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By Michael S. Wieland

The work-principle from thermodynamics was used to formulate a model for predicting toxic fumes from mining explosives in underground chamber tests, where rapid turbulent combustion within the surrounding air noticeably changes the resulting concentrations. Two model constants were required to help characterize the reaction zone undergoing rapid chemical transformations in conjunction with heat transfer and work output: a stoichiometry mixing fraction and a reaction-quenching temperature. Rudimentary theory with an unsteady uniform concentration gradient was taken to characterize the combustion zone, yielding 75% for the mixing fraction. Four quenching temperature trends were resolved and compared to test results of ammonium nitrate compositions with different fuel-oil percentages (ANFO). The quenching temperature 2345 K was the optimum choice for fitting the two major components of fume toxicity: carbon monoxide (CO) and total nitrogen oxides (NOx). The resulting two-constant model was used to generate comparisons for test results of ANFO compositions with additives. Though respectable fits were usually found, charge formulations which reacted weakly could not be resolved numerically. The work-principle model yields toxic concentrations for a range of charge formulations, making it a useful tool for investigating the potential hazard of released fumes and reducing the risk of unwanted incidents. Keywords: Toxicity; Fumes; Explosives

By C. E. Jordan

Domestic cobalt resources are relatively large, but low grade. The full potential for cobalt production from domestic sources is at least 19.4 million lb of cobalt per year exclusive of offshore resources. A summary of the cobalt processing technologies for the major domestic resources is presented in this Bureau of Mines report. The processing technologies for the Blackbird, Madison Nine, Duluth Gabbro, iron ore pyrite, laterites, and manganese sea nodules are nearly complete, but the economics are not favorable. Research on these resources should be limited to approaches that promise to cut the total processing costs by at least 50 pct. The most promising sources of cobalt are the spent copper leach solutions and siegenite from the Missouri lead ores. Research on cobalt processing from these two sources needs to be completed.

Jan 1, 1988

By William D. Mayercheck, August J. Kwitowski, John R. Bartels

This report discusses the Bureau of Mines' efforts to develop partial protective structures for operators of low-coal shuttle cars. In coal seams 48 in high or less, full-coverage canopies are generally difficult or may be impossible to implement on high-speed face equipment due to the restrictions they impose on the operator's vision and comfort. Lim- ited coverage is one alternative that provides an acceptable level of operator protection in thin-seam applications where conventional full- coverage canopies cannot be used. Three possible limited-coverage de- sign scenarios (roll bars, sliding canopies, and flip-top canopies) were designed, fabricated, and evaluated for low-coal shuttle cars. All three designs were determined to be feasible and desirable for low-coal shuttle car application.

Jan 1, 1987

By H. H. Schrenk, L. B. Berger

"INTRODUCTION The Bureau of Mines frequently receives requests for information and advice regarding the equipment necessary for establishing laboratories for the analysis of mine atmospheres. Such requests are made by mining companies, State mining departments, and other agencies concerned with the safety of mining operations. In many instances it is desired to install a complete laboratory, which will necessitate purchase of suitable gas-analysis apparatus and all the minor but important accessory equipment needed to carry on this type of work. Although publications that describe methods and techniques applicable to the analysis of mine atmospheres are available, it is not within the scope of such publications to give detailed information on laboratory equipment or design. Persons unfamiliar with laboratory practices and gas-analysis procedures may find it difficult to decide upon the proper equipment for their particular needs and to itemize the various accessories that must be obtained to set up a complete laboratory.The purpose of this circular is to discuss the different types of equipment that may be used in the analysis of mine atmospheres, with particular regard to the application and limitations of each type. Information on the various accessory equipment needed in a laboratory for the analysis of mine atmospheres is given also, and suggestions on laboratory design are included. As much of the necessary equipment may be obtained from laboratory supply houses, the information should aid in arriving at estimates of the cost of proposed laboratories.The procedures involved in the analysis of mine atmospheres are not described; such information is contained in publications referred to in this circular."

Feb 1, 1948

Provide the mining industry with a method for determining the gas content of ore bodies and associated strata for use in mine planning, Approach Samples of various rock types are collected and tested to determine gas content in conjunction with sample size, the collection method (i.e. whether the sample was collected from a core sample or by hand) mine gas emission, and the geologic location from which the sample was taken, such as near a fault, outburst area, or other geologic anomaly. How It Works Two methods were developed by the Bureau of Mines to determine the gas contents of rock samples. The first method developed involved dissolving minerals to measure gas emission. This method, however, can only be used with soluble minerals. A second method, therefore, was developed for use with insoluble minerals. With this method, the sample is crushed in a ball mill. Although the dissolution method is faster and more accurate to use, the crushing method is also advantageous because its use can more closely approximate a mining situation; the sample is crushed as in mining and the amount of gas released relates to the amount of gas that would be released during a mining operation. The dissolution method is applied to soluble minerals, such as rock, salt, or trona, in a sealed chamber. Gases released during dissolution are collected for analysis by gas chromatography. One advantage in using the dissolution method is that the test apparatus is relatively inexpensive. In addition, test can be performed at any scale, from single crystal samples to a solution mining operation.

