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By Ralph B. Adair

The Bureau of Mines conducted laboratory and small-scale, continuous tests of weathered mica-pegmatite ores from Randolph County, Ala., to determine the feasibility of recovering commercial-grade mica concentrates by flotation. Two flotation methods were used in continuous tests for recovery of mica. One method utilized acid-cationic flotation for the recovery of coarse mica and alkaline-anionic-cationic flotation for recovering fine mica. This method yielded mica concentrates containing 98.6 percent mica with a recovery of 85.9 percent. The other method was based on the Bureau-developed alkaline-anionic-cationic method, and yielded concentrates containing 97.5 percent mica with a recovery of over 90 percent. In both methods, preconcentration of the ground ore on a Humphreys spiral was employed to reject over half of the feed in a product virtually free of mica.

Jan 1, 1968

By T. Christos

The explosive oils, nitroglycerin (NG) and ethylene glycol dinitrate (EGDN), were extracted from dynamites by a halocarbon solvent and were then determined by high-pressure liquid chromatography. Separation was achieved by liquid-liquid chromatography on a column packed with Durapak-Carbowax 400/Corasil II and the eluted NG and EGDN were detected with a double-beam ultraviolet detector.

Jan 1, 1973

By J. E. Emmerling

The Federal Bureau of Mines investigated dust suppression obtained with three different water-spray nozzle systems during underground continuous coal mining at the face. The nozzles were the "regular" nozzle normally used by the mine, and high-efficiency and low-efficiency nozzles selected on the basis of an airborne capture theory of respirable dust by spray drops. The high-efficiency nozzle used one-third less water than the others throughout the testing. Results depended on the type of cutting operation at the face. The sump-downshear operation appeared to involve a significant amount of capture of airborne respirable dust. The same amount of dust was measured when using the high-efficiency and regular nozzles. The dust levels when using the high-efficiency nozzle were about 20 pct less than those measured when using the low-efficiency nozzle. The sump-upshear operation seemed to involve a predominance of other aspects of dust suppression, such as impaction of spray drops onto the face. Compared with the downshear operation, there was a significant reduction in dust levels for a total face operation when using the regular nozzle; dust levels when using the regular nozzle were about 15 pct lower than those measured when using the high-efficiency nozzle.

Jan 1, 1975

By W. S. Sanner

A High Splint coal was carbonized in a low-temperature, fluidized-bed sys-tem to study the effects of thermal cracking on the products of decomposition. The coal was fluidized in recycle gas at 485° to 600° C, and the products were cracked at 600°, 700°, and 800° C in a bed of fluidized coke. Yields of tar, pitch, paraffins, and olefins decreased as carbonization temperature increased. Thermal cracking of the tar vapors produced the highest tar yields at 600° C, and light oil yield increased at cracking temperatures up to 700° C. At an 800° C cracking temperature, the yield of light oil decreased.

Jan 1, 1969

Continuously separate mixture of non-magnetic materials (such as scrap, precious metals, or certain ores) at a reasonable cost. Approach Nonmagnetic materials of different densities are rapidly float/sink separated by an augmented lifting force produced In a magnetic fluid (liquid) by the effect of an external magnetic field. The magnetic fluid is a colloidal suspension of magnetite In kerosene, prepared by a low-cost process. How It Works Separation is accomplished in an open trough filled with magnetic fluid. A magnetic field is established in the fluid, by energizing an electromagnet having poles on each side of the trough. Due to the design of the magnet poles and air gaps, the magnetic field is strongest at the bottom, about 10,000 oersteds, and uniformly decreases in strength to about 2,000 oersteds at the top of the fluid. Therefore, the magnetic field gradient increases with depth. The magnetic force attracts the entire separation medium (magnetic fluid) creating a reaction force of equal magnitude and acting in the opposite direction. This reaction created within a magnetic fluid/magnetic field combination is called a magnetic levitation force. It increases with the field strength. In this case because the magnetic field is strongest at the bottom of the trough, the magnetic levitation force will quickly float lighter material while heavier material sinks.

Jan 1, 1980

To devise an economical, environmentally acceptable method for recycling scrap lead-acid batteries. Approach A combination electrorefining-electrowinning method for recycling lead metal and sludge from scrap batteries was devised which produces a 99.99 + percent pure lead product and eliminates the lead and sulfur oxide emissions that are the normal by-products of high-temperature smelting processes. How the Method Works Lead metal grids and lugs are separated from the battery sludge by washing and screening, and are melted and cast into anodes for electrorefining by the Betts process. The electrolyte used is fluosilicic acid, a large volume waste product generated during the production of phosphate fertilizer. During the electrorefining process, impurities in the anode are trapped and held in an adherent slime blanket on the surface as the anode dissolves while pure metallic lead is deposited on a lead cathode. The major problem in the past has been to recover the lead from the battery sludge which consists of approximately 60 percent lead sulfate, 21 percent lead, and 19 per-cent lead dioxide. In the flow sheet developed by the Bureau

