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By E. B. Kester

In the commercial evaluation of coal tars, a distillation analysis properly carried out is of considerable importance. Close attention must be given to this operation in order to obtain consistent results and to secure the minimum decomposition of the tar compounds, which in many cases are sensitive to undue heat effects. Low-temperature tars in particular contain compounds of this nature, while in the case of tars produced at high temperatures the large proportion of pitch present has an adverse influence during a distillation. If excessive cracking takes place, the composition of the distillate will naturally vary from the normal, with the result that all the analytical criteria subsequently obtained are affected. Where tars, produced over vide ranges of carbonization temperatures are investigated as in the survey of gas, coke, and by-product making properties of American coals nor being conducted at the United States Bureau of Mines Pittsburgh Experiment Station, the method of distillation must necessarily be the sane for all of the tars studied. Also, it must function equally well for both low and high temperature tar, permit accurate fractionation, and reduce adventitious decomposition to a minimum.

Jan 1, 1932

By John P. Borovsky

A 3-year study was conducted to evaluate the problems and benefits of using vegetation to stabilize tailing from a potential Minnesota copper-nickel milling operation. The project consisted of three separate investigations: a waste characterization study, a greenhouse study and a field study. With few exceptions, the physical and chemical characteristics of the tai ling were found to lie within the range of properties of Minnesota soils. The tailing lacks organic matter; is deficient in nitrogen, phosphorus and potassium; and may contain elevated levels of soluble salts and heavy metals, particularly copper and nickel. Numerous grasses, forbs and woody plants will tolerate the tailing as a rooting medium. Peat incorporation and topsoil dressing provided few benefits to the revegetation process which were not provided by a fertilizer application. With fertilization, grass/legume production in the tailing was comparable to local agricultural yields. Concentration of heavy metals in grasses grown in the tailing were generally below suggested tolerance limits for plants and animal forage. Legumes tended to accumulate higher concentrations of copper and nickel, and metal uptake of most plants was positively correlated with rate of fertilization. Tailing drainage water contained elevated levels of heavy metals, and establishment of vegetation had little effect on the quantity and quality of tailing drainage water. However, topsoil dressing significantly increased drainage water volume when compared to unvegetated control plots. Copper-nickel tailing revegetation recommendations were developed.

Jan 1, 1983

By Jeremy P. Doolan, Leigh B. Neindorf, Geoff W. Capes

The development and use of rock mass classification tools have been a key component for improving stope design over the past 4 years at the Xstrata Zinc George Fisher Mine in northern Queensland, Australia. In 2003, stope extraction data from 3 years of open-stope mining provided an excellent situation to review the assumptions in the feasibility study. Extracted stope profile information, drillhole geotechnical data, underground observations, and oral and written communication were used to develop a thorough stope reconciliation performance database. With-out collecting the back analysis data and presenting the data in a usable format, engineers are left to debate opinion instead of engineered judgment. This can lead to biased and uninformed design parameter choices with the potential to repeat poor design. This paper demonstrates some effective, practical examples of empirical data collection where rock mass classifications tools were developed and used to create improved confidence in predicting stope stability and failure profiles. The work contributed to design changes that resulted in a reduction in stope hangingwall dilution and an increase in head grade while continuing to ramp up production from 2003–2005.

Jan 5, 2007

By William F. Hahn

This report describes an illumination system suitable for use in a slope under construction, Simulator work was performed using actual lighting hardware to verify adequate light levels to meet MSHA proposed regulation (as published in the Federal Register, January 13, 1977). The sequence of operating activities for two different slope driving sites are discussed and lighting requirements are defined for each,