Jan 1, 1983

Enhance the critical skill of hazard recognition among miners by providing quality training that can help jot performance and lead to a higher degree of safety in the workplace. Background In mining, as in many other occupations, the safety of the worker depends on his or her ability to recognize hazards in the workplace. Some of the information needed by the miner for recognizing potential areas of danger is available in the form of visual cues found throughout the mine. One aspect of the dynamic mine environment it which the task of hazard recognition is critical for al workers is that of ground control. Regardless of job responsibilities, every worker is continuously exposed to roof rib, and floor hazards. Fatality injury data for the "underground coal" segment of the mining industry continue to show that about half of all fatalities are due to falls of ground each year. It is hypothesized that some of these accident, can be prevented if miners are better able to recognize visual cues that forewarn of potential roof and rib problems.

Jan 1, 1992

By John J. Sammarco

As part of a project to automate coal extraction, computer control of a continuous mining machine test bed has been developed and tested by the Bureau of Mines. A computer system and control software were developed for accurate positioning of the conveyor elevation and swing, stabilizer jack, gathering head, and shear elevation. Tramming actions are also controlled by the computer. The computer system was designed to access data from sensors installed on a continuous miner and to interface with the existing control circuits of the miner. Testing in free space was used to characterize the operation of the machine. From this information, control algorithms were written and stored in the computer. The ability to control each function of the continuous miner with a high degree of accuracy and stability was successfully demonstrated in a series of tests in free space and in mining a block of simulated coal. In the mining of simulated coal, the cutting drum was instructed to position the shearer at the top of the block and shear down to the bottom under closed loop control. The cutting drum came within 0.27 in of the top and within 0.49 in of the bottom of the block for this shearing test.

Jan 1, 1988

By W. R. Reed

A computer model named the "Dynamic Component Program" (DCP) was specifically designed for predicting the dispersion off dust from haul trucks at surface mines. Validation of the DCP was completed by comparing its results with the results of the 1SC3 model and with actual dust measurements taken front two operating mine sires. Comparisons of the field measurements, predictions of the ISC3 model and the predictions of the DCP demonstrate that the results from the DCP represent, on average, an 85% improvement truer the ISC3 dust dispersion model results.

Jan 1, 2008

To more rapidly and economically prepare solutions for chemical analysis, of a wide range of ores, slags, minerals, and metals. Approach A Simple pressure-dissolution system was devised using an inexpensive, heavy wall plastic bottle containing a sample in an acid medium. Using the technique, a complex silicate sample can be dissolved in less than 1 hour. How It Works A weighed portion of a sample, ground to minus 100-mesh, is placed into a polycarbonate or polysulfone plastic bottle. A mixture of hydrochloric acid, nitric acid, and hydrofluoric acid then is added. The bottle threads are wrapped with a layer of Teflon tape to prevent leakage, and the bottle cap is screwed on tightly. The sealed bottle is placed in a balling water bath. In the hot water, the plastic bottle acts as a pressure vessel to contain the pressure generated inside it. This technique should only be used by trained experienced people who are familiar with the hazards of hot acids under pressure. After being cooled in cold water, the resulting solution is brought to the final volume by adding 1.5 weight-percent boric acid solution to the bottle. The cap is replaced, and the bottle and solution is reheated. Precipitated fluorides, as well as any residue, are dissolved by the fluoride-boric acid reaction. The resulting clear solution then is suitable for spectro-photometric examination or other analysis.

Jan 1, 1980

By J. D. Dixon

The Bureau of Mines has developed structural design data for unreinforced concrete tunnel linings in the form of stress and deflection coefficients from which bending, axial, shear, and boundary stresses, moments, thrusts, and shear forces, and structural deflections can be determined at any point on the lining. Results were obtained by structural analyses of nine concrete-lined tunnel configurations subjected to 22 biaxial load conditions. The tunnel configurations include three basic shapes, circular, rectangular, and horse-shoe, with dimensions based on designs evolved by the mining industry. These analyses were made by the direct stiffness matrix method, a computer-oriented procedure. Numerical results agree closely with those obtained experimentally.

