Light plant were used in the " amal gam" being distilled at that time . The results obtained in this examination are presented here .

Feb 2, 1922

Mine closing methods should be carefully considered. If not properly sealed, an abandoned mine may continue to produce acid water. Since 60 to 90 percent of the total acid discharged from all coal mines is from abandoned mines,(58) some states require that provisions for sealing be contained in the mining permit application. Closing an operation to prevent harmful mine drainage into nearby runs and streams is a subject of much concern to states as a result of continuing problems from long abandoned mines which were improperly closed.

Jan 1, 1970

By D. E. Wolfson

The Bureau of Mines investigated the use of preheated coal in carbonization operations. Liquor yields and coking times were reduced, coke quality was improved, and smokeless pipeline charging to coke ovens should eliminate a serious source of pollution.

Jan 1, 1972

The extrapolation of results from reconstructed laboratory soil columns to field conditions is difficult because of the limitations of laboratory experiments. Permeability and elution tests performed in the laboratory differed from the natural state in that the soil was sieved through 1/4 inch screen to remove large stones and roots, its density was controlled by tamping the soil into two-inch I.D. tubes instead of normal weathering, and water and latex were applied with a constant head of liquid. Tube wall effects are important in interpreting data. Conversely, interpretation of field results were confounded by non-homogeneities within the sample tested, a soil profile with gradation of permeability and density with depth, and uncontrolled weather conditions and seasonal changes that affected the results. Nevertheless, both laboratory and field tests showed that a specific latex did perform as a soil sealant. In view of these facts a soil box experiment was designed to overcome some of the disadvantages associated with the small laboratory soil columns and the field experiments. Two wood soil boxes 5 ft x 5 ft x 5 ft were built in the greenhouse at the Uniroyal Research Center. They were lined with plastic PVC sheeting provided with tubes every six inches of depth on one side of each box to measure water removal rates under saturated conditions. Tensiometer gauges were placed at depths of 6, 12, 18, 24, 36 and 48 inches and Bouyoucos blocs and resistance thermometers were positioned at 6, 24 and 48 inch depths. Each box was filled with a uniform sub-soil obtained from Ogdensburg, N. J. The texture of this soil was determined to be a sandy loam by the ASTM Hydrometer method, as shown below: [ ] The boxes were thoroughly wetted by sprinkling to abet settling and allowed to dry by draining to check seepage ports and functioning of tensiometers.

Jan 1, 1972

By C. B. Manula, R. L. Sanford, R. A. Rivell

A generalized flow diagram is presented in Figure 1, which shows the relationship of major model functions. This chart does not necessarily represent the anatomy of the computer program, but is designed to illustrate the informational interchange between major model functions. The related flow-charts-and computer program are listed in Parts I and II, Appendix A, respectively. Mine Car Stations The mine car stations are the activity centers for the model. The locomotive logic structure is designed to provide these stations with adequate cars and to clear them of car buildup. The model is designed to simulate a three stage haulage situation which suggests the need to differentiate station levels by type numbers. These are: a) TYPE 1 stations - mine cars are loaded here; b) TYPE 2 stations - intermediate stop and storage for mine cars; c) TYPE 3 stations - all mine cars that are stored here leave mine; and d) TYPE 4 stations - mine portal. TYPES 1, 2, and 3 have all loaded cars assigned to an ascending TYPE as their next destination. In input, if single stage haulage is designated, TYPES 1 and 3 do not exist, and if two stage haulage is called for, TYPES 2 and 3 are absent. A motor is not permitted to exchange cars between stations of the same type. Station Status Update. One major model function is to continuously evaluate the status of each mine car station. The major evaluations

Jan 1, 1974

By Vijia K. Karra

The goal of aggregates producing companies across the United States is to ensure their workers go home safely each day. At the National Institute for Occupational Safety and Health (NIOSH), researchers are pursuing this vision of safety and health through a fact-finding approach for reducing injury illness in various mineral sectors. Surveillance data from Mine Safety and Health Administration (MSHA) has been the source for such analyses. It helps to focus research efforts on key machinery, workers, and their tasks. The second installment of this two-part series follows last month's focus on crushed stone.

