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By W. H. Eddy

The Bureau of Mines conducted laboratory batch flotation tests and continuous pilot plant flotation tests on a complex calcareous fluorspar ore from Cave-in-Rock, Ill., to determine the technical feasibility of producing commercial-grade concentrates by the sodium fluoride-calcium lignin sulfonate-fatty acid method of concentrating fluorspar previously developed by the Bureau. The continuous flotation tests, treating about 150 pounds of ore per hour, produced fluorspar concentrates assaying 96.4 percent CaF2; 90 percent of the fluorspar was recovered.

Jan 1, 1967

By H. P. Rue

For the proper control of gasoline treating plants there is need of a quick test for corrosion. In "sweetening" gasoline that is, in treating it to remove evil smelling mercaptans or to convert them to disulphides or sulphides the sodium plumbite ("doctor") method is generally used. This method involves agitation of the gasoline with "doctor solution's (sodium plumbite made by dissolving litharge in a solution of caustic soda) in the presence of free sulphur3. One of the common mistakes in the technique of this process is the addition of too much free sulphur, which will dissolve in the gasoline and cause it to be corrosive. In the operation of a continuous sweetening; or treating plant, a check on the corrosiveness of they product is imperative at all times. The copper-strip test commonly used in specifications take, so long to perform that the plant may fail to function properly for some time before the operator discovers it. The writer has investigated a rapid corrosion test method involving the use of metallic mercury, recently developed by Messrs. G. T. Granger, refinery superintendent, and A. B. Comstock, chief chemist, of the Barnsdall Refineries, Inc., Okmulgee, Okla. They have used this test successfully for several months in controlling the operation of their continuous treaters any have come to the conclusion that it has several advantages over the copper-strip test. Chief among these is the time caved, as the copper-strip test takes at least one-half hour, while the mercury test can be wade in about five minutes. It is very evident that this is an important item in controlling a continuous treater.

Jan 1, 1928

By E. J. Gleim

Many people consider the mining of coal to be an extremely hazardous occupation; but it should be remembered that most large industries have to meet special conditions which, if not dealt with properly, might become hazards to life and property. Mining men may not always be fully aware that some practices and certain equipment that is incorrectly designed or maintained can lead to dangerous conditions. In endeavoring to help the coal-mining industry to prevent accidents and disasters, the Bureau of Mines has engaged in a program of education on conditions and practices that must be avoided. An effective way to teach safety is by visual demonstration. For example, it is generally known that certain kinds of electrical flashes have ignited explosive atmospheres in mines, but actually to see and hear explosions caused by electrical sparks of different size and character under laboratory control is likely to teach a much more emphatic and lasting lesson than would be learned by merely reading about them. The interest manifested by those who witness the demonstrations seems to prove that this is true. The purpose of the demonstrations is not to discourage the use of electricity in mines, but rather to indicate what types of equipment (including some generally regarded as harmless) can ignite gas and what safeguards have been developed to prevent such ignitions. It is hoped that this information will improve the ability of mining men to cope with underground hazards.

Jan 1, 1937

By D. A. Paice, A. B. Shimp

A test program was conducted to determine the adequacy of molded case circuit breakers for dc electrical systems in coal mines. Mine electrical system parameters and the most severe operating conditions to be expected were determined. Tests of the interrupting capabilities of several molded case breakers were made under the worst conditions to be expected. Continuous and pulsed current carrying capability of the breakers was also investigated. Breakers from two different manufacturers passed all tests successfully. Based on the results of these tests, a set of guidelines for applying molded case breakers to dc systems has been prepared.