Jan 1, 1983

By Roy H. Grau, John C. LaScola

"This Bureau of Mines report contains a tabulation of methane emissions during 1980 for all coal mines located in the United States with emissions greater than 0.1 MMcfd. Listed for each mine are methane emission quantity, location, and coalbed. The report also compares records of 1975 and 1980 and describes relationships between emissions in 1980 and the Bureau's coalbed gas content data on 11 mines.INTRODUCTIONMethane gas is a threat to safety in underground coal mines. Research by Government and industry has led to great gains in reducing methane gas ignitions and explosions. The development of advanced methane control techniques is necessary for the safe operation of more gassy mines and the implementation of rapid mining techniques.As part of this research, the Bureau of Mines has surveyed total methane emission data from underground bituminous coal mines in the United States and tabulated emissions from mines producing over 0.1 MMcfd of methane. This report is an update of similar studies previously described in Information Circulars 8733, 8659, and 8558 (2-4).3The data from 1980 were compiled from Mine Safety and Health Administration (MSHA) records of air quality-quantity inspections made quarterly at each mine. The inspections involve measuring airflow and collecting air samples in the main returns. From these data, an average methane emission is calculated and used to represent the daily mine emission for each quarter. The methane emissions given in this report are the averages of the four 1980 quarters and do not include mine emissions from other sources such as degasification projects. Since a previous Bureau study showed that emissions from mines emitting less than 0.1 MMcfd represented only 2 pct of all emissions, 0.1 MMcfd was chosen as a lower limit for data collection (4)."

Jan 1, 1982

By T. R. Taubert, D. H. Carlson, J. H. Johnson

The U.S. Bureau of Mines and Michigan Technological University (MTU) are collaborating to develop an apparatus for measuring diesel tailpipe emissions in underground mines. A tailpipe emissions measurement apparatus (EMA) is described that dilutes diesel exhaust and measures the concentrations of diesel particulate matter (DPM), CO, CO, NO, and NO, at known dilution ratios. The EMA was evaluated by side-by-side comparison of its measurements with those by laboratory- grade instruments. Concentrations of CO and CO, measured by the EMA were usually within + 14 pct of concentrations measured by laboratory-grade instruments for CO and 220 pct for CO,. EMA- measured DPM concentrations were, on average, 29 pct lower than those measured by laboratory-grade instruments, with the differences being fairly consistent. The CO and CO, differences are related to the method of calculating the EMA's dilution ratio, and the difference in DPM concentrations is attributed to thermophoretic and/or condensation losses related to the EMA's unheated sample probe. Preliminary analysis of data obtained with a heated sampling probe and modifications in the sampling procedures have indicated reduced variability in DPM and in the calculated dilution ratios.

Jan 1, 1992

By Donald R. Irving

THIS CHAPTER is new to the Minerals Yearbook and will appear regularly hereafter. Its purpose is to present statistics that reflect technologic trends in the minerals and metals industries (except fuels). Much useful information has been collected annually through the Bureau of Mines mineral commodity and employment and injuries canvasses. However, these data must be supplemented by further data to permit evaluation of the type, direction, and rate of technologic change, which are vitally important in long-term mineral planning. In addition to, and fully as important as, expanding the available data is the need to ascertain that the various items collected are obtained from identical reporting units, to enable direct comparisons to be made.

Jan 1, 1960

Minimize the risk of conveyor belt fires in underground coal mines by improving the accuracy of and means by which flammability data are acquired. Approach Develop a large, laboratory-scale flammability test for mine conveyor belting that realistically assesses its fire resistance. Background A conveyor belt fire in an underground coal mine is a serious threat to life and property. To minimize the risk of belt fires, the U.S. Code of Federal Regulations (CFR) for underground coal mines requires approved fire-resistant belting. Despite this precaution, about 25% of the reportable underground coal mine fires from 1983 through 1988 involved conveyor belting. In several instances, hundreds of feet of belting were destroyed. The current flammability test for fire-resistant belting is specified in 30 CFR, Part 18.65 and is conducted by (be Mine Safety and Health Administration (MSHA). The small-scale test is performed in a 21-in-cubical chamber with 6-in-long by 1/2-in-wide belt samples. To evaluate the flammability of conveyor belting under more realistic conditions, the U.S. Bureau of Mines conducted large-scale fire tests of belting. The large-scale data were then utilized in the development of an improved laboratory-scale flame test for fire-resistant belting.

