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By C. Stephan, E. Weiss, J. Trackemas, M. Sapko

The National Institute for Occupational Safety and Health (NIOSH), Pittsburgh Research Laboratory (PRL), in collaboration with the Mine Safety and Health Administration (MSHA), the mining industry, and seal manufacturers recently conducted a series of full-scale experiments within the underground experimental mine at PRL’s Lake Lynn Laboratory. The purpose of the experiments was toe valuate the explosion-resistant characteristics of several new seal designs for rapid deployment during mine emergencies. These seals can be deployed in 6 to 10 hr and are capable of with standing explosion overpressures in excess of 140 kPa (20 psi). These novel seal designs use available mine materials, do not require conventional rib hitching, and, most importantly, can substantially reduce exposure time for coal miners during sealing and mine recovery operations.

By R. Barany

The heat of formation at 298.15 ° K of muscovite was determined by solution calorimetry . The value obtained for the heat of formation from the elements was -1,421.2 ± 1.3 kcal / mole , and the value for the heat of formation from the oxides was -55.9 ± 1.3 kcal /mole .

Jan 1, 1964

By E. G. King

The work described in this Bureau of Mines report was undertaken to fill a need of industry for high-temperature heat-content data for uranium tetrafluoride. Without such data, heat balance evaluations of processes involving this substance are seriously hampered. Measurements of the heat content of uranium tetrafluoride were conducted at temperatures from 298° to 1,350° K. The melting point and heat of fusion were determined. The results are presented in suitable tabular form, and representative heat-content equations are included.

Jan 1, 1961

By M. K. Larson, B. G. White

Researchers at the National Institute for Occupational Safety and Health (NIOSH) are investigating the causes and mechanisms of roof failure in underground mines. It is expected that a better understanding of these causes and mechanisms will lead to better layout and support designs that will help prevent accidents and fatalities associated with fall of ground. Two numerical experiments were conducted by NIOSH researchers using the Fast Lagrangian Analysis of Continua (FLAC) computer modeling program with a strain-softening continuum to simulate fracture zones. Two models, one of a round hole in a plate and one of a rectangular opening, were constructed and boundary conditions were applied to simulate far-field shear. The Particle Flow Code in Two Dimensions (PFC2D) computer program was used to look at the effects of far-field shear in generating fractures around an underground opening, but these models are preliminary until boundary conditions, strengths, and stiffnesses are matched to the FLAC models. Results showed that shear zones propagated from the opposite corners of openings in directions that appeared to be determined by opening shape and far-field stress. Tensile failures also formed and extended away from these shear zones. The consistent direction of shear deformation with respect to far-field shear provides a plausible explanation for preferred directions of shear as seen in geologic environments.

By Thomas M. Barczak

he stiffness characteristics of longwall shields were investigated in this Bureau of Mines study. Since longwall strata activity is characterized by roof-to-floor and face-to-waste displacements, a model with two degrees of freedom was used to describe the load-displacement relationship of the shield structure. The model considers the support as an elastic body and relates horizontal and vertical resultant forces acting on the support to associated displacements as a function of the stiffness of the support structure. Stiffness coefficients under full canopy and base contact configurations were determined by controlled displacement loading of longwall shields in the Bureau's Mine Roof Simulator (MRS). Three two-legged longwall shields of different manufacture were investigated. The stiffness characteristics of these shields were evaluated relative to two parameters, namely, shield height and setting pressure. The test results indicate a reduction in shield stiffness for increasing height. Setting pressure was found to have less of an effect on shield stiffness, producing only a slight increase in stiffness as setting pressure increased. Similar trends were observed for all three shields, indicating a similarity in stiffness characteristics for shields of the same basic configuration.