Jan 1, 1969

To restore ventilation and prevent the accumulation of explosive or toxic gases by quickly installing substitutes for stoppings blown down by an explosion. Approach Temporarily replace blown down stoppings with a parachute-shaped brattice which can be erected in minutes. How It Works The self-sealing brattice is secured to the roof, ribs and floor by anchoring its nylon edge strip at several points using extensible poles, shads, or available projections such as roof bolts. The air pressure in the entry pops open the chute of lightweight sailcloth, forcing it tightly against floor, roof and rib. See Figure 1. This emergency brattice has been tested at two locations in the Bureau's Experimental Mine at Bruceton, Pennsylvania. In a test last December, one MESA inspector wearing full rescue apparel (including self contained breathing apparatus) installed a self sealing brattice in an entry at the Bruceton Mine. Although he did not have any previous experience with the device, he easily erected it in slightly less than 10 minutes, using two extensible supports (pogo sticks). Research to improve and refine the self-sealing brattice is continuing.

Jan 1, 1977

Provide a means of evaluating the in place structural properties of coal seams and coal measure rocks in advance of mining. Approach Develop a sonic logging probe for use in dry wells, a condition common to shallow wells and semi-arid coal regions. How It Works The Bureaus' sonic probe differs from conventional sonic probes because it does not require fluid in the well to couple sonic vibrations to the drill hole wall. A self-contained hydraulic system forces pistons containing the measurement transducers against the wall and clamps them in position until the sonic waveform information has been recorded. The pistons are then retracted and the probe is raised or lowered in the well as required. In the clamped position, the piezoceramic transmitter emits a sonic pulse which travels along the drill hole wall and is detected at the receivers in the form of compressional (P) and shear (S) wave motion. The receivers are designed to be sensitive to either the (P) wave or (S) wave motion as determined by the operator so that discrimination between the two wave types is improved by comparison of the respective output channels, and the travel time between transmitter and detectors can be accurately determined. Use of two receiver stations eliminates errors in timing of pulse travel because of electronic delays inherent in the probe.

Jan 1, 1981

By W. O. Philbrook

Reduced-scale models have long been used in hydrodynamics, aerodynamics, and heat transfer for studying fundamental flow relations or the performance of prototype designs under prescribed conditions. The pilot plant is a common tool of chemical engineering for investigating process variables and as an integral step in developing a new process. The metallurgical industry was rather slow to recognize the applicability of these techniques to some of its established and rather complex processes, but there has been a rapidly increasing number of applications of the principles of modeling in process metallurgy since World War II. Not only have pilot-scale operations been employed for developing methods of extracting metals that have recently achieved commercial importance, as well as new processes for some of the commoner metals, but models have also been used for engineering studies aimed at better understanding of the controlling, variables of time-honored conventional processes, It appears that the principles of similitude have become accepted as a useful tool, when properly applied, in metallurgy as in other fields of engineering. Much of the work of the Pyrometallurgical Laboratory, Region V, involves study of high-temperature smelting and refining processes for ferrous and related metals in pilot-scale equipment, such as the experimental blast furnace, converter, open-hearth, arc furnace, and rotary kiln. It was appropriate for the work of this laboratory that guiding principles for designing apparatus and interpreting results should be set down and that a bibliography of related work should be available for reference. A summary of the principles of model study and a brief review of some of the more noteworthy general papers have been published elsewhere.3/ Also, the Bureau of mines plans to publish a report of investigations describing its experimental work in this field. The bibliography is presented here as a service to others who may have use for it.

Jan 1, 1958

Improve the safety and reduce the cost of longwall entry support. Approach Replace the conventional wood cribbing with stronger, non-rotting and lower cost cribbing made of steel-fiber-reinforced (SFR) concrete. How It Works Conventional concrete can suddenly fail under excessive compression loads, but adding steel fibers to the concrete, before it is mixed with water, changes the failure mode to a gradual and controlled failure characteristic similar to wood. A system for making SFR concrete crib blocks was designed and developed (or use in constructing walls and cribs to support coal mine roofs. The SFR concrete cribbing is stronger and stiffer than wood, and avoids wood's disadvantages of: flammability, deterioration under chemical or bacteriological attack, methane generation, and relatively high cost. Use of SFR concrete also allows freer movement of miners, equipment, and ventilation air, because much less volume of SFR concrete is required than wood for a given amount of support, and because the roof-to-floor closure is greatly reduced by the stiffer supports.

