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By M. Howard Berliner

During the spring of 1944, the Bureau of Mines investigated the Crescent mine area near the village of Rewey, Iowa County, Wis., as part of a general investigation of the zinc-producing area of southwestern Wisconsin. The work was done when every effort was being made to increase the production of metals important to the Nation's war program. The Bureau of Mines completed 24 churn-drill holes in an area immediately to the west of a mineralized section which had been mined through shallow workings for lead and zinc more than 40 years earlier.

Jan 1, 1948

By R. R. Brandenthaler

A series of open-flow tests was conducted in the Chickasha gas field, Grady County, Oklahoma, during June, 1927, under the direction of the U. S. Bureau of Mines and at the request of the Oklahoma Corporation Commission. The purpose of these teats was to determine whether or not any differences existed in the open-flow volume of a gas well when taken through well-head nipples of different diameters, and further, to establish if possible a relationship between open-flow volumes taken through well-head nipples of various diameters. The open flow of a well is the volume or quantity of gas, measured under standard conditions, that a well will produce when open to the atmosphere. There are several methods used for determining the open flow of wells; some of the methods are more suitable under certain conditions than others. The Pitot tube method is the simplest, is applicable to almost any condition, and is the one most commonly used. In the tests described in this paper no attempt was made to compare the Pitot tube method with the minute pressure measurement method or the orifice measurement method.5

Jan 1, 1928

By Blair Burwell

This paper describing the method of mining a deposit of vanadium ore near Rifle, Colo., is one of a series of similar papers on metal-mining methods and costs being issued by the United States Bureau of Mines. This vanadium deposit probably is the largest yet found in North America. It is situated 12 miles northeast of Rifle, Colo. (see fig. 1), on the southern flank of tae White River plateau, and is at an altitude of 6,500 feet. Between 150 and 200 tons of ore are mined daily and trucked to the mill at Rifle. The product of the mill is fined vanadium oxide, which is shipped to the company's plaits at Columbiana, Ohio, and Niagara Falls, N. Y., for the electric manufacture of ferrovanadium. HISTORY The deposit was discovered about 1909 by men prospecting for carnotite. Its outcrop on the bola cliff of Rifle Canon had been known to stockmen for many years.

Jan 1, 1932

By W. D. Ryan

The American public has at all times been prone to discuss important questions that call for consideration and adjustment. Debatable subjects upon which sides may be taken always receive unusual prominence, but other questions equally important may be neglected. The real "paramount issue," calling for remedial action, is the ever-increasing number of deaths caused by preventable accidents. This matter demands the attention of the entire American people; the importance of accident prevention can not be overemphasized, and in many phases of American life, especially among the mining and allied industries, far too little real attention has been given the importance of conserving life and limb by accident prevention. ACCIDENTS COMPARED TO WAR AS A CAUSE OF DEATH Harry T. Hoffman, Wyoming labor commissioner, writes the following: It is one of the peculiar complexes of this rapidly moving age that we all stand aghast at the horrors of war and view with appar- ent indifference the greater havoc of industrial peace. Did you ever stop to think that approximately twice as many people were killed by accidents in the United States in 1929, as there were American soldiers killed in the entire period of the World War? Every employer and every worker should be thoroughly aroused over the tremendous toll levied against industrial forces by accidents which are largely preventable and develop a faith in safety efforts that will fire them with a zeal as pronounced as that of their religion or their patriotism. Let us remember safety-first to the end that the workman shall live to enjoy the fruits of his labor; that his mother shall have the comfort of his arm in her age; that his wife shall not be untimely a widow; that his children shall have a father; that crip- ples and helpless wrecks who were strong men shall no longer be a by-product of industry.

Apr 1, 1931

By Van E. Shaw

Fusion of an 86-percent euxenite concentrate with ammonium sulfate was investigated by the Bureau of Mines. Reaction for 4 hours at 400° C results in conversion of both the rare-earth elements and the titanium-columbium components to water-soluble compounds. Similar results are obtained with ammonium bisulfate. Stirring the fusion mass decreases the reaction time substantially. Alternatively, treating the fusion product with a 3-hour, 650° C calcining step renders the non-rare-earth constituents insoluble, thereby allowing selective leaching of a pure rare-earth fraction with an overall yield of 97 percent.

