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By Volney Viana Nogueira

A recirculação interna de gases em bombas de vácuo é uma falha frequente em estações de desgaseificação de aço e está associada ao aumento dos tempos de processo, a um maior consumo energético e a não obtenção da pressão de trabalho adequada. O tratamento de tais desvios pode ser complicado pela falta de informação disponível sobre os modos de falha dos equipamentos. Este artigo descreve um método experimental para encontrar valores de referência para testes que podem ser realizados na planta para a detecção de não conformidades em bombas de vácuo constituídas de ejetores a vapor e condensadores; tal método é composto por testes lógicos, sequenciais e não intrusivos. São fornecidas tabelas com os valores esperados das grandezas testadas, assim como diversas causas de redução de desempenho e de perda de função dos componentes.

Oct 30, 2017

By Horace C. Porter

Much has been written of the changes undergone by coal in storage and the deterioration of coal through exposure to the weather. In order to obtain definite information for the benefit of the Government departments and of all who store coal in large quantities, a series of tests was begun in the fall of 1909 under the supervision of J. A. Holmes, then chief technologist of the United States Geological Survey, and was continued by the Bureau of Mines after its establishment in 1910. The tests were confined to determinations of the loss in heating value of the coals and did not include a study of other deterioration; for example, in coking quality or the yield of by-products in coking. The Bureau of Yards and Docks of the Navy Department cooperated in tests of New River (W. Va.) coal, a variety largely used by the Navy. A preliminary report presenting a brief account of the early results of these tests has been published by the Bureau of Mines as Technical Paper 16.a The detailed report is presented in this bulletin, which gives a full account of the tests and the analytical data covering a period of five years' storage. Data of somewhat similar experiments for shorter periods with gas coal from the Pittsburgh bed, with Pocahontas coal on the Isthmus of Panama, and with Sheridan, Wyo., subbituminous coal, which is used for railroad and other purposes in the West, are included.

Jan 1, 1917

By Armando Rivera, Ángel Cueva

El proyecto Mirador, ubicado en la provincia de Zamora Chinchipe en Ecuador, es un sistema mineralizado del estilo pórfido – cuprífero, tipo cobre – oro. Constituido por una zona superior de óxidos, adyacente a un área transicional de óxido –sulfuro dentro de una zona mineralizada con sulfuro hipógeno (calcopirita– pirita), tiene potencial para generar drenaje ácido de roca (DAR), lo que crea preocupación ambiental respecto de los recursos de agua superficial y subterránea. En este artículo se describen diferentes etapas de muestreos de los núcleos de perforación con variación en profundidades y litologías, el análisis de los factores que influyen en la transformación de residuos sulfurosos, y la realización de pruebas estáticas estándares y cinéticas.

Feb 28, 2019

By Medardo Echegaray

Desde el punto de vista de análisis químico se buscaba estudiar un método de determinación de fierro que ofreciese una buena precisión en una zona de concentraciones. En ese sentido, el presente texto señala la determinación colorimétrica del fierro a través del método de complejo aceto-férrico. No existe intlerferencia por el manganeso, fluor o níquel. El cromo interfiere cuando se encuentra en cantidades mayores a su máxima concentración permisible o sea 0.1 mg .

Mar 1, 1963

By Ronald Benito

El presente texto señala el algoritmo basado en grafos como la técnica que determina el límite óptimo de minado a cielo abierto. Por ello, se adaptó la técnica de Lerchs y Grossmann y intermedias (algoritmos) y fue usada para crear nodos, arcos y estructuras de árboles en tablas para determinar la máxima cerradura de un grafo.

Sep 1, 2013

By Otto Sandovel Zea

El compromiso de minería perfecta se limita no solo a la preservación del medio ambiente, sino a la prevención de riesgos por desprendimiento de rocas y aplastamiento en el interior de la mina. En ese sentido, el presente texto señala la factibilidad de minar a sección plena todos los tajeos a través de la simulación de las condiciones más favorables y desfavorables de la mina, determinando como la alternativa más viable la bóveda en arco. Dicha estructura otorga estabilidad a las labores de minado -en tanto da sostenimiento activo a través del (Shotcrete SFR y Pernos Hydrabolt), así como desarrolla mayor productividad y menores niveles de riesgo por desprendimiento de rocas, menores grados de sobre excavación y genera de vibraciones al haber implementado la voladura de Pre-corte en sus labores.

