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By Jan Yaozhong

The composition and the possible utilization of Ti bearing blast furnace from a titanomagnetite blast furnace smelter were studied. The slag contained about 20% Ti02 and trace Sc. The mineralogical analysis indicated that Ti in the slag is mainly as perovskite. By means of magnetite separation, the Ti containing phase could not be enriched. An effective hydrometallurgical approach was proposed with sulphuric acid leaching. The method proposed for processing the studied slag renders product Ti02 and SC203. Besides the recovery ofTiO2 and SC2O3' the leaching process yields fine grained residues which can used as additives for making cement.

Jan 1, 1996

By Z. Farhat

In spite of advances in cutting tool technology, the understanding of the basic wear behavior and failure mechanisms needs further study. Tool wear is the main factor contributing to geometrical error and thermal damage in machined components. Manifested as a reduction in tool life, it also affects the workpiece surface finish, increases cutting forces and induces residual stresses. Furthermore, the emergence of high and ultra-high speed machining processes necessitates the investigation of tool wear under these severe working conditions. Tungsten carbide-cobalt composite material has been used traditionally as wear resistant materials for many years. One main application of this material is in cutting tools. WC-Co tools consist of hard WC particles imbedded in a tough Co matrix, which functions as a binder phase. More recently, Cubic boron nitride (CBN) tool material have attracted special attention due to its high hardness and excellent wear resistance. Boron nitride in its cubic form is known to be the hardest material next only to diamond. In this paper microstructural and tribological properties of commercial grade WC-Co and CBN cutting tool materials are investigated under high speed cutting conditions. The CBN cutting tools were found to be superior to tungsten carbide (WC) tools. Four-fold increase in productivity and significant reduction in chipping and cratering was achieved for CBN as compared to WC. Wear mechanisms are proposed and are related to the observed wear characteristics in the cutting zone.

Jan 1, 2006

By F. F. Peng

Fine Coal Cleaning Processes including froth flotation, aggregative flotation or oil agglomeration, depend upon the wettability of coal particles in the aqueous solution. The wettability of coals of various ranks, hydrocarbon oil treated coals and oil-agglomerates have been measured using film flotation, induction timer, and froth flotation. Various hydrocarbon collector dispersion techniques are used to alter the surface wettability of coal particles. Change in wettability behaviors, measured by flotation responses, due to various ranks with or without of hydrocarbon collector modification are explained in terms of surface chemistry modifications as analyzed by induction time, film flotation as well as DRIFT Spectroscopy. The relationship between the wettability of coals and collector treated coals, and floatability are discussed.

Jan 1, 1993

By John B. Cocanour

The U.S. Bureau of Mines (USBM) has developed a laboratory-scale on-line analysis and process control system for a decopperization electrolytic circuit. This system is software driven, running on a 486DX-33 personal computer (PC) utilizing a portable energy- dispersive x-ray fluorescence (XRF) spectrometer as the sample analyzer. The XRF copper reading obtained was used as the control variable through an RS-232 serial interface to the PC for software-based control of feed flowrates. When the copper concentration in the electrolytic cell (as measured by the XRF) deviated from the set point, the feed flowrate to the cell was automatically altered using software-based proportional-integral-differential (PID) computer control to yield the desired copper concentration at the electrolytic cell outlet.

Jan 1, 1994

By Howarth W. J, Sowerby B. D, Watt J. S

On-line analysis systems have found widespread application in the metalliferous mineral and coal industries. The continuous analysis and rapid response of these systems has led to improved control of mining, processing and blending operations, with increased recovery of valuable minerals and coal combustibles.The paper reviews developments in on-line analysis by CSIRO and Mineral Control Instrumentation Ltd which led to the award of the Australia Prize 1992. These commercialised systems analyse mineral and coal slurries; determine the ash and moisture contents of coal on conveyors, and the moisture content of coke on conveyors; and determine the carbon content of fly ash. These gauges are estimated to have resulted in productivity increases valued at $50 million per year to Australia.

Jan 1, 1993

By David Hughes

The paper covers the utilization of on-line analysis in process control of solvent extraction in nickel leach solvent extraction processes in Finland and Australia and in copper heap-leach and solvent extraction in Chile. The goals of and requirements for controlling the solvent extraction stages of the processes are reviewed. The applications at three plants are compared. The development of the technology used is reviewed and design considerations are discussed. Requirements for on-line control and analyzer performance are compared. A new generation of analyzers and its effect on the set-up process of a project is introduced.