Jan 1, 1981

By John T. Aydelotte, Martin J. Gavin

" Oil shale contains little or no oil as such , but it contains an organic material from which oil may be produced by destructive distillation" . This statement , or others conveying the same meaning, appears in many popular and techni cal articles on oil shale . It is based on the belief that the ordinary solvents of petroleum have but little action on the organic substances contained in oil- yielding shales , although on distillation these same shales may yield upwards of 50 gallons of crude shale oil per ton . A 50 - gallon shale thus yields by distillation 18.73 per cent of its weight as oil ( assuming the specific gravity of the oil to be 0.900 ) , although only a relatively small part of this can be recovered by extraction with such solvents as chloroform , carbon tetrachloride , and the like . In the course of certain experiments designed to determine the solubilities of different shales after they had begun to yield oil by distillation , it was found desirable to determine the quantity dissolved from certain unheated shales by various solvents , at or near the boiling points of these solvents . The method used and results obtained are presented below. These experiments were made in connection with the oil - shale investigations being conducted by the U. S. Bureau of Mines , in cooperation with the States of Colorado and Utah .

Jan 1, 1922

By Frederick C. Trutt, Jeffery L. Kohler, Joseph Sottile

Condition-based maintenance (CBM) of industrial equipment is generally recognized as being the most cost-effective means for improving equipment availability. However, prerequisite to successful implementation of CBM is a reliable detector of failing components. One such detector, termed the effective negative-sequence impedance, had previously been identified as an indicator of induction motor stator winding degradation. However, a limitation of this detector is that it does not change in a predicable manner under certain motor operating conditions. This paper presents an experimental investigation of an improved technique for on-line detection of induction motor stator winding degradation. The paper begins with a brief description of the detectors, followed by a detailed description of the experimental setup, the experiments conducted, and results.

By G. L. Oldright, John D. Sullivan

"The present article is the second of a series of papers dealing with the dissolution of copper minerals in various reagents. Work done on the problem has been carried out at the Southwest Experiment Station of the United States Bureau of Mines, in cooperation with the Department of Mining and Metallurgy, University of Arizona. The first paper4 dealt with the dissolution of azurite, malachite, chrysocolla, and tenorite. Preceding articles5 have also dealt with other factors involved in the leaching of copper ores.Cuprite (Cu20) is usually considered as a mineral which is not adaptable to sulphuric acid leaching. Hofman,6 in describing leaching by sulphuric acid, states: ""Cuprite is decomposed into CuO and Cu; and ore carrying cuprite has to be oxidized (weathering, roasting) before treatment."" Greenawalt7 says: ""When acted upon by dilute sulphuric acid, it is partly reduced to metallic copper and partly oxidized into copper sulphate. When heated with strong acid it is entirely oxidized to sulphate."" Work to be described in this article was undertaken to ascertain the conditions whereby all the copper in cuprite could be converted into the soluble sulphate."

Dec 1, 1929

Provide roof to floor closure rate measurements during underground mining, especially retreat mining of coal pillars, thereby helping the miners predict an imminent roof fall. Approach An electronic device and rugged potentiometric extensometer were developed to provide a means fur measuring total closure and the rate of closure. How It Works An intrinsically safe, battery operated instrument is enclosed in a rugged, hand carried field case. The unit is constructed using low-power, integrated circuits to provide minimal battery drain. Two digital Light Emitting Diode (LED) readouts are used; one displays the rate, the other displays the total closure. The unit will measure one extensometer continuously or two extensometers alternately. Two potentiometric extensometers with a closure measurement range of 6 inches are attached to the readout unit. As the roof to floor closure changes, the potentiometric resistance

Jan 1, 1982

Provide a simple and effective means of measuring mining-induced pressure changes in coal mine roof and pillars. Approach Develop a reliable, easy to fabricate and install borehole instrument which measures mining-induced pressure changes in pillars and in the mine roof. Ground pressures are monitored through use of aluminum platens coupled with d copper flat jack. How It Works The Bureau's instrument measures mining-induced pressure changes by transmitting strata pressure through the aluminum platens to an oil-filled borehole platened flat jack (BPF). Pressure in the flat jack is displayed on a gage located outside of the borehole. The instrument is in-stalled in the borehole by inflating the flat jack using a hand-held hydraulic pump. In addition, the platens have been designed to allow up to three BPFs to be installed in a single borehole, thus permitting pressure change measurements in more than one direction from a single borehole. Installation pressure is calculated on the basis of the estimated pressure exerted by the overburden and the percent of recovery after intial mining has

Jan 1, 1986

By L. B. Berger

Studies showing the effect of mixing hot exhaust gases with tie intake air of a four-stroke-cycle Diesel engine are described. The results indicate a marked increase in carbon monoxide in tip exhaust gases, a decrease in oxides of nitrogen, and no significant effect on aldehydes. The increase in carbon monoxide was greater at higher fuel-air ratios and was caused partly by the increase in fuel-air ratio end partly by the decrease in oxygen concentration resulting when exhaust has was added. The application of these results to the use of Diesel engines underground is considered.

Jan 1, 1940