Improve the field-of-view into the front-right blind spot for drivers of large haulage trucks, thereby reducing the growing collision hazard in surface mines. Approach Reduce the glare problem found in the first generation fresnel lens blind area viewer design by eliminating the upward-looking section of the fresnel lens and adding a rear hood to reduce backlighting. How It Works The first generation blind area viewer was developed and in-mine tested as an aid to improved visibility for large haulage trucks. Other aids were improved left-and right-hand mirrors. Evaluations showed that a blind area viewer mounted on the right-front of the radiator deck was effective and was readily accepted by drivers. Nevertheless, because glare was a problem under certain conditions, a low-profile viewer was developed. Glare control louvers from the earlier design were kept and a backlighting glare control hood was added. The height of the hardware was reduced by eliminating the top three inches of the fresnel lens. This portion of the lens contained an upward-looking segment which originally was thought to be needed so the driver could see the horizon when he looked through the viewer and be better

Jan 1, 1982

Reduce fire warning time and avoid activation of false alarms in underground mines. Approach A heat activated stench/tracer gas system was developed which automatically releases the gas mixture into the mine ventilation air. How It Works A canister approximately 12 inches long and 3 inches in diameter is charged with 50 grams of ethyl mercaptan or other appropriate stench gas and 500 grams of instrument detectable Freon. The canister is then pressurized to 100 psi with nitrogen. A disc is used to seal the contents of the canister. A low-temperature alloy designed to melt at a predetermined temperature is used to restrain a spring loaded plunger. Upon exposure to heat, the alloy melts and the plunger is released. The plunger ruptures the disc and the mixture of stench and tracer gas is released from the canister. Canisters are mounted in areas of a mine which are susceptible to fire such as near

Jan 1, 1983

This section contains a summary of our investigation of the soil conditions (type, porosity, moisture content, etc.) at the two sites (Lanse and Kato, Pennsylvania) selected for field testing of latex as a soil sealant. Other natural conditions such as rainfall, frostline, depth of the water table, etc., were also measured and recorded for possible later use in assessing the effect of the latex seal on the total environment. The numbered sites referred to throughout this report are shown on the maps of the Lanse and Kato sites (Figures 1 and 2). KA, RB and KC are positions at the Kato site - all other numbered positions refer to the Lanse site. Two other terms used throughout the report which should be explained are “horizon” and "profile". These are synonymous terms for soil layer, A horizon (or A profile) referring to topsoil and B horizon (or B profile) referring to subsoil. The properties that control the flow of water through the soil are of special interest because these will also govern the passage of a sealant into and through the soil. Normally the particle size distribution is a good measure of soil permeability, which is directly proportional to sand content and inversely proportional to silt and/or clay content. Tables I1 and I11 show the percentages of gravel or stones, sand, silt and clay of Lanse and Kato soil samples. According to the United States Department of Agriculture classification, the gravel is ,ignored and the residue separated into sand, silt, and clay fractions. Figures 4 and 5 indicate by means of the USDk soil texture triangle that the variability of composition of Lanse soil ranges from sandy loam in the creekbed to clay loam. The variation is even greater among soil samples from Kato. Porosity of soil, also known as percent voids, is another indication of how readily water will travel through soils. Soil density usually increases and porosity decreases with depth, and as expected, the porosity of the top soil at Kato, a forest, is exceptionally porous and open (see Table IV) The pore diameter and length of soil capillaries is extremely variable, and its distribution in the field is impossible to determine. In addition to the capillaries, soil also contains many macro cracks, crevices, and passages around stones and roots. All these affect the flow rate of water through soil. Poiseuille's law states that the rate of flow of a liquid through a narrow tube is proportional to the 4th power of the radius of the tube. Pore size normally decreases with depth and in soil containing appreciable amounts of silt and clay this is especially true. Thus, deeper soils should be less permeable and such was the case at Lanse and Kato.