Jan 1, 1975

By A. A. Cochran

Methods of preparing small heats of steel containing radioisotopes were developed, and the techniques of stripping film autoradiography were used to detect and study the carbide and sulfide phases in titanium-bearing steels. Metallography had revealed areas of titanium sulfide and ferrite or pearlite adjacent to areas of titanium carbide and ferrite, and unidentified, irregular phases at the boundaries between these two areas. Sulfur 35 was used to deter-mine the extent of the titanium sulfide inclusions, and carbon 14 was used to delineate the titanium carbide phase. Individual radioactive areas were located with a resolution of approximately 10 microns. A general background exposure that was not correlated with microscopically visible phases was observed in the carbon 14 autoradiographs. The evidence from both sulfur 35 autoradiographs and carbon 14 autoradiographs indicated that the unidentified inclusions were sulfides rather than carbides. INTRODUCTION The use of radioisotopes to facilitate the work at the Rolla Metallurgy Research Center was expanded in fiscal year 1959 when the Bureau of Mines authorized the installation of an intermediate-level radioactivity laboratory. Before this time, sealed cobalt 60 sources had been employed for radiography, but no tracer work was done. The primary objective of the first experiments conducted in the new laboratory was to supplement physical metallurgy investigations of selected problems in steel research.

Jan 1, 1962

By Frank E. Cash

The iron-ore ranges in the Lake Superior district are the liarquette in Michigan, Menominee and Gogebic in Michigan end Wisconsin, and the Vermilion, Mesabi, and Cuvuna in Minnesota. These ranges produce about 85 percent of the iron ore mined in the United States. Accident experience in connection with this production is better than that of the regions producing the remaining 15 percent. Production and shipments vary slightly from year to year but closely approximate each other over a period of years. During the 4-year period 1940 to 1943, inclusive, 323,667,599 long tons of iron ore was shipped from the Lake Superior district.4/ Michigan and Wisconsin shipped 65,386,608 tons, or 20.2 percent of the total, and employed approximately 15,000 men; Minnesota shipped 258,280,991 tons, or 79.8 percent of the total, and employed approximately 10,000 men. The tons produced per man employed is much, greater in Minnesota than in Michigan and Wisconsin owing to the large open-cut production in Minnesota.

Jan 1, 1945

By R. V. Ramani, W. Miola, R. Srikanth, S. C. Soboleski

"Dust control in high-production longwalls requires attention to operating practices and ventilation schemes. Several studies have shown that the shearer is the major source of dust on a longwall face. Support movement has not been regarded as a major source of dust in US longwalls. Yet, under certain conditions, 31% of the shearer operator's dust exposure can be due to support movement.Several methods have been developed for the control of shield-generated dust. But the need for better methods is apparent. In this paper, the amount of airborne, respirable dust generated per shield move is estimated from specially designed experiments on longwall faces. Ten experiments were conducted on five longwall faces in four mines. Each experiment involved one face visit and lasted three to six hours. The contribution of shield movement to the airborne, respirable dust concentration immediately downwind of the shield move varied between 0.12 and 1.75 mg/m3 in the five longwall faces. The mass of airborne, respirable dust gener-ated by shield movement was found to vary between 39 and 386 mg per shield move. The results from this study reveal that control of dust from longwall shields requires a combi-nation of approaches involving alternative operating prac-tices, reducing shield dust generation rate, increasing face air flow and decreasing personnel exposure.IntroductionIn 1992, longwall mining accounted for about 36% of US underground coal production, a 240% increase from a decade ago. The absolute longwall tonnages were 46 and 133 Mt (51 and 146 million st), respectively. Compared with room-and¬pillar mining systems, the longwall mining system is charac¬terized by higher recovery, enhanced safety and higher pro¬ductivity.However, personnel dust exposure on a longwall face is higher than in other types of mining. According to Mine Safety and Health Administration (MSHA) data, fewer longwalls were in continuous compliance with the applicable dust standard in 1992 than in 1989.Controlling shearer-generated dust and reduction of per-sonnel exposure to airborne dust have commanded attention in the design of longwall faces, operational practices and ventilation schemes. Studies in the United States and abroad have revealed that support-generated dust can be a major obstacle to compliance under certain conditions (Becker et al., 1989; Bradley et al., 1983; Jankowski and Organiscak, 1983; Jankowski et al., 1990; Organiscak et al., 1985)."