Sep 12, 2011

By J. C. Barcellos

El presente estudio describe el método de empleo para la determinación del espaciamiento óptimo de muestreo en la Mina Casapalca. La técnica comprende cuatro pasos: recolección y preparación de datos, procesamiento electrónico de datos, análisis de los resultados y la verificación de las conclusiones. Dentro de las conclusiones, se considera que los métodos estadísticos son los más útiles en la solución de los problemas de la industria minera , puesto que cualquier dato numérico pueden ser convertido a un número más simple a través de la computadora.

Nov 20, 1972

By Luis Huere

La calcopirita es uno de los minerales de cobre más difíciles de lixiviar. Si bien es posible generar un PLS en un medio muy oxidante, las recuperaciones son muy bajas como para considerarlo una alternativa de procesamiento de esta mena de cobre. Con el objetivo de elevar la recuperación de cobre en el PLS obtenido, en este estudio se realizaron diversas pruebas de lixiviación de un mineral de cobre calcopirítico para determinar los mejores parámetros de lixiviación que produzcan la mayor recuperación de cobre en el PLS que se dirige a la extracción por solventes y electrowinning respectivamente. Se realizaron prueban con oxidación por ozono, sulfato férrico, ozono-sulfato férrico, sulfato férrico-ozono y sulfato férrico con temperatura elevada. La prueba con mejor resultado fue la de sulfato férrico, pues produjo la mayor recuperación de cobre.

Sep 20, 2019

By Aníbal Gatañaga Coll

Dada la peligrosidad del sílice libre como principal problema en el campo de la higiene industrial, el objetivo del trabajo es controlar y evaluar la concentración de dichos polvos a través del uso de tres métodos: El método químico, el de difracción de rayos X y el petrográfico. El primero (N. A. Talvitie), utiliza un reactivo que descompone y disuelve a todos los constituyentes de la muestra, excepto al cuarzo, quedando calcinado y filtrado; el segundo método es eficaz, pero requiere de un equipo muy costoso, mientras que el método petrográfico muestra una mejor identificación de los minerales, determinando las cualidades de los materiales que se producen en la composición del polvo, así como precisa la pequeñez de las partículas encontradas en los polvos industriales y sobre todo de la capacidad del operador.

Jul 20, 1955

By C. H. Lau, I. T. Ng

Uniaxial Compressive Strength (UCS) of rocks is an important mechanical parameter for many civil engineering and rock engineering applications such as tunnel excavation, slope stability and foundation design. Macau is one of the world's fastest growing and most densely populated cities, many large and important infrastructures have been being continuously built using pile foundations which are designed to be supported by granitic bedrock. In Macau, the UCS of the granitic bedrock is required almost for every project involving pile foundations and is always measured directly from UCS test in the laboratory. However, direct measurement of UCS requires high quality rock core sample which is not only time-consuming and expensive but also requires high level of operating skill. In view of this fact, estimation of UCS using some empirical correlations will be more practical and efficient because they are relatively fast and economical compared to the direct measurement from UCS test. In the past, some empirical correlations had been established and widely used for estimating UCS of rocks in common engineering practice. However, it has been well recognized that the rock properties are generally varied with sites or geological regions in other words an empirical correlation developed from one region or one country may not be applicable for other regions or countries. Due to the reason that the empirical correlations for predicting UCS for granite are scarce in practice, in this study an extensive experimental program has been performed and a large database containing data such as UCS, Point Load Index (Is50), Schmidt Rebound Hardness (RL), porosity (?), water absorption (S), specific gravity (Gs) and dry density (?d) has been developed. An attempt has been made for developing a new empirical correlation for estimating the UCS of Macau granite. Accordingly, a comprehensive statistical analysis for correlating UCS with Is50, RL, ?, S, Gs and ?d has been performed and a local empirical relationship based on the developed database is proposed for obtaining reliable estimation of UCS for the granite of Macau. Finally, the performance of the proposed correlation is accessed by using another independent testing database developed in this study. It indicates that Is50, RL, ? and S have strong correlation with UCS whereas Gs, ?d have poor correlation with UCS. This study not only proposed a proper predictive empirical correlation for UCS determination for Macau granite but also provides detailed statistical information which is beneficial to engineers for obtaining better characterization of Macau granite.