Jan 1, 2003

On-line radioisotope gauges determine information on the characteristics of ore to enable improved control of processing operations. In the metalliferous mineral industry, in-stream analysis systems based on radioisotope X-ray techniques determine concentrations of valuable minerals at various stages of the concentration process. In the coal industry, on-line gauges determine ash and moisture contents, and the specific energy of coal.In-stream analysis systems developed in Australia are installed in about 30 mineral concentrators. Their use has led to the increased recovery of valuable minerals, and the time taken to recover the cost of installation is usually several months. The savings to Australia resulting from use of these analysis systems is estimated to be more than $A 15 million per year.Australian experience in the training of mineral industry personnel shows that the most effective approach is to combine courses on nuclear techniques and control of processing operations. This is the basis of Australia's contribution to the minerals sub-project of the United Nations Development Program (UNDP) Industrial Project.

Jan 1, 1985

By S. M. I Kytö, J .. K. Mäkinen, K. Saarhelo

"At the Outokumpu Oy Harjavalta Copper Smelter the control philosophy of the flash smelting process has been changed from the slow feed-back control to feed-forward control. This is important as the fluctuations in the flash smelting furnace matte grade and slag temperature are desired to be minimized.The system is based on a specially designed automatic sampling device and the Outokumpu Courier 20 on-stream X-ray fluorescence analyzer. A microcomputer-based Analyzer Operator Station (AOP) controls the system and calculates the process parameters for the furnace from the analyzed chemical composition and other existing data.A considerable reduction in the deviation of the matte grade and slag temperature has been gained. This has resulted in conservation of energy and refractories, lower copper losses and higher through-put in the flash smelting furnace and converters.1.0 IntroductionThe flash smelting technology for copper concentrates was developed at the Outokumpu Oy Harjavalta Smelter soon after the World War II. The incentive for this development was shortness and high price of any form of energy. The fact that smelting can be carried out autogenously, without external energy by utilizing the latent heat of sulfide combustion was known decades before, but Outokumpu Oy was the first company to take the advantage of this knowledge in practical operation. A further advantage of this technology was that the SO2 containing gases suited well for sulfuric acid production, thus minimizing the detrimental effects on the environment (1).The very heart of the flash smelting process is the reaction shaft of the flash smelting furnace (see Appendix I). Heating up of the dried feed mixture, dissociation of several compounds, ignition and oxidation of the feed take place very intensively in the reaction shaft during 2 - 3 seconds, which the fine grained particles reside in the reaction shaft. A very accurate control of the amounts of the feed materials as well as of oxidizing gases, fuel, etc. is of primary importance."

Jan 1, 1989

A system for rapid on-line determination of weight percentage coal in slurry and weight percentage ash in coal has been developed at the Julius Kruttschnitt Mineral Research Centre, University of Queensland. The gauging system is suitable for use with coal flotation slurries or slurries having a maximum particle size of about 1 millimeter. The system is based upon measurement of gamma ray transmission; radioisotope sources emitting photons of two widely different energies are employed. The inaccuracies of measurement that would normally result from variable amounts of air entrained in the slurry are substantially reduced by pressurising the slurry to approximately 2MPa (300 psi) using a Mono pump. The equipment can be used to make measurements on more than one slurry stream by pumping streams sequent- ially. The system is being tested at the Peak Downs Mine of the Utah Development Company in Central Queensland. This paper describes the theoretical principles of the gauge design, the experience gained to date in the commissioning of the equipment, including the installation of a PDP 11/03 computer, and the progress made in developing satisfactory interpretations of the gauge count-rate output.

Jan 1, 1978

By C. L. Lin

A PC image-based on-line coarse particle size analyzer has been developed to measure particle size distributions under plant situations where overlapped particles are being transported on a moving belt conveyor. Although previous testing had shown satisfactory performance of this image-based system for separated particle size measurements (the non-overlapped case), it was necessary to modify original algorithms in order to solve the overlap problem and make the system suitable for plant operations. On-site testing has been conducted at a large copper concentrator in the southwestern U.S. for further investigation of the overlap problem.