Jan 1, 1981

By Graham W. Marks

Recently it was shown the total energy method of spectrochemical analysis is suitable for the quantitative estimation of many of the elements of which ores are composed. It was shown how this method can be applied to the determination of germanium, tin, and lead. Continuing, this work, the present report deals with analyses for beryllium, zinc, cadmium; and indium. There are three basic problems in these investigations. The first is to study the influence of those elements that make up the greater part of an ore sample on the spectral-line intensities of the elements for which analyses are being made, the latter generally being the minor constituents. The second is to develop proper methods for the preparation of standard spectrographic curves. Finally, we are concerned with improvement in equipment and procedure, so that greater accuracy can be achieved. As discussed previously, it is better to study as groups those elements that belong to the same group in the periodic table because their spectra are similar. Beryllium, zinc, and cadmium are thus related. Indium was included in this work because it is, associated with zinc and cadmium in zinc ores.

Jan 1, 1948

By Joseph M. Kurtak

The Bureau of Mines is currently conducting a four year mineral assessment of the 5.7 million acre Valdez Creek Mining District in Southcentral Alaska, as part of its ongoing statewide mining district evaluation program. This report is a summary of the 1987 field work, which included the examination of mines, prospects, and mineral occurrences in the study area. Placer gold has been the most important metal produced in the area, and production totaled 161,131 oz, with the majority of the production coming from the Valdez Creek Mine. Lode gold and silver production totaled 1,581 oz and 8,617 oz, respectively and came mainly from the Golden Zone Mine. Varying amounts of other metals, including copper, lead, zinc, molybdenum, antimony, chrome, nickel, cobalt, tin, tungsten and platinum exist in the study area. Occurrences of industrial limestone and coal are also located in the area.

Jan 1, 2011

By L. Garner McDonald

The U.S. Bureau of Mines, under contract to the U.S. Department of Energy, investigated the erosive-wear properties of seven commercial alloys with potential applications as valves for coal-conversion plants. A dry particle, jet-erosion apparatus was used to determine the wear of seven materials: 316 and 440-C stainless steels, K-68, K-701, and K-801 cemented tungsten carbides, HC-250 white cast iron, and Haynes 6B. The alumina abrasive entrained in the nitrogen gas jet had particle sizes of 27 or 50 µm, the abrasive velocities were 55 to 170 m/s, and the particle impingement angles were 15° to 90°. The maximum specific wear for ductile materials was found to occur at impingement angles of 15° to 30°, and the minimum specific wear occurred at 60° to 90°. For the brittle materials, maximum specific wear occurred at impingement angles of 50° to 85° and minimum specific wear was at the lowest angles. As the velocity and erosive particle size increased, the specific wear increased. The specific wear was related to the velocity by the power function WocAVn, where n was 1.8 to 3.9 for ductile materials and 1.8 to 3.6 for brittle materials.

Jan 1, 2010

By Donald F. Reed

In the Coastal Plain sedimentaries of northeastern Mississippi, high-alumina clays and kaolins, which are bauxitized locally to varying degrees, are found in many places along the contact between the Midway (Paleocene) and the Wilcox (Eocene) series. The trace of the contact extends from Tippah County, on the Tennessee border, south to Winston County, thence southeast to Lauderdale County, and into Alabama. Its length within Mississippi, disregarding sinuosities, is 185 miles (fig. 1). Commercial production of bauxite from the region has amounted to about 400 tons, shipped from one outcrop in Komper County. In December 1941 and January 1942, the Bureau of Mines and the Federal Geological Survey made a reconnaissance survey of the contact zone and selected the most promising areas for further study. In 1942, four areas in Benton, Union, and Pontotoc Counties were investigated by auger and rotary core drilling, and in 194, core drilling was done on five areas in Kemper, Noxubee, and Winston Counties. The present report records the work done by the. Bureau of Mines and the factual data obtained from the investigations of the nine areas in the two projects.