Dec 1, 1996

By Thomas E. Marshall, Roy H. Grau

The U.S. Bureau of Mines has developed an acoustic test for determining if a rock salt sample is from a "normal" nongassy salt face or from a gassy face where an outburst has the potential to occur. The test is based on the observation that a salt sample taken near an outburst-prone zone produces an audible popping sound when it is dissolved in water. The sound is produced when pressurized gas that is trapped in salt samples is released. In the acoustic test, the sound is electronically measured, digitized, and transmitted to a microcomputer; the output is an average decibel value that classifies the sample as "normal" or "outburst." The acoustic test procedure and equipment are described, and raw test results and data analysis are shown. Results are also shown for several salt samples that were analyzed using a laser Raman microprobe.

Jan 1, 1990

By H. R. Shell, Robert C. Johnson, Wilbur H. Warwick

Alpha silicon nitride fibers , Si3N4 , were successfully grown in graphite crucibles by a new method utilizing silicates and silicon ( S in equations below) as sources of silicon and using carbon , aluminum , and silicon as reducing agents (R in equations below ) . The basic reaction mechanism is believed to be generally as follows : 1,300 - 1,500 ° C S + R + N₂ SiO + RO + N₂ › 3Si0 + R + 2N₂ _1,300 - 1,500° C 3RO + Si¸N • ( 1 ) ( 2 ) A build - up of coatings on the solid raw- material particles hindered the evolution of silicon or silicon monoxide vapor and thereby slowed down further formation of silicon nitride fibers . Free oxygen in the crucible caused the formation of amorphous silicon dioxide ( SiO2 ) fibers . This problem was solved by passing , entering , and exiting gases through layers of lump graphite inside the reaction vessel . The silicon nitride fibers grew best around 1,400 ° C. Nitrogen flow rates from 4 to 6 liters per minute were adequate . The fiber widths were generally only a few microns whereas their lengths sometimes reached one - quarter inch or more . Chemical and X- ray analyses indicated that bulk fiber samples were usually 80 to 90 percent Si3N4 . The fibers had good oxidation resistance to about 1,260 ° C. Thermal shock resistance was excellent . Electrical resistance was determined .

Jan 1, 1964

By G. S. Rice, R. V. Wheeler

"In September 1923, a proposal was made through official diplomatic channels by the British Safety in Mines Research Board to the United States Bureau of Mines for ""closer cooperation between the two countries in investigations into the causes and means of prevention of mining dangers."" This proposal was cordially accepted by the Bureau of Mines and was officially approved.In the spring of 1924 cooperation was .formally begun. It contemplated, as stated officially, ""full exchanges of information, a joint program of research, and periodic exchange of personnel so as to assure concordant results. By making the resources of both organizations available it will hasten the attainment of results, will secure better: checks for, accuracy, and in the end will save money for both by avoiding duplication and repetition.""This joint work has been carried-on successfully since that time and has developed valuable results, reports on which have been issued from time to time. The progress report which follows gives the results of the studies and work carried on in 1929.During 1929 all the phases of our cooperative research, begun in previous years, have developed normally. The exchange of formal monthly reports on all programs of mutual interest has been continued and has proved an invaluable, means of maintaining contact between the investigators of both organizations. There has been no diminution in the exchange of routine progress reports on specific subjects or in direct correspondence. The interchange of personnel has been maintained, and we can say that the mutual benefits to be derived from this form of cooperation are so great as to be difficult to overestimate. It leads to an appreciation of methods of research and modes of thought in the interpretation of results obtainable in no other way, and engenders a frankness and intimacy which must continuously enhance the value of future cooperation.Dr. S. R. Katz, who was assigned for service with the Safety in Mines Research Board in April, 1928, returned to America in May, 1929. During his stay in England he completed, in cooperation with members of the board's staff, the equipment of a gas-mask laboratory and designed and tested a new form of gas-mask canister. A publication of the Safety in Mines Research Board dealing with this investigation has been prepared and approved and will .be .issued in the near future. In additions Dr. Katz imparted to those with whom he was associated much of his knowledge and technique regarding his particular subjects. He delivered two lectures to the board's staff, the subjects be ""Gas Masks"" and ""The Intensity of Odors"", and gave papers before the Midland Institute of 'lining Engineers and the Birmingham University Mining Society on the subject of ""Industrial Gas Masks""."