Jan 1, 1967

By David F. Smith

The American Society for Testing Materials4 has recommended that the melting temperature of potassium chromate be used-for indicating the temperature to which a coal sample should be heated in the standard method of analysis to determine its volatile matter content. The specified temperature is 950± 20° C., the melting point of potassium chromate being noted as 940° C. Le Chatelier5 originally found the melting point to be 975°; later6 he found 9400. According to Shemtschushny7 the melting point is 984°; he also found a transition at 679°. Groschuff8 found the melting point to be 971° and the transition temperature 679°. Amadori9 reports a melting point of 9.78° and a transition point of 666°. The International Critical Tables10 take the melting point as 975°, which is estimated to be correct to two significant figures. In view of the apparent uncertainty existing, it has been though worthwhile to make a careful redetermination of this datum. It is of interest not only to determine the melting point of the pure salt, but also of the commercial product, in order to test its suitability for use as a temperature indicator. The work was suggested by A. C. Fieldner, chief engineer, experiment stations division, U. S. Bureau of Mines.

Jan 1, 1929

By Richard L. Rains

The 15,770-acre Worm Creek Roadless Study Area is in southeastern Idaho about 8 miles (mi) west of the northern portion of Bear Lake. U.S. Bureau of Mines personnel examined the roadless, area during the summer of 1984. No mineral resources were identified within the study area. There were no mines or mining claims in the study area in 1984. However, the study area is blanketed with oil and gas leases, but no known productive horizons have been identified within nor nearby. The roadless area is in the Cordilleran fold-thrust belt and is underlain by Paleozoic and Mesozoic marine strata more than 50,000 feet thick. The trace of the Paris thrust fault is 2 to 3 mi east of the study area and has an eastward displacement of about 4 to 7 mi.

Jan 1, 1985

By Steven E. Mischler

The exposure of mine workers to diesel particulate matter (DPM) and gases is an issue of great concern to the underground mining community in the United States. Approximately 30,000 underground miners are potentially exposed to high concentrations of DPM. In January of 2001, the U.S. Mine Safety and Health Administration (MSHA) promulgated rules setting compliance standards for both underground coal and metal / nonmetal mine workers. As industry works to achieve compliance with these standards, mine operators are looking for feasible methods for reducing DPM concentrations in their mines. In addition, the industry needs methods to accurately measure DPM to ensure that the control strategies they adopt are working successfully. The Pittsburgh Research Laboratory (PRL) of the National Institute for Occupational Safety and Health (NIOSH) conducts research to evaluate control technologies and monitoring instrumentation that can be used to reduce the diesel particulate matter (DPM) exposure of mine workers. An overview of the strategies being utilized in underground US mines to reduce DPM concentrations will be presented. Also, updates on the development of diesel monitoring instruments such as the continuous elemental carbon monitor or the Personal Dust Monitor for DPM measurement will be provided.

Jan 1, 2010

By J. M. Harrington, C. W. Owings

"The transportation of explosives, and especially their distribution from the supply magazines of the manufacturers or dealers to the mines, quarries, or other points where they are to be used, by means of horse-drawn vehicles is an old-time practice, and the records of accidents of the past show this to have been a hazardous undertaking requiring for safety the taking of many precautions not required in the transportation of other merchandise.Displacement of the horse-drawn vehicle by the motor vehicle for the transportation of explosives is increasing rapidly. A consideration of the facts that the vehicle is operated by an explosion engine, using easily vaporized liquid fuel; that the charges in the engine are fired and the vehicle lighted by electricity; and that the vehicle, being operated insulated from the ground, may accumulate static charges led to the conclusion that new hazards are being introduced into the transportation of explosives through the use of motor-operate& vehicles, and that therefore additional special precautions must be taken against these additional hazards.That accidents have already occurred in this use of motor-vehicle transportation is evidenced from the following examples:Recently in California a driver loaded a box of granular powder in the rear of an automobile truck and a box of electric detonators in the front. Suddenly, while traveling along a highway, the explosives detonated, demolished the truck, and blew the body of the driver into small pieces. No evidence was left to show the cause of the explosion, but it is assumed that a jar or other means caused the detonators to fire, and that they in turn detonated the explosive. It should be recognized that it is unsafe to transport detonators and explosives in the same compartment, and this rule should be strictly enforced. At present this rule appears to be either unknown or, at least, frequently ignored.There are usually so many possible causes of ignition or detonation of a truck load of explosives that it is often impossible to state definitely the exact cause in a given case. This is well illustrated in the following account of an accident: A trucking company was hired to haul a truck load of explosives about 200 miles. The driver had had experience in driving trucks of explosives, and it was stated that he inspected the truck carefully before leaving the garage. Eighty 50-pound boxes of explosive were placed in tiers on each side of the truck and 265 25-pound kegs of black blasting powder were placed in the center of the truck. The boxes were placed flat and the kegs were placed on end, arranged in tiers. While the truck was being driven along the highway there was a muffled explosion. When some men, who were about a quarter of a mile away, arrived at the scene the truck was in flames and they could get no nearer than 100 feet. The driver was sitting in his seat and had apparently been killed instantly either by shock or fumes. When the flames were finally quenched, the driver's body was recovered, badly charred. It was, found that several boxes of explosives had been thrown about 40 feet by the initial explosion but were uninjured. A total of half a ton of dynamite was recovered. The cover to the gasoline tank could not be found."