Jan 1, 1952

By Walter D. Holland

This instructors guide is intended for use in a course which teaches metal and non-metal mine inspectors to perform surveys for inhalation contaminants in above ground metal and nonmetal mine work areas. The handbook entitled "Handbook for Surveys of Inhalation Contaminants in Above Ground Metal and Nonmetal Mining and Processing Work Areas? is used as a manual during the course. The manual contains a survey check list, rules for determining if sampling is required, a list of most frequently encountered contaminants, a list of candidate contaminants and their sampling conditions, and a description of control procedures and devices. There are several experiments in this guidebook which the trainees perform to acquaint them with the sampling systems.

Jan 1, 2011

1. Domestic Production and Use: In 1982, 13 companies operated 30 primary aluminum reduction plants, with 3 firms accounting for 55% of production. Washington, Oregon, and Montana accounted for 34% of the production; Texas, Louisiana, Missouri, and Arkansas 18%; Tennessee, Alabama, South Carolina, and North Carolina 14%; other central and eastern States 34%. Based on published producer prices, output of primary metal in 1982 was valued at over $5.5 billion. Aluminum consumption by 25,000 firms was centered in the East Central United States. Packaging accounted for an estimated 39% of domestic consumption in 1982, transportation 20%, building 14%, electrical 8%, consumer durables 8%, and other uses 11%.

Jan 1, 1983

By M. J. Ferrante

The Bureau of Mines investigated the applicability of the freeze-drying technique for preparing dispersion-strengthened tungsten powders suitable for conversion by powder metallurgy into materials which might have improved high-temperature strength. Extruded rods from compacts of tungsten-5 vol pct thoria had at 1,650° C a tensile strength of 30,300 psi and a 10-hour stress-rupture strength of 12,700 psi, These are slightly below those measured for swaged rods of commercial tungsten-3.7 vol pct thoria. Only those tungsten-thoria dispersions containing a stoichiometric deficiency of oxygen yielded a significant strengthening effect. A low-melting eutectic formed in extruded tungsten dispersions containing either zirconia or yttria, which caused a lowering of the tensile strengths. These tensile strengths were only slightly higher than strengths of elemental tungsten made from commercial powder having a particle size of 2.4 microns (Fisher subsieve). Sheet made from this commercial tungsten had a slightly higher tensile strength than tungsten made by freeze drying, but the freeze-dried tungsten sheet had a lower recrystallization temperature, a lower ductile-to-brittle transition temperature, and a higher purity.

Jan 1, 1971

By Kim B. Shedd

The U.S. Bureau of Mines Particulate Mineralogy Unit examined the habits of six zeolite minerals commonly occurring in domestic zeolite deposits. Mineral habit is of interest because current theory on the potential for sarcoma production in test animals emphasizes the size and shape of mineral particles, without regard to composition or structure. A scanning electron microscopic study revealed that, of these six minerals, only mordenite and erionite crystallized in acicular to fibrous habits, The fibrous varieties of these two minerals were characterized by size and shape on the transmission electron microscope, and their dimensions were compared with those of asbestos and amphibole cleavage fragments. When comminuted, these two minerals possess "fibrosity indices" similar to those of amphibole cleavage fragments. One sample, a rare woolly erionite, has uniform widths, large aspect ratios, and a "fibrosity index" similar to those of asbestos.

Jan 1, 1982

By K. J. Liles

The Federal Bureau of Mines conducts a comprehensive test program on clay and shale at the Tuscaloosa Metallurgy Research Center. All samples are subjected to standard preliminary ceramic tests, which include firing formed briquets at temperatures ranging from 1,000° to 1,250° C to identify firing range and colors, and quick-firing to determine bloating characteristics. Materials that shop potential as structural products are further tested after either extrusion or dry-pressing. If the quick-fire test is positive, bulk samples can be fired in a rotary kiln to evaluate their potential as light- weight aggregate A number of miscellaneous tests also can be conducted if requested. These tests determine properties such as refractoriness (pyrometric cone equivalency), oil-bleaching characteristics, oil absorbency, viscosity for drilling-mud applications, sand-bonding properties for foundry usage, and pelletizing characteristics.