Jun 1, 1930

By Robert L. Thorne

Cassiterite deposits on Sullivan Creek in central Alaska were investigated by the Bureau of Mines in the spring of 1943. Gold miners in the area have been recovering cassitorite each season as a byproduct of gold placer operations. Approximately 300 tons of tin concentrates have been shipped from the district. The deposits were sampled though trenches and small shafts. An average tin content of 0.28 pound per cubic yard was indicated. A detailed description of sampling methods and sample analyses is presented in this report.

Jan 1, 1948

By J. R. Long

The investigations described herein are concerned with a portion of a systematic research, by the Federal Bureau of Mines on ductile titanium. The Bureau's work on the metal has resulted in development of a semi commercial process for the preparation of titanium and has also made available significant information on the fabrication and physical properties of this new strong, light, corrosion-resistant metal. Considerable interest has been aroused by this work, and a number of other laboratories have begun similar investigations. However, the necessity for Consolidating titanium by normal powder metallurgy methods presents difficulties in producing commercial forms and shapes on a large scale. This investigation was therefore undertaken for the purpose of improving the technique for consolidation of titanium powder into solid nonporous metal.

Jan 1, 1949

By W. A. Cole

As the mines get older and the active workings get Farther and farther away from the original mine openings, it becomes increasingly difficult and expensive to ventilate most coal-mines properly. At the same time, the avenues of escape for those employed underground have become so extended' as often to make it impossible for them to make their way out of the mine in the event of a fire, mine explosion, or other emergency. Where such Conditions exist, the only satisfactory solution is to make new ventilation and emergency-escape openings near the active mine workings. At most mines this would necessitate sinking shafts, which is often slow and expensive.

Jan 1, 1945

By John F. Wiggert

The first signal system used in the Homestake mine between the cagemen and hoisting engineers was a mechanical one. It consisted of small cables or jointed steel rods hung in the cage compartments and counterbalanced with weights or springs. These cables or rod strings were connected to the mechanically operated gongs at the engineers' positions by means of bell cranks and steel wires. At the various stations the bell lines were also fitted with bell cranks and connected levers, so that the cagemen could operate the bells from the stations when they were handling rock or other material and not riding on the cages. Such a system was inherited from the days before extensive electrical development. It served quite well for shallow shafts, but for depths of a thousand feet or more it was very slow and cumbersome. It required consider-able muscular effort to operate it quickly, because of the inertis of its great weight and also because of frictional resistance. The maintenance cost was quite high because of the many wearing parts.

Jan 1, 1937

By D. E. Shanks

As part of its program to lessen dependence on foreign bauxite as the Nation's primary source of cell-grade alumina, the Bureau of Mines is investigating sulfuric acid (H2S04) leaching procedures for the recovery of alumina from domestic aluminous materials. The successful application of a H2S04 leaching process depends on the recovery of the aluminum values in an easily washed and filtered form, containing a minimum of water to be driven off in the subsequent calcination step. This goal was met by the high-temperature hydrolysis of simulated aluminum sulfate [A12(S04)3] leach liquor. Crystalline, insoluble aluminum hydroxy sulfate [A1(OH)S04], which had a water-to-alumina mole ratio of 1:1, was produced. Eighty-six percent of a solution containing 127 g of A12(S04)3 per liter and 76 pct of a solution containing 336 g of A12(S04)3 per liter were hydrolyzed to insoluble aluminum hydroxy sulfate by autoclaving for 1 hr at 320° C and rapidly quenching to room temperature. Higher operating temperatures were precluded by corrosion of the autoclave. The yield of aluminum in the hydrolysis product increased with increasing hydrolysis temperature and decreasing A12(S04)3 concentration.