Jan 1, 1995

By Cutmore NG

The moisture content of iron ore is important in handling, stockpiling, transport and further processing operations. Typically these ores contain both `free' and `bound' moisture, the latter being moisture that is not removed in a conventional laboratory determination of moisture by air drying at 105¦C, and it is the free moisture that is important in dust control and ore handling. The CSIRO Division of Mineral and Process Engineering has previously developed and commercialised gauges, based on capacitance and microwave techniques, for the on-belt determination of moisture in coal and minerals. However, these gauges determine total moisture, and have a different sensitivity to free and bound moisture in the material analysed. Consequently, the accuracy of determining total or free moisture alone may be significantly affected by variations in the bound moisture content. An investigation has been carried out on the simultaneous determination of free and bound moisture in iron ore fines (

Jan 1, 1993

By Sowerby BD

The CSIRU Division of Mineral Engineering is developing various techniques for the on-line determination of moisture in coal and coke, and some instruments are now commercially available. These techniques permit accurate and rapid determination of moisture in materials directly on conveyor belts or in bins. The most promising techniques for direct on-belt measurement of moisture in coal are capacitance and microwave transmission. A non-contacting under-belt capacitance and gamma-ray backscatter technique has determined moisture in coal to better than 0.5 wt'/. in field tests at BHP Stockton Borehole Colliery, NSW. Mineral Control Instrumentation Pty Ltd have been licensed to manufacture the capacitance gauges and have installed five commercial units in the coal industry and other industries. Microwave transmission techniques have an advantage over the under-belt capacitance technique in that they are not sensitive to vertical segregation of moisture in coal on the conveyor belt. A laboratory prototype of a microwave transmission gauge has been constructed and tested. Microwave techniques, based on a measurement of attenuation and phase shift, are under development and are expected to be field tested in 1987. These new techniques will enable a wide range of thickness changes to be accommodated. Capacitance and microwave transmission methods are unsuitable for materials of high electrical conductivity, such as coke. CSIRO is therefore developing a fast neutron and gamma-ray transmission technique, which is proving very accurate in laboratory tests. This technique overcomes many of the limitations of thermal neutron moisture gauges and it is expected to be field tested in 1987.

Jan 1, 1987

By M. G. Irish, E. E. Vidal, M. J. Jahraus, P. R. Taylor

An experimental system has been designed to monitor on-line variations of leaching parameters in a closed circuit of cyanide leaching solutions and gold bearing ores. Experiments performed to deter-mine variations in some important leaching parameters of the solution: pH, dissolved oxygen, free cyanide, oxidation/reduction potential, gold content, temperature, pressure and solution chemistry. By comparing results obtained when the leaching solution is allowed to become acid or kept basic, it was possible to infer the chemical reactions that occurred between the solution and the ores.

Jan 1, 2004

By K. Zenger, J. Kaartinen, J. Huuskonen, S. Torttila, S. Lähteenmäki, J. Pietilä

"Pyhäsalmi Mine in Finland has a long history of continuous process development. The concentrator processes Cu-Zn-sulphide ore with high recoveries. An on-line flotation simulator has been developed to maintain and further improve the flotation performance. Consisting of a flotation kinetic dynamic model, and interconnected with process control software, the simulator can be used for training new control room operators in various scenarios. For daily operation, the model parameters are continuously adapted to take into account the changing process conditions. On-line simulator tracking the process can provide the process operator new information in several ways: a) values of unmeasured process variables are obtained by displaying the corresponding simulator values, b) predictions of future process states and outputs are calculated and displayed, c) information of changing process parameters can be used as an indicator of e.g. change in the processed ore type. This paper describes the adaptive simulation system and its usage at the Pyhäsalmi concentrator.IntroductionPyhäsalmi massive sulphide orebody is located in central Finland. Operation of the mine started in 1962 and it is currently producing copper (Cu), zinc (Zn) and sulphur (S) concentrates. The concentrator control and optimization system has a long history of successful continuous development during the past decades (see e.g. Huuskonen & Moilanen, 2010). An on-stream analyzer has been a part of the automatic process control since 1968 (Lähteenmäki, Miettunen & Saloheimo, 1999). First control algorithms based on a flotation mathematical model were developed in 1971 (Koivistoinen & Miettunen, 1985). In 1990’s the development of a froth machine vision systems started (Kaartinen, 2009; Kaartinen, Roine & Hätönen, 2009). More recently Pyhäsalmi Mine Oy has been involved with several national development projects dealing with particle size distribution measurements (Kaartinen & Tolonen, 2008), spectral analysis of flotation slurries (Haavisto, Kaartinen & Hyötyniemi, 2008), and dynamic simulation of flotation processes. The latter topic is further elaborated in this paper."