Jan 1, 1988

By Launa G. Mallett, Dana Reinke, Charles Vaught, Michael J. Brnich

As mines become safer and major disasters fewer, the number of experienced emergency responders is decreasing. This decrease will create a gap in response expertise which could have serious ramifications during future mine disasters. While working toward safety goals which may make emergency response obsolete, it would be reckless not to acknowledge that the potential for disaster still exists and that the protection of miners in such circumstances must remain a priority. The Mine Emergency Response Interactive Training Simulation (MERITS) is a computerized mine emergency simulation that meets a variety of needs. It allows personnel in leadership positions to test their knowledge and skill. Groups of individuals composed of representatives from mining companies, labor, and government agencies can practice working together during the simulated mine emergency much in the same way an actual emergency would require. An individual could also run the program to enhance his or her response skills. With this training tool, responders will be able to learn from their mistakes before facing situations with potentially catastrophic consequences. This paper discusses MERITS and its use in providing command center training.

Provide an instrument for continuous remote monitoring of carbon monoxide concentration in underground mines. Approach A carbon monoxide fixed? point continuous monitor consists of two modules. A line-powered control module is designed to power a remote transducer module; provide continuous readouts, visual and audible alarms, operational checks; and activate fans and equipment shutdown circuits if preset CO concentration levels are exceeded. How It Works The control module must be used in conjunction with a single transducer module. Developed under contract. the control module is a wall-mounted Instrument which contains a readout and alarm capability and power supply

Jan 1, 1981

By J. M. Stuve

Provisional values for the heat of formation of europium trichloride and europium sesquioxide were determined by solution calorimetry utilizing europium metal of more than 99-percent purity. The resulting values for the heats of formation of Eu203 (cubic) and EuCls (hexagonal) were -386,970 ±l,200 cal/mole and -218,740 ±650 cal/mole, respectively, measured at 298.15° K.

Jan 1, 1965

By W. W. Adams

luring the past two years the Bureau of ?,lines has been receiving from 100 to 150 coal mines in various States a report of each accident causing death, permanent total disability, permanent partial disability, or temporary disability lasting beyond the remainder of the day or shift on which the accident occurred. For each 100 accidents in these groups, there are perhaps from 35 to 45 accidents that do not disable the employee beyond the remainder of the day, and of these fraction-of-a-day accidents the Bureau has compiled no statistics. Information revealed by the reports is to the effect that falls of roof and coal in bituminous coal mines are responsible for 28 per cent of the temporary injuries to underground workers and 33 per cent of the days lost from all temporary injuries underground; they also indicate that falls caused 59 per cent of the deaths from all causes underground. Figures compiled by R. N. Hosler, of the Pennsylvania. Mine Rating Bureau, and covering accidents in bituminous; minis in that State, chow that 61 per cent of the deaths underground during the years 1917-1921 wore due to falls. Neither of these percentage figures includes deaths in major explosions; figures for all bituminous mines in the United States during the five years 1920-1024, inclusive of deaths in major explosions, show that 52 per cent of the deaths underground and in shafts were due to falls of roof and coal.

Jan 1, 1925

By A. A. Afshari, D. G. Frazer, C. F. Stanley

"INTRODUCTIONThe primary function of the lung, i.e. gas exchange, occurs in peripheral units termed alveoli• Diagnosis of lung dysfunction ls therefore dependent on techniques to evaluate the status of the peripheral airways. Since these airways and alveoli are very small, it is difficult to determine directly how they function or how the function is changing due to disease. Yet this unde1·standing is critical to the design of instrumentation to detect early changes in lung function due to disease.An interesting hypothesis describing one aspect of small airway function has been proposed by Frazer (1) as gas trapping due to the formation of menisci in the airways. An additional study (2) proposes that the breaking and possibly the formation of these menisci could generate lung sounds, i.e. crackles. These lung sounds were recorded by placing a microphone at the trachea of an excised rat lung. The lung was degassed and then inflated and deflated. At points along the path of inflation, lung sounds were recorded. However, determination of the origin of the sounds was not attempted due to the difficulties induced by contacting the lung st1rface with a microphone.The purpose of this paper is to describe a non-contacting, whole field technique to monitor and describe the movements of the lung surface during inflation - deflation cycles.HOLOGRAPHIC INTERFEROMETRYHolographic interferometry is a full field, non-contacting and non-destructive technique that measures deformations of an object with a sensitivity in the order of the wavelength of light. A laser beam is split, with one beam reflected from an object and the other used as a reference beam. Both beams combine to produce a hologram of the object on a photographic plate. The process utilizes the concepts of interference, i.e. the two wave amplitudes will add at the points where the difference in optical path lengths over the exposure period is zero or a whole number of wavelengths and will subtract at other points."