Jan 1, 2015

By Gregoire Gutzeit

THE development reported in this paper was begun by the author a number of years ago, while he was a lecturer on complex chemistry and metallurgy at the University of Geneva, Switzerland, and in charge of that institution's research laboratory. Completion of the development and reduction to practice did not occur until last year at the Westport mill, laboratories and testing plant of the Dorr Company, where this method is now in general use for identifying and localizing the mineral constituents of both metallic and nonmetallic ores. It has proved to be a practical tool of the metallurgical staff at the Westport mill, devising unusual milling flowsheets for complex and refractory ore bodies. In a number of instances the findings have been successfully used as fundamental factors in the design and specification of complete metallurgical plants. Seven examples of the use of this method in solving practical milling problems are included in this paper. GENERAL OUTLINE The microscopic study of an ore, at first only of scientific interest, has proved extremely useful both in practical geology and in ore dressing. The binocular magnifying lenses for rough observation of the products of an ore-dressing plant have been in use for a long time; but only within the last few years has a systematic microscopical examination of ore samples become a normal tool of any research laboratory dealing with ore-dressing problems. Such an investigation avoids considerable loss of time as well as empirical trials and useless experimentation. It will generally indicate the correct grinding and often will suggest the proper method of treatment. The petrographic determination of transparent minerals in thin sections, or even in grains, has been perfected, and very accurate methods have been devised to meet any requirement, such as Feodorof's rotating stage on the petrographic microscope. Almost all transparent minerals can be positively identified by their optical properties; i.e., isotropism, anisotropism, color, pleochroism, refractory index, cleavage, crystal form, birefringence, and others. The identification of opaque minerals is a much more difficult problem and can be done only by using polished specimens. Unfortunately, most of the valuable metallic ores, and even some of the nonmetallic ones, are not transparent; therefore it has been necessary to develop a special technique for the determination of these minerals. Some optical properties-for instance, isotropism, anisotropism, color, cleavage, reflecting power-are often adequate in roughly classifying the mineral. Only "reflecting power" is a measurable value, provided special photometric equipment (ocular photometer or Orcel's photoelectric cell) is available. The other optical properties mentioned are more or less relative,

Jan 1, 1942

By George P. Demopoulos, Yan Zeng, Zhibao Li

Precipitated silica is marketed with a rising demand as reinforcing filler in the rubber industry and as a potential raw material for the synthesis of lithium-ion battery electrodes. Due to an awareness of the environmental impact of the existing processes for the production of precipitated silica, a green and sustainable process was proposed by using sodium bicarbonate (NaHCO3) as an alternative to sulfuric or hydrochloric acid in the precipitation reaction with sodium silicates. The use of NaHCO3 allows for better control of the supersaturation and pH to form silica with desired quality. Additionally, Na2CO3 solution as the process by-product is recyclable because it could be recovered to produce NaHCO3 by absorbing CO2. The solubility of sodium metasilicate nonahydrate (Na2SiO3·9H2O) in the Na-CO3-HCO3-OH-H2O system was measured using a dynamic method in the temperature range from 288.15 to 308.15 K. It is found that the solubility of Na2SiO3·9H2O decreases with increasing concentration of either Na2CO3 or NaOH over the investigated concentration range. With the aid of the OLI platform, a chemical model for the Na2SiO3-Na-CO3-HCO3-OH system was established with newly obtained interaction parameters of the Bromley-Zemaitis model by regression of experimental solubility data. The new model predicted the solubility of Na2SiO3·9H2O in multi-component systems with good agreement and was used to conduct a preliminary feasibility study of the new process.

