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By W. H. Eddy

The Bureau of Mines conducted laboratory batch and continuous flotation processing tests on waste granite fines from South Carolina to determine the possibility of recovering high-quality feldspar and glass sand. Three flotation systems were used for removal of the iron-bearing biotite: Two employed an alkaline anionic-cationic circuit and the third employed an acid cationic circuit. Commercial-grade products were obtained when the remaining biotite was magnetically removed from the feldspar and quartz concentrates. Continuous flotation processing yielded a feldspar concentrate containing, in percent, 3.60 Na20, 5.60 K20, and 2.25 Ca0, with recoveries of 75.3, 66.6, and 72.6 percent, respectively. The feldspar tailing was high quality glass sand containing 98.0 percent Si02 and 0.025 percent Fe203; about 60 percent of the quartz was recovered.

Jan 1, 1972

By David A. Monaghan, Kenneth R. Maser, Adi R. Gurdar, D. Randolph Berry

APPENDIX E EQUIPMENT USED FOR FIELD TESTING OF MINE SEALING SYSTEM I. Drilling Operation - Equipment supplied by local drilling contractor 1. Mobile drill rig. 2. Flat bed truck, containing 20 lengths of drill pipe. 3. Auxiliary compressor. 4. Pickup truck for small parts and supply of diesel fuel. 5. Bulldozer. 6. Water supply, in this case the nearby stream. 7. Supply of casing, positioned next to the drill rig. 8. Ready mixed cement grout. 9. Drill bits, stabilizer units, cutting and welding equipment, other miscellaneous tools and supplies. II. Sonar Probing Operation 1. 25 foot tower with pulley mounted atop. - FMA 2. Electric winch with 100 feet of 1/4-inch cable, Model No. 100A, City Engineering Co. , Indianapolis, Indiana. 3. 400 feet of 1-1/2-inch-diameter aluminum pipe with alignment holes and coupling grooves. - FMA*

Jan 1, 1973

By S. L. Windes

"INTRODUCTION For a number of years the bureau of Mines has been engaged in the detection, recording and interpretation of earth- and air-transmitted disturbances, man-made and natural, related to mining operations. For the measure¬ment of such disturbances, special equipment was developed (1, 2, 3, 4, 8) 3/ and results of the measurements have been reported (5, 6; 7,9).In general, the ranges of amplitude end frequency of vibration encountered and recorded in the earth-transmitted disturbances were 0.00005 to 0.1 inch and 5 to 5,000 cycles per second; in the air-transmitted disturbances, pressures ranging from 0.001 to 100 pounds per square inch and 0 to 20,000 cycles per second were recorded.One characteristic of the earlier tests was that either the arrival time of the disturbance to be recorded was predictable or the recording speed was slow enough so that the record covered extended periods of time (for example, 4 hours). As the investigations continued, it became apparent that a recording device was required that would respond to transient vibrations arriving at indeterminate times and at the same time provide a permanent record of displacement or acceleration versus time on a scale that would permit the analysis of waves having frequency components up to 10,000 cycles per second. A film or paper speed of 720 inches per second was found to be adequate, as this provides approximately 3/4 inch of record for each 0.001 second."

Dec 1, 1947

By R. V. Ramani, C. B. Manula, A. Owili-Eger

That a close analogy exists between the flow of air in mines and the flow of current in electrical networks- has been known for a long time. The laws that have been used to solve series and parallel electrical circuits have been used to solve for the equivalent resistance in mine ventilation problems. Kirchhoff's current and voltage laws have also been adopted in solving mine ventilation network problems. It will be best to define a few terms here regarding networks, and with reference to Figure 1, these definitions can be elucidated. Figure 1 can be represented by the network in Figure 2 without losing any essential details. 1. A junction is a point where two or more airways meet. 2. The segment of a roadway connecting any two junctions is known as a branch. 3. A mesh is a closed path through the network. In the above network, B, C, D and F are the junctions, CF and CD are two of the branches and CFDC is a mesh. Kirchhoff's current law states that the sum of currents entering a junction. Applying this law to the junctions in the ventilation network, one obtains for junctions C and F, the following relationships: JUNCTION C: Q1 = Q4 + Q3 (1) JUNCTION F: Q2 + Q3 = Q5 (2) Similar relationships can be drawn for other junctions. Kirchhoff's voltage law states that in any complete electric circuit, the algebraic sum of the emf's must equal the algebraic sum of the voltage drops. In mine ventilation, the square law (Atkinson's