Aug 1, 1930

By S. R. B. Cooke, J. Bruce Clemmer, Will H. Cognill, F. D. DeVaney

"INTRODUCTION The domestic production of potash has made rapid strides in the past 4 years. In 1929 the United States produced 109,820 tons of potash-bearing material, equivalent to 61,590 tons of pure potash (K20). In 1933 to this had increased to 331,110 tons, containing 143,378 tons of potash, due chiefly to the development of the potash deposits near Carlsbad, N. Mex. The potash ores of that district occur at a depth of about 1,000 feet and as mined consist of a mixture known as sylvinite containing about 40 parts of sylvite (KC1) and 60 parts of halite (NaCl). By careful mining the extraneous material does not amount to more than 2 or 3 per cent. Such ore was used in the experimental work here reported.The usual chemical method for the recovery of potash from sylvinite, while efficient in the production of pure potassium chloride, requires,expensive equipment and is costly to operate. It occurred to the Bureau of Mines that ore-dressing methods, which have been applied to other nonmetallic minerals, might be adapted for the production of a grade of potash suitable for the fertilizer industry. After preliminary study by the Bureau of Mines showed that ore-dressing treatment was possible the investigation was extended under a cooperative agreement between the U.S. Bureau of Mines, the Potash Company of America, and the Missouri School of Mines and Metallurgy, Rolla, Mo.ACKNOWLEDGMENTSAcknowledgment is here given for valuable assistance in the laboratory of R. G. O'Meara, assistant metallurgist. U.S. Bureau of Mines, Tuscaloosa, Ala. who was on detail at the Rolla station during the early work; by E. W. Gieseke and Albert Ollar, temporarily employed by the Potash Company of America; and to N. H. Lenz, an engineer temporarily assigned to the station."

Feb 1, 1935

By A. M. Cummings

During August 1943, the Bureau of Mines undertook sampling and measuring of the Kennedy zinc tailing pile near Hazel Green, Lafayette County, south-western Wisconsin, as part of a general investigation of this lead-and zinc-producing area at a time when it was extremely important to increase the production of metals for the Nation's War program. The tailing pile was the residue from old jigging plants that treated ore from the Kennedy mine, one of the oldest and. largest mines in the district. Because retreatment of tailing by modern milling methods was proving economically successful at other sites in the southwestern Wisconsin field, the Bureau?s investigation was designed to assist the potential operators in evaluating the feasibility of a retreatment operation at this site. The study involved measurement of the tailing pile and sampling by means of auger to determine the average metal content within the narrowest possible limits. A total of 46 auger holes ranging in depths up to 40 feet and aggregating 886.5 feet of bore were drilled in the tailing pile, and weighted samples from each hole were analyzed and averaged to determine the zinc and iron content of the tailing.

Jan 1, 1949

By H. H. Schrenk

The Bureau of Mines midget impinger dust-sampling apparatus was described first in 1937.4/ Two supplementary reports5/6 were published in 1938. These reports are now out of print. The material published previously is combined in this paper to make information on this device available for distribution. The impinger was developed by the Bureau of Mines in cooperation with the United States Public Health Service in 1922. The underlying principle of this instruments is based on impingement land wetting, of the dust particles by drawing air through a nozzle at high velocity onto a smooth surface under a bubbling column of liquid. The dust particles are retained in the liquid. The apparatus has been used widely and permissible limits of dustiness have teen established in the United States on the basis of results obtained with this device in correlation with medical studies. However, it has been criticized for its bulk, weight, and power requirements.