Jan 1, 1981

By H. S. Hardman, G. T. Adams, Will H. Goghill

"Usually a newly developed machine leaves the factory ""on a wing and a prayer."" The manufacturer hopes that the operator will hasten to report defects. In turn, when the suggestions arrive the manufacturer makes the required changes and maintains close collaboration with the operator. Thus the history of our machines of today is written.Laboratory concentration tables are exceptions to growth by experiment and collaboration. Their operation never enters directly into the cost sheet; they are seldom used for longer periods than 10 minutes; and the experimenter, while hurrying to another job, accepts the table, good or bad, for a quick test on his ore. Thus we go back about 50 years when we use the preset in factory-built laboratory table.The Southern Experiment Station, Bureau of Mines, in cooperation with the University of Alabama, recognized the existence of a tabling problem net usually considered. That is, instead of using the table to test the ore, the ore was used to test the table. In this critical examination of laboratory table six defects were encountered (and remedied). They are:"

Oct 1, 1945

By Leroy Dockter

The grinding characteristics of lignite in a ball mill were investigated. The variables studied were initial lignite moisture content, degree of in-the-mill drying, and lignite source. The mill tested was a pilot-p1ant-size conical ball mill which had a maximum output of from 80 to 180 lb/hr pulverized product depending on the lignite and test conditions. The capacity of the test mill ranged from 82 to 103 lb/hr depending upon mine source, in pulverization of as-mined lignite with minimum drying, The capabilities of the ball mill could not be correlated to Hardgrove index of the individual lignites or other observed physical properties. Predrying lignite from its 35 to 40 percent raw moisture content to about 10 percent moisture before grinding improved the mill capacity 87 percent, compared to an increase in capacity of 74 percent with in-the-mi11 drying to the same product moisture.

Jan 1, 1967

By M. F. Dunn

A handbook to provide a quick reference guide for selecting and using jet fans in a variety of conditions was prepared. The document is intended for use by front-line supervision, ventilation engineers, and mine planners. Included are discussions of jet fan characteristics, selection and use critieria, and do's and don't's for easier operation, safety, and performance. The handbook is based on research at three underground metal/nonmetal mines having cross-sectional areas of 900 to 2,000 ft2.

Jan 1, 1983

By C. J. Mains

The gas -flow oil-shale retort is a continuous, crass flow, gas -to -broken solid heat-exchange system in which heat is transferred by convection from the gas to the solide.2/ This type of heat transfer presents a problem of analysis that cannot be solved by methods in common use. Solution of this problem is necessary for design, operation analysis, and predict ion wherever that type of heat exchanger is used. This report embodies a method for calculation of heat transfer coefficient and temperature histories of gas and solid in the gas- flow retort operating at equilibrium conditions. Detailed calculations are presented to show the application of the method explained in this report to conditions of an actual run made in the gas-flow retort. Although used here for a specific case, the method is applicable to all heat exchangers that are characterized by continuous, crossflow, gas -to-broken solid heat transfer. INTRODUCTION In any direct, gas -to -broken solid heat -transfer system, it is difficult to measure the temperatures of the gas and solid inside the heat exchanger. The driving force for heat transfer between the two media in the bed there- fore usually is unknown. The major resistance to heat transfer is in the gas film surrounding the solid particles, and the thickness of this gas film is neither uniform nor can it be determined readily. It is well to point out also that determination of the surface area of the particles is of poor accuracy. Since the driving force, the major resistance, and the surface area in the heat-transfer system are such uncertain quantities, It is not feasible to calculate the heat transfer by usual methods. All of the fore- going statements are true of the gas-flow retort; as a result, efforts were made to determine apparent heat-transfer coefficients and temperature histories of gas and solid in the heat -exchange bed by calculation using those data that were available. The heat -transfer coefficient calculated has the following dimensions: B .t .u. per second, °F., cubic foot of bed volume, where heat - transfer coefficients normally have the units; B .t .u . per hour, square foot, °F. Only the Schumann-Furnas formulas may be used to determine the heat- transfer coefficient and temperature histories in this type of heat exchanger.

Jan 1, 1953

By W. L. Falke

Procedures in which manganese compounds are reduced and the metal is volatilized and selectively condensed, a hitherto neglected area, were investigated. More than 95 percent of the manganese was recovered from high-melting-point ores whether vacuum volatilization or atmospheric pressure volatilization was used, but neither process is economically attractive under present price-cost conditions.

Jan 1, 1966