Jan 1, 1977

By John R. Bartels

Remote operation of continuous mining machines has enhanced the health and safety of underground miners in many respects; however, numerous fatal and non-fatal continuous miner struck-by accidents have occurred. In an effort to prevent these injuries, NIOSH researchers at Pittsburgh Research Laboratory studied the workplace relationships between continuous miner operators and various tramming tasks of the equipment using motion capture data, operator response times, and field of view data to evaluate the factors influencing operator-machine struck-by events (contact with a solid object) in a virtual mine environment. It is not feasible (nor ethical) to use human subjects to directly evaluate factors that precipitate such injuries. However, use of motion analysis data and digital human models can facilitate analysis of struck-by accident risk by allowing investigators to manipulate factors that influence injury. Factors included in this study included machine speed, direction of escape, the direction the operator was facing relative to the machine, work posture, distance from machine, and operator anthropometry. Close proximity to the machine, high machine tramming speeds, a right-facing orientation and operator positioning near the tail all resulted in high risk of being struck.

Jan 1, 2008

By S. L. Gerhard

In the United States the performance characteristics of permissible explosives are controlled by routine tests, which include firing the explosive into a gallery filled with a methane-air mixture. These tests are made by the staff-of the Explosives Division of the Bureau of Mines and are similar, in general, to those employed in other countries. This control has helped to reduce the frequency of accidents involving the ignition of firedamp by explosives but has not clarified the basic causes of the ignition. To advance this control and to minimize potential hazards further, this fundamental knowledge is needed. Some of the results of recent research on the causes of the ignition are described herein. NATURE OF THE PROBLEM When an explosive ignites firedamp in the gallery tests, the source of the ignition must be one or more of the emissions from the steel borehole. It has been accepted generally that these emissions are (1) particles, (2) the shock wave, and (3) hot gases and flames. Photographs show that the shock wave emerges from the borehole first, followed closely by hot gases. At first the velocities of these are high and approximately equal, but the velocity of the gases decreases more rapidly than that of the shock wave, and by the time the reactions causing the flame are complete the shock wave travels in an otherwise undisturbed medium. The particles are originally enveloped in the hot gases but some soon begin to break through and eventually out-distance the shock wave. The approximate geometry of these emissions about 1 millisecond after the shot is fired is illustrated in figure

Jan 1, 1939

By H. R. Babitzke

As part of a continuing project to develop refractory metal alloys for high-temperature structural applications, the Bureau of Mines applied solid solution and precipitation strengthening techniques to improve the properties of columbium alloys. The purpose was to investigate the effects of hafnium, tungsten, and boron on the formability, strength, and oxidation resistance of columbium. The experiment was of factorial design with two replications which called for 72 ingots of 36 basic compositions, weighing 150 grams each. Hafnium, tungsten, and boron were evaluated at 3, 3, and 4 levels, respectively. Values of alloy content are all in atomic percent. The highest strength observed was 29,000 psi at 1,200° C for alloys Cb-15Hf (No. 3), Cb-7.5Hf-5W-2B (No. 14), and Cb-15Hf-5W-2B (No. 15). At 1,200° C, the ternary alloy Cb-15Hf-5W (No. 6) which has shown good properties in previous Bureau of Mines investigations was the most resistant to oxidation For boron additions, the alloys oxidized more readily with increasing amounts of this element. The fabricability of the alloys high in boron became increasingly difficult, resulting in an inadequate number of alloys required for a complete statistical analysis for all the tests. As a result of the decrease in ductility, an insufficient quantity of tensile samples were available for a proper analysis for the high-temperature strength data.

Jan 1, 1970

By Parviz F. Rad

This Bureau of Mines report reviews laboratory and in-mine techniques for determining mechanical properties of coals, with special emphasis on the relationship between these properties and the minability of coal. An extensive bibliography is included.