Jan 1, 2015

By P. M. Soupios

The study of soft soil (wastes above the rock bed) an issue of great importance in civil engineering, is usually addressed by drilling boreholes. This method is rather expensive and time-consuming and although the information obtained is usually accurate, on the other hand it is much localized. Recently published researches have demonstrated the ability of the combination of geophysical exploration methods to estimate the thickness of deposited wastes, which provides the layered structure of the study area and certain, method depended, mechanical parameters as well. By theory, the frequency of resonance of an upper layer is a function of its thickness and the average shear velocity in it. Furthermore, the application of H/V spectral ratios of micro-tremors is a fast, straight forward and cost effective methodology, yielding the determination of the main resonant frequency of the soil. Based on this framework, 20 microtremor measurements have been carried out in a Landfill in Heraklion-Crete. Some of these measurements were deliberately close to drilled sites, where the basement had been reached. Three electrical resistivity tomographies were also used, in order to define the landfill structure such as, thickness, determination of different wastes distribution in the study area and other parameters. In addition, estimation of predictive Vs using empirical relationship between shear velocity and penetration resistance (SPT?s) were also conducted. Knowing the thickness and the resonant frequency, we estimated the shear (Vs) velocity of the waste cover. The final Vs model was confirmed using the results from the Vs-SPT correlation. The combinative implementation of the above mentioned geophysical and geotechnical methods have successfully defined geometrical and geotechnical/geophysical characteristics of the area under investigation in a fast and cost effective way.

Jan 1, 2005

By Joachim Ulrich

The spreading and splashing behaviour of single tin, lead, copper, aluminium and steel droplets impacting on a solid surface were experimentally examined. The droplet impact was observed using a high speed video imaging technique. The onset of splashing and the mass of the secondary droplets of impacting tin and lead droplets was quantified by the weight difference of the droplets before melting and the splat after the impact. The spread factor and the mass of the secondary droplets in dependence of the impact velocity is shown for different droplet materials, initial droplet diameters, target temperatures in ambient air and inert gas atmosphere. An empirical found correlation predicting the transition from spreading to splashing is presented by means of dimensionless numbers.

Jan 1, 1999

By B. C. Jena

Activities of carbon, cobalt and nickel were evaluated in the ternary systems iron-carbon-cobalt and iron-carbon-nickel for the temperature range 1300-1600°C for cobalt and 1300-1700°C for nickel. The carbon activities were determined from the knowledge of activities (1) in the binary system iron-carbon, (2) in the dilute ternary systems and (3) from the knowledge of carbon saturation data. The activities were mathematically expressed with the Taylor series expansion of Wagner's interaction parameter formalism modified to suit concentrated solutions. The cobalt and nickel activities were determined from the knowledge of carbon activities by applying the Gibbs-Schuhmann integration and from cobalt and nickel activities in the binary systems iron-cobalt and iron-nickel. Partial molar enthalpies of mixing were determined based on the temperature behaviour of the activity coefficients.

Jan 1, 1992

By Karl E. Burgher

Since World War II, the need for the use of explosives with testing, construction, demolition, mining and quarrying near urban areas has increased dramatically. Once remote, testing areas have been encroached upon by commercial and residential areas. Evidence has been found that overpressure levels near these areas can be estimated using meteorological conditions. This paper reviews a study where 205 test shots were fired, meteorological conditions recorded, and over-pressure levels estimated using multiple regression techniques.

Jan 1, 1988

By François Robert, Steve Green, Tyson Birkett, Dan Richardson

Abstract -Detailed sampling using a portable diamond drill, and interlaboratory comparison of selected samples have been combined with statistical studies of truncated populations to establish the gold content of several outcrops in the Val d'Or area. The outcrops chosen are non-mineralized. The background gold concentration in the rocks of the region is 5 ppb or Jess. Gold is distributed relatively homogeneously within the outcrops studied except for slightly increased concentrations within quartz-tourmaline veinlets. Three samples, of which 20 grams of powder are analyzed for each, can adequately determine the gold concentration of a structurally simple outcrop in the Val d'Or area.