Jan 1, 2015

By S. Banisi, J. A. Finch, A. R. Laplante

"A technique for on-line simultaneous estimation of gas and solids holdup (volume fraction), based on a combination of conductivity and pressure difference measurements, is proposed and tested in a laboratory flotation column (10cm in diameter and 447cm in height). Fundamental concepts underlying this technique and the effect of relevant parameters are discussed. In the studied range, 3-30 %v/v gas holdup and 2-18 % v/v solids holdup, experimental results showed good agreement between the estimated and actual holdup values (as determined by an isolating technique). The relative accuracy of the solids holdup estimation increased when solids density or solids concentration increased. Frequent re-calibration of pressure transducers was found necessary for accurate phase holdup estimation.IntroductionGas holdup is a key parameter in controlling the performance of flotation columns. For example, flotation rate is affected by bubble size and gas rate both of which, in turn, affect gas holdup. Moreover, gas holdup also determines the slurry residence time which indicates a direct influence of gas holdup on recovery.Gas holdup determination has been the focus of many studies (e.g., Castillejos, 1986; Marchese et al., 1992). Some of the techniques which have been used are given in Table 1."

Jan 1, 1994

By Sami Makni, Ahmed Bouajila

"To remain competitive in an open market, mining companies are more and more requested to optimise their complex and highly multivariate processes. The increasing amount of process data, brought about by intensive use of instrumentation and the progress in computer data acquisition, enhances the need for more and more powerful and robust tools for the analysis and modelling of the process data. Now, with the emergence of multivariate data analysis (MDA) techniques, on-line clustering of mineral process behaviour is possible and could help in the extraction of valuable process operation indicators. MDA can be used in different mineral processes such as flotation, grinding, smelting etc. In this paper, the focus will be on grinding process as it is the one of the most costly node in the mineral processing scheme (i.e. power consuming) and it is a highly multivariable process. Particularly for primary grinding mills (SAG/AG), more instrumentation outputs and more powerful and significant process indicators are needed for efficient control and optimisation.MDA is a novel approach suitable for understanding mineral process behaviour compared to the traditionally approaches based on empirical and phenomenological modelling. Multivariate techniques can be used for several purposes. In this paper, the following objectives will be addressed:operation diagnosis: Shift differentiation and operation test differentiation can be showed by using MDA tools such as principle component analysis and factorial discriminant analysis.operation performance monitoring: operation regimes can be evaluated by clustering based on an economic criterion performance such as costs, tonnage, product quality, profit, etcIdentification of operation behaviour (monitoring) and selection of drift correction trajectories (control):MDA can be used to identify periods of unusual or abnormal process behaviour and to diagnose, if it is possible, causes for such behavior."

Jan 1, 2003

By Michael Taylor, Thomas W. BoBo

Currently two of the most important characteristics of construction aggregates are (a) the particle size distribution (psd) and (b) the “shape” of the aggregate particles. The long established test methods and standards for these properties require substantial resources and most suppliers can take samples and conduct tests at intervals measured in days (psd) or even months (shape). Furthermore these tests require time: so the results are available only after material has been stockpiled or shipped. In the rare cases where problems are found the out-of-spec material has often been shipped to points unknown. There are substantial advantages to be obtained if the psd and other geometrical properties could be obtained from the material as it moves through the production processes and if the results could be reported back within seconds or minutes to Plant Control Managers. This paper describes a single on-line system used to evaluate production of crushed material in a production quarry. The system consists of an enclosure (containing the camera and lighting etc.) mounted over a production belt. Images are fed by fiber optic cable to a nearby control room where the data are analyzed; stored; displayed; and made available for integration into a process control system. Numerous forms of display can be created according to the needs of the producer. Once programmed by an automation engineer all functions of operation are fully automated. The system has permitted over 400 tests per hour with a feed back time less than 2 seconds. Sufficient geometrical measurements are made so that many different “shape” factors can be computed on a similar time scale. The paper summarizes the results from approximately 100 shifts of about 8 hours each and compares the imaging method with the current standard hand methods. Study of the data generated showed that, when combined with additional plant information, the system can be used to generate additional useful control information.