Jan 1, 1975

By Ted C. Briggs

The Bureau of Mines is evaluating the thermodynamic properties of helium and helium-containing mixtures. Twenty-two compressibility runs were made with helium at 0° C and pressures to 800 atmospheres using a Burnett-type apparatus. Data from the 22 runs were treated simultaneously and as separate runs while different functional forms and weighting factors were used. A fourth-degree-polynomial equation in the pressure gives a statistically satisfactory representation of the compressibility factor when the data are treated simultaneously and a weighting factor of Pr-3/4 is used. The second virial coefficient of helium at 0° C from this investigation is 11.997±0.015 cm3 mole-1. The stated uncertainty is the random error standard deviation. Compressibility factors determined by this investigation are precise to better than 0.01 percent and are believed to be accurate to better than 0.02 percent.

Jan 1, 1969

By W. M. Deaton

[Knowledge of the ten?erat~rre to wkich n gas ullder3atur~ted xith re- srplc t to water vapor may be cooled before the water p?f 11 3egin to condense 8 is desirable .and frec-uently iq neceTsarp in nWy resenrch md industri~J activities. This tenperrture, the dew point, i s 2 nrrticulnrly innortmt factor in high-pressure gas transmission, PS water cox?-ensate any interfere i with the flow of gos in the line. Sonetimes this interfexnce is due only to the yresence of the liquid water. At other tfncs, under certain condi- tions of pressure and teriperature, the cogdense;? water cn!nhines with the 93 to farm solid .y2: hydrctes. These solid coar~ouncis ma:/ ccllect in sufficient quantit;. to rehce materially the c~xrying cap.citg of the pipe line or ever, to ply thc line coimletelp.]

Jan 1, 1938

By W. M. Deaton

[Knowledge of the ten?erat~rre to wkich n gas ullder3atur~ted xith re- srplc t to water vapor may be cooled before the water p?f 11 3egin to condense 8 is desirable .and frec-uently iq neceTsarp in nWy resenrch c~d industri~J activities. This tenperrture, the dew point, i s 2 nrrticulnrly innortmt factor in high-pressure gas transmission, PS water cox?-ensate any interfere i with the flow of gos in the line. Sonetimes this interfexnce is due only to the yresence of the liquid water. At other tfncs, under certain condi- tions of pressure and teriperature, the cogdense;? water cn!nhines with the 93 to farm solid .y2: hydrctes. These solid coar~ouncis ma:/ ccllect in sufficient quantit;. to rehce materially the c~xrying cap.citg of the pipe line or ever, to ply thc line coimletelp. ]

Jan 1, 1938

By C. I. Pierce

The Bureau of Mines conducted laboratory tests to determine if ultrasonic energy could reduce either the residual water or oil content of petroleum reservoir-rock samples from Appalachian area oilfields. Brine-saturated core samples were flooded with oil to residual brine saturation and subjected to 20 kilocycles per second ultrasonic energy. Then they were flooded with brine to residual oil saturation and again subjected to ultrasonic energy. Additional water displaced as a result of the application of ultrasonic energy to the flow system ranged from 0 to 4.3 percent of the original brine and averaged 1.9 percent. The increase in oil recovery as a result of the ultrasonic energy ranged from 0 to 9.0 percent of the original oil and averaged 3.1 percent. On the basis of the tests, it appears that 20-kcps acoustic waves would not have field application for oil recovery.