Jan 1, 1972

By John J. Sammarco, Edward F. Fries

This report (Independent Functional Safety Assessment 4.0) is the fifth in a nine-part series of recommendations addressing the functional safety of processor-controlled mining equipment. It is part of a risk-based system safety process encompassing hardware, software, humans, and the operating environment for the equipment’s life cycle. Figure 1 shows a safety framework containing these recommendations. The reports in this series address the various life cycle stages of inception, design, approval and certification, commissioning, operation, maintenance, and decommissioning. These recommendations were developed as a joint project between the National Institute for Occupational Safety and Health and the Mine Safety and Health Administration. They are intended for use by mining companies, original equipment manufacturers, and aftermarket suppliers to these mining companies. Users of these reports are expected to consider the set in total during the design cycle. • 1.0 Safety Introduction.—This is an introductory report for the general mining industry. It provides basic system/software safety concepts, discusses the need for mining to address the functional safety of programmable electronics (PE), and includes the benefits of implementing system/software safety program. • 2.1 System Safety and 2.2 Software Safety.—These reports draw heavily from International Electrotechnical Commission (IEC) standard IEC 61508 [IEC 1998a,b,c,d,e,f,g] and other standards. The scope is “surface and underground safety-related mining systems employing embedded, networked, and nonnetworked programmable electronics.” System safety seeks to design safety into all phases of the entire system. Software is a subsystem; thus, software safety is a part of the system’s safety. • 3.0 Safety File.—This report contains the documentation that demonstrates the level of safety built into the system and identifies limitations for the system’s use and operation. In essence, it is a “proof of safety” that the system and its operation meets the appropriate level of safety for the intended application. It starts from the beginning of the design, is maintained during the full lifecycle of the system, and provides administrative support for the safety program of the full system. • 4.0 Safety Assessment.—The independent assessment of the safety file is addressed. It establishes consistent methods to determine the completeness and suitability of safety evidence and justifications. This assessment could be conducted by an independent third party. • 5.0 Safety Framework Guidance.—It is intended to supplement the safety framework reports with guidance providing users with additional information. The purpose is to assist users in applying the concepts presented. In other words, the safety framework is what needs to be done and the guidance is the how it can be done. The guidance information reinforces the concepts, describes various methodologies that can be used, and gives examples and references. It also gives information on the benefits and drawbacks of various methodologies. The guidance reports are not intended to promote a single methodology or to be an exhaustive treatment of the subject material. They provide information and references so that the user can more intelligently choose and implement the appropriate methodologies given the user’s application and capabilities. [ ]

Jan 5, 2003

By C. P. Hood

"The amount of ash in anthracite coal interests every buyer, and occasionally produces caustic comment, but there is a lack of authentic figures that will take the subject out of the realm of opinion and agitated fancy and. give a true picture of the quality of coal actually delivered. What per cent ash is to be expected when the coal is good, and when have we a right to make serious complaint?During the past summer the Bureau of Mines took 127 samples of 1000 pounds each, representing nearly 30,000 tons of anthracite is dealers' yards in seventeen cities in the State of Massachusetts. There were three objects in view, to discover the average and the variation in amount of ash in anthracite in some easily described area; to demonstrate standard sampling methods, and to learn something about the feasibility of itinerant coal sampling. Massachusetts was selected because its principal cities could be visited in a single season. There also appeared need for demonstration of standard sampling of coal, since a coal quality law had been passed in the State, to be administered by those unfamiliar with coal sampling."

Feb 1, 1924

Assist in controlling or extinguishing fires that occur in abandoned mine lands (AML) by providing a compilation of information on past fire control projects, the estimated extent of the current problem, and factors affecting the occurrence, propagation, and extinguishment of AML tires. Conventional fire control methods and their probable effectiveness are evaluated. Background Fires that occur in abandoned coal mines, waste banks, and coal outcrops constitute a serious health, safety, and environmental hazard from toxic fumes, deterioration of air quality, and subsidence. Although fires on AML occur in every coal-producing State, the severity of the problem varies, with most underground fires occurring in Kentucky, Pennsylvania, and Wyoming. Surface fires are prevalent in Kentucky, Pennsylvania, and West Virginia. Methods to extinguish or control AML fires, including excavation, fire barriers, and scaling, are generally expensive and have a relatively low probability of success (see figures 1 and 2). Bureau of Mines Study The Bureau compiled information from a variety of sources and found that the problem of AML fires is a serious one. Such fires can involve a high degree of hazard and can be difficult and costly to control. AML fires usually involve smoldering combustion in outcrops, waste banks, or abandoned mines. Given the nature of these fires, it is unlikely that the extent of the problem or the cost of solutions will decrease in the near future.

Jan 1, 1992

By Alan H. Goode

The advancement of high-temperature drilling fluid technology for application in geothermal environments is part of the Bureau of Mines program for more efficient development of our Nation's energy resources. The bentonite constituent of water-base drilling fluids is sensitive to destabilization by high-temperature and salinity. A substitute material for bentonite, phosphate slime, which is reported to be saline resistant, was considered. These studies show that spray-dried slime suspensions have more favorable rheological behavior, but poorer filtration properties, as compared with bentonite suspensions.