Jan 1, 1991

By Charles L. Kimbell

The series summarizing the prices of the major nonferrous metals on the stock exchanges of the United States and the United Kingdom has been continued this year in tables 23 and 24. Time constraints have prohibited preparation of other price information that has appeared in this study in previous years. Users are urged to consult the 1993 USBM publication Metal Prices in the United States through 1991, which gives an analysis of historical price series and trends, or the 1993 edition of Mineral Commodity Summaries for current U.S. prices on non fuel commodities, and to utilize U.S. Department of Energy sources for information on fuel material costs.

Jan 1, 1993

By 1928-05-01

"The carnotite ores of Colorado and Utah were the chief source of radium for many years. In the fall of 1922; news of the very rich deposits of radium ore discovered in the Belgian Congo caused almost complete cessation of domestic production. The Congo ore contains pitchblend and a number of alteration products, including the new minerals bequerelite, curite, kasolite, stasite, and dewindite. Reports indicate that a considerable amount of ore containing over 50 per cent U308 has been produced. It seemed certain that radium could be extracted from the Congo ore at a much lower cost than from the relatively low-grade carnotite; and in order to preserve their elaborate marketing organizations, the larger American producers made agreements with the Belgium syndicate to market the foreign product in this country. The price of radium has been held at $70 per milligram. Extraction of radium from carnotite by the usual methods does not appear to be profitable at that price. With one exception, all American firms ceased production after their accumulated stocks of ore had been treated. The United States Radium Co., which continued to treat carnotite for several years, has recently shut down its plant.Although there is probably a large profit derivable from the treatment of Congo ore, it is not likely that the Belgium Syndicate will meet sufficient competition to cause any reduction in the present quotations. It is not known how long the high-grade ore will last, but when exhausted the price of radium may be expected to advance. According to K. L. Kithil3 it is the opinion of interested parties that, so far as can be forseen, radium will in future years never again be obtained at the present low price.Carnotite contains the valuable element, vanadium, which is not present in the Congo ore. The recovery of-vanadium is an important factor in the cost of extracting radium from carnotite, and under favorable conditions carnotite can be profitably treated for the vanadium alone. Vanadifecous sandstones are found ranging all the way from roscoelite (vanadium mica), containing little or no uranium; to a high-uranium and low-vanadium carnotite. Ores containing 2 per cent or more U308 are classed as radium ore and are sold on the basis of the uranium content, which is proportional to the radium content. Only in exceptional cases have ores been evaluated on the basis of both the radium and vanadium contents, although the presence of vanadium has undoubtedly influenced the price of radium ore."

May 1, 1928

Provide a means for reliable in situ stress change measurements in soft, friable geologic materials under high stress. Background Effective mine design requires a knowledge of changes in rock stress generated by a mining operation. In situ stress measurement can provide a means of obtaining this knowledge from an active mine for the ultimate purpose of design verification and analysis. The Bureau of Mines has designed and tested a device for measuring changes in rock stress-the borehole platened flatjack (BPF). It has found application in investigating stress anomalies due to geologic structures, stress concentrations from multiple seam interaction, and stress abutments from pillar retreat and longwall mining.

Jan 1, 1990

By Howard E. Parkinson

The mine pager phone to public telephone interconnect system permits mine paging telephones to be interconnected with the public phone system, thereby providing emergency and off-hours communications. The system, a push-to-talk, push-to-listen system, is compatible with any mine paging system utilizing dc voltage on the line to enable paging. A tone generator of the proper frequency enables an outside caller to page over mine pager system loudspeakers. A caller inside the mine can make an outgoing call to a preselected, preprogramed number with the use of a proper frequency tone generator. The system includes an automatic hangup timer that restricts the time off-line due to a wrong number or incorrect hangup to 20 seconds and 6 minutes, respectively.

Jan 1, 1974

By Deno M. Pappas, Christopher Mark, Eric R. Bauer

During 1998-99, groundfall incidents resulted in 27 fatalities and were responsible for over 70% of all deaths in U.S. underground coal mines. To obtain a better understanding of where and why these incidents occurred, a comprehensive analysis of ground fall injuries and fatalities was conducted. The first portion of the study examined various factors associated with roof and rib fall injuries and reportable roof fall noninjuries that occurred during 1995-98. The study found that the room-and-pillar mining method has twice the groundfall incident rate than the longwall method. Mine locations with high groundfall rates seem to correlate to regions where there is a higher concentration of problematic coalbeds. For example, the Illinois Basin has very high groundfall rates, which can be traced back to several key coalbeds-Kentucky No. 13, Herrin/No. 6/Kentucky No. 11, and Springfield No. 5/Kentucky No. 9. High rib fall rates were found in mines located in thick seams. Groundfall rates were found to be 30% to 40% higher during the months of July through September, possibly due to high humidity that may cause the shale mine roof to deteriorate. The second part of the study examined the root causes of failure by reviewing all groundfall fatality reports for 1996-99. Primary and secondary hazard factors were assigned to each groundfall incident. The primaryf actors resulting in these groundfall fatalities were pillar extraction, traveling under unsupported roof, skin failure, construction, longwall faces, intersections, and geologic discontinuities. Defining prominent ground control incident trends and hazards will identify areas where additional study is needed and where innovative solutions need to be developed to reduce these severe occupational hazards.