Jan 1, 1968

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

B 3 Principle Program Nomenclature The principal variable names used in the computer program are defined below. The following dimensions are applicable, unless otherwise indicated. Distance - Ft Velocity - Ft. /Minute Time - Minute

Jan 1, 1976

By W. N. Poundstone, W. M. Merritts, B. A. Light

A joint investigation by the Bureau of Mines and the Christopher Coal Co. at the Humphrey No. 7 mine, operating in the Pittsburgh coalbed in northern West Virginia, was undertaken to gain more insight concerning the hazardous emission of methane gas in mining. This report describes the equipment, procedure, and results. Horizontal bleeder holes drilled in the faces drained large quantities of methane, eliminating downtime of mining equipment. Also, larger quantities of methane were removed by forcing 14 to 25 g,.p.m. water at 25 to 200 p.s.i. 5 pressure into the bleeder holes. In one infusion test a fluorescein dye was added to the infusion water; in later mining operations, the infusion water was traced for a distance of 1,500 feet. With vacuum pump applied to the horizontal hole the gas-flow rate increased, and the methane content decreased. Tests indicated that methane and water infused in bleeder holes traveled along the bedding planes of the Pittsburgh coalbed at a faster rate than across the planes. Methane associated with coalbeds is produced by the slow decomposition of carbonaceous material in the absence of air and the presence of water. It is lighter than air and, depending on its concentration, forms an inflammable or explosive mixture with air. It is believed that methane is entrapped in and around the pores of the coal and adjacent strata--often under great pressure. In many cases where the strata have been disturbed by geologic movements the

Jan 1, 1962

By D. B. Taliaferro

An accurate knowledge of the water content of oil-bearing sands4/ now is recognized as an important factor in calculations of the flow of oil through the sands to producing wells and in the estimation of oil reserves. To this end the Bureau of Mines laboratories are using a method that is an adaptation of the A. S. T. M. method of determining the water content of petroleum products (1).5/ However, the apparatus and technique have been altered slightly, as described in this report, to increase the precision of the method without affecting the simplicity of procedure or speed with which determinations may be made. Until recently petroleum engineers, when estimating reserves assumed that the entire pore volume of the oil-saturated parts of producing sands was filled with oil, as it was generally thought that the oil, water, and gas in any formation had separated completely during geologic time into distinct layers because of their difference in density. In 1929 Lindthrop and Nickolaeff (12) reported experimental results from which they concluded that 22 to 30 percent of the pore volume of producing sands in the Grozay district, Russia, was filled with water when the fields were discovered. Since that time numerous investigators (5, 7, 8, 10) have found evidence of water in the sands of now oil-producing fields and old fields that never produced water with the oil.

Jan 1, 1940

By D. B. Taliaferro

An accurate knowledge of the water content of oil-bearing sands4/ now is recognized as an important factor in calculations of the flow of oil through the sands to producing wells and in the estimation of oil reserves, To this end the Bureau of Mines laboratories are using a method that is an adaptation of the A. S. T. M. method of determining the water content of petroleum products (1).5/ However, the apparatus and technique have been altered slightly, as described in this report, to increase the precision of the method without affecting the simplicity of procedure or speed with which determinations may be made. Until recently petroleum engineers, when estimating reserves assumed that the entire pore volume of the oil-saturated parts of producing sands was filled with oil, as it was generally thought that the oil, water, and gas in any formation had separated completely during geologic time into distinct layers because of their difference in density. In 1929 Lindthrop and Nickolaeff (12) reported experimental results from which they concluded that 22 to 30 percent of the pore volume of producing sands in the Grozay district, Russia, was filled with water when the fields were discovered. Since that time numerous investigators (5, 7, 8, 10) have found evidence of water in the sands of now oil-producing fields and old fields that never produced water with the oil.

Jan 1, 1940

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

C 3 Hoist Assemblies (Man rated) A total of nine companies were identified who manufacture and supply man-rated hoisting equipment suitable for below ground installations. 1. The Coeur d' Alenes Company

Jan 1, 1976

By Lloyd A. Morley

This report abstracts project work performed under USBM Grant GO155003 during the period 4 November 1975 to 3 November 1976. The research was funded, as a continuance of previous support from USBM Grants GO133077 and G0155003, to gain further knowledge in mine electrical system safety. Five reports have been separately produced, all under the grant title, "Coal Mine Electrical System Evaluation," and are as follows: 1. Volume I - Continuous Monitoring, 2. Volume II - Transient Analysis, 3. Volume III - Shielded Cables, 4. Volume IV - Computer Modeling, and 5. Volume V - Battery and Battery-charging Safety. Abstracts of these comprise the balance of this document with one exception. The task ?d-c offsett currents," does not fall under the scope of the other report volumes and, further, the material to be presented does not justify a separate report. Hence, this subject concludes the Executive Summary.