Jan 1, 1992

By Tyson Birketi, Françoi Robert, Steve Green, Dan Richardson

Detailed sampling using a portable diamond drill, and inter laboratory comparison of selected samples have been combined with statistical studies of truncated populations to establish the gold content of several outcrops in the Val d'Or area. The outcrops chosen are non-mineralized. The background gold concentration in the rocks of the region is 5 ppb or less. Gold is distributed relatively homogeneously within the outcrops studied except for slightly increased concentrations within quartz-tourmaline veinlets. Three samples, of which 20 grams of powder are analyzed for each, can adequately determine the gold concentration of a structurally simple outcrop in the Val d'Or area.

Jan 1, 1992

By Anthony T. C. Goh

"For deep excavations in soft clay, it is common to use jet grouting piles (JGP) prior to excavation to minimize wall deflections and ground settlement, and to prevent basal heave instability. In this paper, finite element analyses were carried out to assess the basal heave factor of safety for excavations in soft clay supported by JGP. Comparison of the factor of safety from the finite element analyses with limit equilibrium methods was then performed. Subsequently, to account for the uncertainties in the soil and JGP properties, a simplified reliability analysis procedure is proposed to estimate the probability of basal heave failure for deep excavations supported by JGP.INTRODUCTIONJet grout piles (JGP) are often used to prevent basal heave instability and to minimize excessive wall and ground movements associated with deep excavations in soft clay deposits (Shirlaw 2003; Wen 2005; Ou 2006). The jet grouting process which is carried out prior to any excavation works produces a series of short overlapping grout columns resulting in a “continuous” base slab (commonly termed as jet grout pile or JGP) below the final excavation level that spans across the entire excavation (Gaba 1990; Hsieh et al. 2003; Ho and Hu 2006). Typically, the JGP thickness ranges from 2 m to 4 m.The focus of this paper is on the assessment of basal heave instability for deep excavations in clay stabilized with JGP. Finite element analyses were first conducted to determine the basal heave factor of safety for deep excavations in clay with JGP. Comparisons were then carried out with factors of safety based on conventional limit equilibrium methods. Since the conventional factor of safety approach does not explicitly reflect the uncertainties of the soil and JGP properties, it is demonstrated in this paper that a simple reliability based approach (Hasofer and Lind 1974) can be used to assess the probability of basal heave failure.LIMIT EQUILIBRIUM METHODFor excavations is clay, the Terzaghi (1943), Bjerrum and Eide (1956) and Eide et al. (1972) methods which are based on bearing capacity theory, are commonly used to determine the basal heave factor of safety. Another commonly adopted method in Japan and Taiwan is the slip circle method which involves taking moments about the lowest strut level (JSA 1988; Hsieh et al. 2008; Luo et al. 2012). The slip circle method has also been applied for excavations with a JGP at the base by incorporating the undrained shear strength of the JGP. In the slip circle method, the basal heave factor of safety FSslip is assessed by taking moments about the lowest strut level (Fig. 1)"

Jan 1, 1900

By Theophili CN, Kapenis AP

Seismic tomographic imaging has been applied to determine the blast induced damage zones in bauxite pillars in underground mining. At the retreating stage, when pillar dimensions are reduced from 8 x 8 m to approximately 5 x 5 m, the' seismic tomographies reveal, through measurements of the P-wave velocities which is a measure of the degree of fracturation of the pillar rock mass, the presence of three zones within each pillar. In the external zone, where velocities recorded are below 750 m/s. extensive pillar damage occurs which is attributed to both the growth and coalescence of pre-existing cracks and even the creation of new cracks in the rock mass. This effect is in agreement with literature, when considering the peak particle velocity as a criterion for rock failure in tunnels. In the intermediate zone, where velocities range between 7S0-1000 m/s, damage to a much lesser extent occurs which is due mostly to growth of pre-existing cracks and widening of their apertures. The inner zone, where velocities exceed 1000 m/s, is considered to be unaffected by blasting. Simple remedial measures of low cost, which are based on blasting mechanics are proposed to minimise the blast induced damage zone and consequently the transition zone.

Jan 1, 1995