Jan 1, 1973

By Phillip R. Moyle

Several deposits in the Sheep Hole/Cadiz Wilderness Study Area (WSA) have small identified or potential for undiscovered gold and silver resources. One prospect area is a potential target for molybdenum. Most base and precious metals and one uranium deposit in the study area are of the fissure-filling, contact metamorphic type associated with late stage fluids of the Cretaceous Cadiz Valley batholith. Some evidence suggests limited Tertiary and Quaternary mineralization. Mineral deposits are controlled by faults, shear zones, and joints which strike northwest and dip northeast or southwest. Although undefined, calcium, sodium, lithium, and strontium brines are inferred within the study area. Some potential for oil and gas and geothermal resources is indicated by the interest private industry has shown in the eastern part of the study area. INTRODUCTION The U.S. Bureau of lines and U.S. Geological Survey conducted a mineral survey of the Sheep Hole/Cadiz Wilderness Study Area (p1. 1) which encompasses approximately 205,000 acres (83,000 ha) in south-central San Bernardino County, California. The U.S. Bureau of Mines studied the mineral resources of mines, prospects and mineralized areas; geological, geochemical, and geophysical investigations were conducted by the U.S. Geological Survey.

Jan 1, 1982

By S. L. Gerhard

In the United States the performance characteristics of permissible explosives are controlled by routine tests, which include firing the explosive into a gallery filled with a methane-air mixture. These tests are made by the staff of the Explosives Division of the Bureau of Mines and, are similar, in general, to those employed in other countries. This control has helped to reduce the frequency of accidents involving the ignition of firedamp by explosives but has not clarified the basic causes, of the ignition. To advance this control and to minimize potential hazards further, this fundamental knowledge is needed. Some of the results of recent research on the causes of the ignition are described herein. NATURE OF THE PROBLEM When an explosive ignites firedamp in the gallery tests, the source of the ignition must be one or more of the emissions from the steel borehole. It has been accepted generally that these emissions are (1) particles, (2) the shock wave, and (3) hot gases and flames. Photographs show that the shock wave emerges from the borehole first, followed closely by hot gases. At first the velocities of these are high and approximately equal, but the velocity of the gases decreases more' rapidly than that of the shock wave, and by the time the reactions causing the flame are complete the shock wave travels in an otherwise undisturbed medium. The particles are originally enveloped in the hot gases but some soon begin to break through and eventually out-distance the shock wave. The approximate geometry of these emissions about I millisecond after the shpt is fired is illustrated in figure

Jan 1, 1939

By Martin D. Conyac

A 1984 Bureau of Mines investigation identified ho mineral resources in the Wilderness Study Area (WSA). However, four prospects in the WSA contain anomalous amounts of copper and silver minerals; one had traces of gold. Stratabound copper-silver occurrences appear to be prevalent. Quartz veins in the WSA locally contain trace gold, and one mine adjacent to the area produced some gold in the late 1800's. The WSA is underlain principally by Precambrian and early to middle Paleozoic quartzites, argillites, dolomites and limestones that have been complicated by faulting, generally tilted northeastward, and thrust southeastward over sequences of late Paleozoic sedimentary rocks. The stratabound copper-silver occurrences and gold-quartz veins are in Precambrian and Cambrian rocks in the western part of the WSA, as are similar deposits regionally. Sand and gravel, and limestone are abundant, but plentiful resources of these commodities are nearer established markets. In November 1983 there were 5 small groups of current claims oh the WSA boundary; none are patented claims. Probably less than 35 claims have been located within the WSA, mostly in the northwestern portion; hut over 100 claims have been located outside, near the northwestern boundary. Oil and gas leases nearly surround the boundary and 6 extend up to 1 mile into the study area. There has been no recorded mineral production from within the WSA. From 3 to 5 miles to the west, several lode nines in the Johnnie district have produced several million dollars worth of gold from quartz veins, and some silver and lead from galena-calcite veins. These veins generally trend northeasterly and dip northwesterly and probably do hot extend into the study area.

Jan 1, 1985