Jan 1, 1977

By E. G. King

Cerium and thorium sulfides have found use as crucible materials for melting certain radioactive metals. However, thermodynamic treatment of these sulfides has been hampered by lack of experimentally derived entropy values. This Bureau of Mines report describes heat-capacity measurements between 51° and 298° K, and entropy evaluations at 298.15° K, for cerium monosulfide (CeS), cerium sesquisulfide (Ce2S3), and thorium disulfide (THS2). The entropy values, with Literature results for the heats of formation, are used to obtain free energies of formation at 298.15°K. MATERIALS The samples used in this work were supplied by Prof, Leo Brewer of the Department of Chemistry, University of California. The methods of preparation and some of the physical and chemical properties of these sulfides were given by Eastman and coworkers.3 4/ Chemical analyses, conducted in our laboratory, gave the following results:

Jan 1, 1959

By John D. Sullivan, Edward P. Barrett

The experimental work on the utilization of tin-plate scrap at the North- west experiment station of the U. S. Pireau of Mines in cooperation with College of Mines, University of Washington, necessitated the selection of a simple method for the determination of tin in the iron produced. Some of the standard methods for the determination of tin which were tried are given below: 1. Dissolving in acids and precipitating the tin as sulphide, igniting and weighing as Sn02. 2. Dissolving in aciis, reducing with nickel, cooling in an atmosphere of carbon dioxide, end titrating with standari iodine solution. 3. Dissolving in acids, precipitating the tin as sulphide, dissolving this sulphide in H3 and H2S04, heating until fumes of 503 are evolved, reducing with nickel or sheet lead, cooling in an atmosphere of carbon dioxide, ani titrating with a standard iodine solution.

Mar 1, 1923

By Steven J. Page, John A. Organiscak

Airborne dust generation is one of the byproducts of coal mining, processing, and handling. The amount of airborne total dust (ATD, respirable size and larger) and airborne respirable dust (ARD) generated is of primary interest for designing the level of engineering controls needed for adequate dust abatement. Laboratory crushing experiments were conducted in a wind tunnel with a roll crusher to identify relationships among crushing parameters, product size, coal rank properties, and airborne dust generation. Through the first series of experiments, the effect of primary and secondary breakage processes on both product size and airborne dust generation was examined. Through a second series of experiments, the effect of coal rank properties on product size and airborne dust generation was studied using a uniform crushing process with secondary breakage. Laboratory results indicate that secondary breakage of a particular coal notably increases the specific amount of ATD generated, while negligibly impacting the specific amount of ARD generated. A strong positive relationship was identified between the specific amounts of ATD and ARD generated during the primary breakage process (with minimal secondary breakage), but a negligible relationship was observed between the same two variables when secondary breakage was introduced into the crushing process. This indicates that most of the ATD and ARD is generated from the primary breakage, while secondary breakage has a more of an influence on generating additional amounts of larger sized ATD. Additional experiments involving the uniform crushing of eight different bituminous coals showed that the coal rank, expressed as the inherent moist fuel ratio (MFR = fixed carbon =(volatile x inherent moisture)), had diverse relationships between the product size created and the amount of airborne dust generated. As bituminous coal rank or MFR increased, the amount of coal product fines < 250 gm increased while the mass percentage of ATD and ARD liberated from these < 250 µm product fines decreased. Air dry loss (ADL) moisture in the coal was found to be inversely related to the dust cloud electrostatic field, influencing dust liberation from the coal product fines. Since the MFR was directly related to the dust cloud electrostatic field, opposite the ADL-electrostatic field relationship, the diverse relationships between the product size created and the amount of dust liberated from the < 250 µm product fines were explained. Finally, 12 to 14 times more ATD was generated as compared to the ARD generated during these experiments. These results should provide a fundamental basis for initial estimation of the airborne dust loading requirements of engineering control methods for coal crushing.