Jan 1, 1989

By George S. Koch

The distribution of gold in part of the Getchell mine, Humboldt County, Nev., is presented through the statistical analysis of 956 assays of rock cuttings from wagon-drill holes. Two methods to predict grade in undeveloped parts of the ore body are evaluated, and the possibility of sampling bias is tested. The distribution of gold is compared with that in three other Nevada gold deposits of the same type characterized by gold particles mostly of submicron size associated with carbonaceous rocks, and also with that in deposits with coarse-grained gold. Usually, fewer samples of a given type are required to make a satisfactory grade estimate for submicron deposits than for coarse-grained deposits. The economic consequence is that submicron gold deposits are likely to be less expensive to sample and evaluate than coarse-grained deposits.

Jan 1, 1970

By L. A. Haas

The degree of reduction of various silica-graphite mixtures was studied in a batch reactor to determine optimum physical conditions for maximizing the carbothermic reduction of silica. The extent of interaction was determined for reactant mixtures in loose powder and briquet forms at pressures less than 0.01 torr and temperatures up to 1,445° C. Molar ratios were varied from 0.05 to 6.5 with maximum reaction at a ratio of about 1.5. The solid-solid reaction did not appear to involve gaseous intermediates. The extent of reaction better correlated with the number of interparticle contacts than with the true surface area of the reactants. Carbonized dextrose was a better reductant than graphite.

Jan 1, 1968

By Stephen Gerard Sawyer

The Bureau of Mines developed a method for analyzing elastically certain types of protective cabs and canopies used on underground electric face equipment. The method is based on plane frame theory, and to be amenable to analysis by this method, cabs and canopies must contain symmetry about one plane. Additionally, protective structures with one or more top members in the long direction that do not frame into the columns should be approximately twice as long as they are wide and have two or more internal top members in the short direction. The assumptions and limitations of the plane frame method as regards analysis of three-dimensional cabs and canopies are discussed. A step-by-step procedure for application of the plane frame method is given, and three example canopies are analyzed following this procedure. Elastic strengths calculated for the three example canopies compare within 10 percent of those computed by the more complicated space frame analysis. Formulas employed in plane frame analysis of cabs and canopies are given in the appendixes.

Jan 1, 1973

By A. Z. Dimitroff, A. C. Moschetti

An improvised rock- dust disseminator, consisting of a 10-gallon galvanized metal milk can that dispenses rock dust in return air currents by the injection of compressed air has reduced the float dust explosion hazards at the Koehler coal mine, Koehler, N. Mex.

Jun 23, 1964

By N. F. Le Jeuns

For a number of years the Bureau of Mines has conducted semi-annual surveys to determine the changes in motor gasoline being sold in the United States. It was pointed out in the previous survey that there was an apparent tendency toward greater uniformity in the character of gasoline marketed in the United States. This practically uniform tendency which continued from April, 1917 to January, 1923, has been interrupted in the, present survey, as shown by an examination of the column marked "Difference," as given in Table 1. The figures in this table were obtained by averaging the end points of the least volatile and most volatile samples of gasoline. For example, of 850 samples analyzed in 1919, the 10% ,(85 samples) having the highest end points and the 10% having the lowest end points mere grouped, and the end points of each group averaged. These averages are represented in the table as the "Maximum 10%" and the ?Minimum 10%? respectively. The same process was used on the other surveys.