Jan 10, 2000

By W. L. Cornell

The Missouri Pb ores are the only domestic Co resource being mined and processed for other metals; therefore, they present a viable short-term opportunity for Co production. Lead, zinc, and copper concentrates are produced from the ore. The Cu concentrate can contain up to 30 pct Co and the Pb concentrate up to 15 pct Co. Since Co is detrimental to the processing of the Zn concentrate; the remainder of the Co is rejected to the tailings. The tailings can contain as much as 50 pet Co originally present in the mined ore. Researchers at the U.S. Bureau of Mines have successfully tested on a continuous basis a process that recovers a bulk sulfide concentrate from mill tailings. The concentrate contains up to one-half of the Co and from 50 to 90 pct of the Pb, Zn, and Cu. Concentrate weight represents 10 pet or less of the total tailings.

Jan 1, 1989

To develop and design a bit that will rapidly drill smooth and precise instrumentation holes in soft rock. Approach Use a one-piece bit made by combining a drag bit and a diamond bit. Because a smooth-walled borehole with a precise diameter is needed for borehole pressure cells (BPC) and other borehole instruments, a diamond bit is usually used. However, diamond bit drilling is slow, and the bit will tend to bind when squeezing ground is encountered. On the other hand, the drag bit will cut faster, but the walls of the drill hole will be rough and the diameter will not be as precise. The combination will provide a bit which penetrates as rapidly as a drag bit, but retains the smooth-wall and precise borehole diameter of a diamond bit. How It Works A three-foot-length of EW-size drill rod is centered in a diamond bit by welding it to three equally-positioned spacers at each end of the bit. A drag bit is attached to the EW rod with a standard EW-to-drag bit adapter as shown in the diagram. Three equally-spaced diamond inserts are set to the desired hole size and welded to the diamond bit barrel behind the crown. These inserts increase the smoothness and precision of the hole by cut-ting away any hole closure. Three equally-spaced shims are set approximately 0.020-inch under the overall insert diameter size and welded to the rear of the diamond bit barrel. The combination bit should be used on a diamond drill with either water, mist or air as the coolant.

Jan 1, 1982

By Robert King

Splicing portable trailing cables used in underground coal mines is usually less expensive in terms of capital outlay and production time lost than replacing them. However, handling trailing cables may result in electrical arcs, shocks , and burns. Also, destructive forces encountered during a mining operation may shorten the effective life of a cable splice. This report gives the results of an analysis of cable splice defects in an effort to establish cable splice performance criteria, determine testing standards for cable splices, establish guidelines for training programs in cable splicing, and indicate areas for improvement.

Jan 1, 1975

To improve mining safety and efficiency by providing a practical way of detecting faults and channel sands that disturb coal seams. Approach A seismic system using a shallow blasthole has been developed and tested. How It Works A small shock is caused in a shallow hole, sending seismic waves through the ground. These waves are reflected from the top of the coal seam, acid are detected by a line of geophones on the earth's surface. Dampening of the seismic signals by channel sands and other discontinuities in the seam is detected and recorded. See Figure 1. The seismic shock wave can be produced by exploding small charges, dropping a weight, firing a gas gun, or actuating a vibrator. Depending on the soil cover, the shock is usually generated in shallow vertical holes about 10 feet deep. Hole depth depends on the soil mantle thickness because it is preferable that the seismic shock originate below that layer.

Jan 1, 1976

By Forrest T. Moyer

OVERALL data for 1963 on injury experience and the levels of employment, worktime, and operating activity of the mineral industries are shown in the statistical tables of this chapter. The general groupings of the industries are presented in greater detail in Volumes I and II of the Minerals Yearbook. A corresponding chapter in Volume I contains additional breakdowns of the data on metal, nonmetal, sand and gravel, slag, and stone mines and quarries together with separate information on the related processing mills and plants including primary nonferrous smelters. The more specific information on the anthracite and bituminous-coal, petroleum and natural gas, peat, and natural asphalt industries is given in the similar chapter of Volume II. Injury and employment data were collected from coal producers on the mandatory basis required by the Federal Coal Mine Safety Act (30 U.S.C., sec. 455). Producers of all other minerals (fuel and nonfuel) voluntarily reported the requested injury and employment data. The figures for 1963 are preliminary except for anthracite, coke, petroleum and natural gas, native asphalt, and slag which are final. Data for earlier years are final. The figures represent full coverage for all industries except the oil and gas industries for which coverage is not complete, particularly with respect to small companies.

Jan 1, 1964