By McHenry Mosier

The diamond-drill method was tried at the site selected for driving a 5- by 6 -foot air shaft at the east end of the Bellefonte mine . This method of sinking consisted , first , of drilling a 5-3/4 -inch-diameter cut hole from the surface , then drilling parallel 1.5 - inch ( EX ) holes around it at appropriate distances for a balanced blasting round . The cut hole was not charged with explosive but served as a relief chamber for the incipient expansion of the ground broken by. blasting the surrounding 1.5 - inch holes . The length of each hole was 236 feet , which was the finished depth of the shaft . The nature of the work in the air shaft was largely experimental , and many difficulties arising from the lack of special equipment and proper technique for precise alinement of the drill holes caused expensive delays before they could be overcome . Drilling the 5-3 /4 - inch hole , which was impeded by frequent core blocks in the core barrel , required 10 shifts . average advance per shift for an EX hole was about 150 feet . The The holes were charged and fired from the surface . The length of the section blasted in one cycle was 10 feet . Blasting progressed from the bottom of the shaft upward . The broken stone dropped into a chute , from which it was drawn into cars on the haulage level . The Bellefonte mine is an underground limestone mine.3/ The primary objective in undertaking the research on shaft sinking by diamond drilling was to perfect a method for driving connections between levels of the mine .

Oct 1, 1948

By Wilbur I. Duvall

Nineteen quarry blasts were instrumented with particle-velocity gages mounted in a uniform soil overburden, back of one face in a quarry in Iowa. Three components of particle velocity, radial, vertical, and transverse, were recorded at each of eight stations back of each blast. Distances from blast area to gage stations ranged from 150 to 3,000 feet. Eleven of the quarry blasts employed millisecond delays, and eight were instantaneous blasts. Charge weight per hole was 200 pounds, and the charge weight per delay interval, including the instantaneous blasts, ranged from 100 to 3,000 pounds. Analysis of the data from these tests shows that the particle velocity, V, produced at distance, D, by a quarry blast of charge per delay interval, W, can be represented by an equation of the form, V=KWb D-n, where b and n are exponents, and K is the intercept constant which is a measure of the level of vibration. The value of K for a millisecond-delayed blast employing one hole per delay interval is about 42 percent larger than the value of K for a single-hole blast. The value of K for a multiple-hole milli-second-delayed blast is about the same as that for an instantaneous blast when the charge per delay for the millisecond blast is equal to the total charge for the instanteneous blast. The vibration level from millisecond-delayed blasts employing one hole per delay is shown to be independent of the length of the delay interval and the number of delay intervals over the range of the variables tested: 9, 17, and 34 milliseconds and 3, 7, and 15 delays per blast.

Jan 1, 1963

By A. R. Mumford

The fuel economy ot a. plant m be better than ite anxious friend.a J'ealize. A watchful a-aper1.ntend.ent of a Goverment plant, kn.owing that improvements in plant equipment bad. been made since hie atOkel'e were installed, was almosi per­ suaded to aubatitute a new t.,pe. The Bul'eau. of Mines was asked to aaoertain the a.cti.i&l performance ot the old stokera and tound. the plant alr doing from three to five per cent better than was promieed for the new egp.ipment. Tbe va.1.ue ot accurate knowledge of plant perfoimarice, am the need. ot eqm.pment to weigh and measure quantities is thus demonstrated. The boiler and ,tour ett1c1enc, was found to be 75 per cent, and the overall efficiency of the boiler, etoker• and economize, wae 78 per cent. Both records are high, and are to be attributed to ce in operation, to good working condition of the plant, and to the low rate ot evaporation, which was only aboui two-third., et the botler'e rated. capacity. The plant teated conaiated ot two la.boock & Wilcox boiler, tired b1 means of over teed 1toker1 and equipped wi t,b. a fuel economiaei- 1n the uptake. The bo1lel'a ,upplied ateam to two large water pump being used only intermittently.

Jul 1, 1922