Jan 1, 1923

By C. A. Wilson

The Bureau of Mines started a continuing program to investigate and evaluate analytical techniques to assist governmental agencies to select simple, rapid, reliable methods for crude oil spill identification. Six crude oil samples were analyzed to evaluate gas-liquid chromatography, atomic absorption spectrophotometry, infrared spectoscopy, sulfur and nitrogren determinations, mass spectrometry, nuclear magnetic resonance spectroscopy, and ultraviolet spectrophotometry. Samples were studied from the following selected fields: El Morgan, Egypt; Duri, Indonesia; Minagish, Kuwait; Bachaquero, Venezuela; Gach Saran, Iran; and Prudhoe Bay, Alaska. These samples were chosen to represent high-production fields that are likely to be involved in oceanic transport. Over 50 years of Bureau of Mines analytical research on petroleum served as the basis for evaluation of the experimental results to determine which of the methods are effective techniques to identify crude oil spills. Gas-liquid chromatographic analysis, atomic absorption spectrophotometric analysis, and sulfur-nitrogen determinations are recommended as the most useful of the techniques investigated.

Jan 1, 1975

By Van E. Shaw

Fusion of an 86-percent euxenite concentrate with ammonium sulfate was investigated by the Bureau of Mines. Reaction for 4 hours at 400° C results in conversion of both the rare-earth elements and the titanium-columbium components to water-soluble compounds. Similar results are obtained with ammonium bisulfate. Stirring the fusion mass decreases the reaction time substantially. Alternatively, treating the fusion product with a 3-hour, 650° C calcining step renders the non-rare-earth constituents insoluble, thereby allowing selective leaching of a pure rare-earth fraction with an overall yield of 97 percent.

Jan 1, 1967

By R. S. Olsen

The Bureau of Mines is engaged in a continuing research effort toward the recovery of alumina from kaolinitic clay and other nonbauxitic domestic minerals. Hydrochloric acid extraction of calcined clay is among the acid processes under consideration. Although aluminum is easily leached from calcined clay, the presence of fines and slimes in the leached residue has hindered the application of this and other acid leaching processes. A clay feed preparation method was therefore developed that eliminated the slimy nature and the separation problems normally associated with leached clay residues. The preparation process consists of crushing the raw clay to minus 20 mesh, dampening the crushed clay with a fine water mist while tumbling on a rotating disk, and calcining the misted clay at 750° C. The misting process increases residue settling rates threefold to 9 cm/min (18 ft/hr) and filtration rates by two orders of magnitude. Leaching-kinetics were determined for misted clay feeds in a batch, stirred-tank reactor. Rapid leaching occurred during the first 85 to 90 pct of the extraction. The linear relationship of extraction to time during this initial phase corresponded to a zero order reaction with a rate constant of around 10 pct/min.

Jan 1, 1981

By R. C. Wang

Solid-liquid flow in different pipe geometries was investigated. This investigation was conducted by measuring delivered solids concentration and head loss. The delivered solids concentration was measured to study the effect of pipe geometry on the minimum carrying velocity above which solids do not lag behind the fluid. Head loss was measured to study the effect of pipe geometry on the friction loss. A mathematical formula was developed for determination of the minimum carrying velocity. Darcy-Weisbach's equation and Durand's equation were used for comparison of head losses of pipe shapes. Of the different pipe shapes studied, each having the same interior cross-sectional area, the rectangular pipe with the wide side oriented as the base yielded the lowest minimum carrying velocity at high solids concentrations. The minimum head loss at low velocity and high solids concentration also was attained with this pipe. Although the circular section is known to be the best for transporting liquid only, the present study suggested that pipe geometry is a factor in lowering the operating velocity and reducing head loss in solid-liquid flow.

Jan 1, 1973

By R. V. Ramani, R. Stefanko, G. W. Luxbacher

TEST DECK – ALTMETER SURVEY WITHOUT PLTTMETER TEMPERATURE CCRRECTION DATA INPUT

Jan 1, 1977