Jan 1, 1975

By C. M. Flynn

The Bureau of Mines prepared and investigated xanthated sawdust adsorbents to determine their effectiveness in removing heavy metal ions from dilute aqueous solutions, mine-drainage waters, and brines. Stripping of the metal values from the metal-laden adsorbent was also investigated. The treated sawdusts had an adsorption capacity of 0.3 to 0.4 meg/g dry adsorbent for Mn, Co, Ni, Cu, Ag, Zn, Cd, Hg, or Pb from feed solutions with pH 5 to 6. The feed solutions tested included mine-drainage waters and geothermal brine. Effluent metal concentrations as low as 0.05 to 0.1 mg/l were obtained at effluent pH values of 6 to 9. The order of affinity of metals for the sawdust adsorbent is Na«Ca~Mg~Mn<Zn<Ni<Cd<Pb~Cu. The presence of Ca, Mg, or Na in concentrations as high as 2 g/l does not seriously impair the heavy-metal adsorption. Metals were desorbed from the metal-laden adsorbent by elution with dilute mineral acids, sodium cyanide, or salts of ethylenediaminetetra-acetic acid.

Jan 1, 1979

Reduce the noise radiated by the auger miner cutting head (typically 105 dBA at the face) by 10 dBA without compromising the durability or productivity of the tool. Approach Research was conducted by the Bureau of Mines to identify the noise sources of auger miners with emphasis on the cutting head and coal cutting process. The overall noise level generated by the coal cutting process was found to depend greatly upon the structural characteristics of the auger cutting head. Based on this information, a quieter cutting head was

Jan 1, 1982

By A. A. Berk

In the course of a study of the formation of external deposits on tubes in water-tube boilers it became desirable to determine the sulfur dioxide (SO2) and sulfur trioxide (SO3) in the Due gases. Determinations made by the A.S.M.E. method for SO2 and SO3 in gaseous products of combustion did not give accurate results. It was found that minute quantities of copper, present in the flue gases from the coal in use, caused oxidation of sulfite in the absorption bottle and that the carbon dioxide (CO2) in the flue gases caused high values for SO2. The A.S.M.E. test procedure was revised to prevent oxidation of sulfite in the absorption bottle and to allow for the effect of CO2; subsequent analyses of flue gases produced reliable results. The revised procedure is described.

Jan 1, 1950

To provide a method for locating trapped miners promptly and accurately. The Approach: Develop a wireless emergency system that is intrinsically safe, compact, easy to operate, reliable, sturdy, and economical. How It Works: A (one transmitter has been developed under Bureau of Mines contracts. The transmitter weighs only a few ounces, is powered by a cap lamp battery, arid can be carried on the miner&apos;s belt. A compact loop antenna, which could either be carried by the miner or strategically located in the mine, is used to generate a magnetic field that is sensed by a mobile receiver on the surface. When needed, the antenna is deployed to form a single loop. In mines where the overburden is less than 600 feet, a loop of No. 19 wire approximately 30 feet in circumference is normally adequate. This antenna weighs less than one half pound. In deeper mines, a heavier wire and bigger loop is required; a No. 10 wire deployed around a pillar has been used.

Jan 1, 1974

Engineering controls for overburden drilling include dry dust collection systems, wet dust suppression systems, and enclosed cabs [Zimmer and Lueck 1986; Volkwein et al. 1979]. Proper maintenance of the dust suppression system is critically important for drills using dry dust suppression methods. Failure to rigorously maintain these systems will result in inadequate dust control. Acute silicosis has been reported in miners operating equipment that relies on dry dust suppression [NOSH 1992].

Jan 1, 1997

By Ruth A. Holmes

A Bureau of Mines method for recovering nickel, cobalt, and copper from low-grade domestic laterites is described, which includes the unit operations of solvent extraction and electrowinning. Previous Bureau work indicated that addition of Na2S04 (sodium sulfate) to the nickel electrolyte improved current efficiency in nickel electrowinning. The present study determines the compatibility of Na2S04 with nickel strip-ping in the solvent extraction operation of the Bureau method. The effect of adding 100 g/l Na2S04 on nickel stripping, phase disengagement, and pH was determined in comparative laboratory-scale tests. In continuous-circuit testing, Na2S04 reduced stripping efficiency to the extent that five, instead of four, strip stages were required for complete stripping of nickel from the loaded solvent. In tests made in a phase-disengagement cell that had a variable settler area, the addition of Na2S04 did not significantly affect phase separation characteristics. The pH of the nickel electrolyte in the temperature range of 20° to 65° C was also unaffected by the addition of Na2S04. An economic evaluation showed that the energy saved by adding Na2S04 to the electrolyte would more than offset the cost of adding another stripping stage.

Jan 1, 1983

By Howard E. Parkinson

Since 1969, the Department of Interior, Bureau of Mines, has carried out communications research. Research has been directed toward developing emergency and nonemergency mine communications. This paper gives an overview of the progress made in the last two years. Particular emphasis is given to the overall program, noise and signal measurements, systems studies, guidelines, products, and demonstrations now being carried on in operating mines.