Jan 1, 2005

By Dany Pelletier, Yeves Breau, Ahmed Bouajila, Claude Gagnon

"In flotation circuits, direct measurement of the volumetric flow rate delivered by electromagnetic flowmeters is often difficult to obtain particularly due to piping and flow constraints. However, on-line material balance calculation could offer a reliable alternative to flow rate sensing. This paper describes an on-line material balance software package as applied to a copper flotation circuit for mass flow rate estimation mainly based on the output of an x-ray fluorescence onstream analyser. Rule-based procedures for the management of the main calculation modules are designed and integrated to a Comdale expert system. Attempts to diagnose the flotation process from mass flow rate data are also discussed.INTRODUCTIONThe need for improved process diagnosis, control and optimisation has become more evident for the mineral processing industry in the last decade. Therefore, new process variables need to be inferred or measured particularly in highly multivariable processes such as flotation. This process is subject to a wide variety of disturbances mainly generated by frequent and sometimes abrupt changes in physical and chemical characteristics of the ore and due to some irregularities in manual process operating procedures.A flotation circuit scheme is always a complex network counting more than two dozens of slurry streams. Information about those streams (%solids, metal content analysis, and flow rates) are important for process diagnosis, performance evaluation control and optimization (1,3).On-line sensing instruments such as x-ray fluorescence (XRF) on-stream analysers (OSA), gamma density gauges and electromagnetic flowmeters have been developed for the measurement of those variables. Unlike the other variables, stream flow rates could be determined by different ways:"

Jan 1, 2000

By P N. Holtham

Magnetic separation is routinely used in the processing of titaniumminerals, and the efficiency of these operations can be determined bymeasuring the magnetic properties of the process streams. The valuable components in the feed to a titanium minerals plant have specific magnetic susceptibilities ranging from -10-9 m3 kg-1 (zircon) to 10-6 m3 kg-1 (ilmenite). However, in an industrial environment, in which the mineral temperature may range from 20 to 120¦C, it is difficult to measure susceptibilities lower than about 10-7 m3 kg-1. Hence laboratory testing of spot samples from magnetic separators is currently required to obtain accurate performance data. This is an inherently slow process and where feed grades are variable, optimum performance of magnetic separators is generally not achieved.This paper describes the development of an inductance-basedinstrument for measuring very low levels of magnetic susceptibilityon-line. The signal from the instrument can be used for process control purposes to maintain optimum magnetic separator performance.A prototype instrument has been installed in the zircon scavengercircuit in an Australian titanium minerals plant. The circuit consists of a roll magnetic separator treating a feed consisting mainly of monazite and stained zircon. The monazite-rich magnetic fraction is returned to the mine site for disposal, while the non-magnetic fraction is recycled to the zircon wet circuit. Splitter positions in the separator are adjusted when the final zircon product fails to meet specification, or the magnetic fraction contains more than 30 per cent zircon. Weekly composite grain counts show that sub-optimal operation of the magnetic separator results in significant zircon losses into the magnetics fraction.Using the instrument, the zircon content of this stream can now beaccurately determined from the measured magnetic susceptibility,provided a correction for the effect of mineral temperature is applied using the Curie - Weiss relationship.

Jan 1, 2001

By Derek J. Fray

"A need exists for fast and accurate analysis of species in various phases at elevated temperatures. Although modern analytical techniques are very efficient, the equipment is usually situated some distance from the industrial operation and time is spent taking the sample and sending it to the analytical facility. Several minutes can easily lapse and, during this time, heat must be supplied in order to keep the system molten and, if the composition is changing rapidly due to a refining process or reaction with the environment, the information may only be of retrospective use. Perhaps more important reasons for the use of on-line sensors are that instantaneous analysis gives better control, process optimisation and the minimisation of energy losses and pollution. To date oxygen has been the only element which is measured widely using solid electrolytes. However, the analysis of many more elements is required and possible electrolytes for other species are discussed. For some elements, ~here is no suitable conducting electrolyte and, therefore, a different approach is adopted where the electrolyte, in which one species is mobile, comes to equilibrium with another species. IntroductionThere is an ever increasing demand for the development of sensors for on-line measurements in most areas of technology and, in particular, metal processing. This is especially relevant in situations where greater control can be achieved by monitoring the chemical composition of the melt during processing and where a minor constituent in the melt can have a major effect on the properties of the finished alloy. Although modern analytical techniques are fast and reliable, the equipment due to its complexity, is frequently situated away from the process area and valuable time may be spent in sampling and transportation. During this period, heat may have to be supplied to prevent solidification and the refining reactions may be continuing, and, therefore, the analytical information may not be of direct use."

Jan 1, 1988