Jan 1, 1939

By E. D. Gardner

About 300 tons of gold ore per week was being produced in February 1934 by Thomas D, Herron and Con Laster from the old lake Superior and Arizona workings; the ground was leased from the Magma Copper Co. The workings adjoined but were not a part of the Magma mine. The lessees had been employees of the Magma Copper Co, at the time the Magma closed down for the summer of 1932. Work on the lease began in July 1932 on an exposure of $2-per-ton ore disclosed in a drift; after a few hand-drilled rounds were blasted the gold content increased to about $30 per ton. Extensive sampling by pannings elsewhere of exposed portions of the vein indicated that other ore shoots existed. The last work previously done in the mine was during the World War, when lessees mined a number of small shoots of copper ore. In some of the stapes the copper miners had left a quartzose streak on the hanging wall that carried $15 per ton of gold. This material did not look as if it cried values and evidently never had been sampled. The first shipment of gold ore was made on September 28, 1932. Up to April 1, 1933, 3,778 tons had been shipped and from September 1, 1933, to January 31, 1934, 3,125 tons.

Jan 1, 1934

By V. F. Parry

Under the present emergency every consumer should store as much coal as he can. Although there is no shortage of coal, there is likely to be a shortage of labor to mine excessive quantities in the fall, and railroads cannot be expected to deliver coal promptly on account of the need for transporting war materials. Some miners must join the armed forces, and those who are left may be unable to mine coal as rapidly as you will need it when winter comes. When the first cold days arrive, there may be a shortage of trucks to deliver coal. Deliveries may be planned in advance, and your turn might not come until it is too late.

Jan 1, 1942

By Lon Santis, Scott Deitchman, John A. Decker

This report describes three cases of carbon monoxide (CO) poisoning in a manhole, including one fatality, from CO migrating through soil after nearby use of explosives. A municipal sewer project involved installation of new pipes and manholes. Work of the general construction contractor was interrupted when a subcontractor detonated 265 pounds of nitroglycerin-based explosive 40-60 feet south of the manhole to break up underlying rock. A construction worker who descended into the manhole 45 minutes after the explosion collapsed within minutes, and two co-workers descended into the manhole to rescue him. One rescuer retrieved the unconscious worker, and the other rescuer died in the manhole. All workers had elevated carboxyhemoglobin levels. In the subsequent NIOSH investigation, air monitoring was conducted with real-time instruments, and air samples were collected in Tedlar bags. Laboratory analyses of the bag samples collected near the bottom showed 1905 parts per million (ppm) CO, 19.5% oxygen, and 3% carbon dioxide. Direct reading instruments showed progressively higher concentrations as the sensor was lowered into the manhole. Subsequent chamber tests on sample explosive yielded 27 liters CO per kilogram detonated. Based on this value, the surface blast at the construction site may have produced about 3,250 liters (114.8 cubic feet) CO. The CO in this incident most likely was released from the nearby explosion and migrated through soil and fractured rock into the manhole. The blasting and construction industries should be made aware of this previously unrecognized CO exposure hazard associated with surface blasting. The extent of CO exposure from explosives used in construction is not known, and additional information on the extent of CO exposure must be collected. In addition, confined space entry procedures (including monitoring confined space atmospheres before entry) should be observed; CO monitoring of confined spaces in the presence of blasting can prevent future incidents such as this one.

Oct 30, 1997

By Marie Farnsworth

"The Anhydrite ProblemThe Nonmetallic Minerals Experiment station of the Bureau of Mines at Rutgers University, New Brunswick, N. J. has recently undertaken a study of the chemical and physical properties of anhydrite having in view its wider utilization anhydrite (CaSO4) in contact with water at ordinary temperature and pressure rehydrates, slowly forming gypsum (CaSO4.2H42O). In nature this is an extremely slow process, and laboratory experiments are being conducted to determine methods of accelerating the rehydration. The tests recorded herein cover one this study, and while they are negative in character in so far as the major problem is concerned, certain facts established by the tests, bearing on the stability relations of gypsum and anhydrite seem sufficiently important to be placed on record.Early Researches on Gypsum and Anhydrite.It is to Lavoisiar that we are the first scientific study of the calculation and hardening of plaster of Paris. He sums up his experiments in the following passage: ""If gypsum, which has been deprived of its water of by means of heat, is again treated with water (to make what is commonly called mortar) it takes it up with avidity, rapid and irregular crystallization occurs, and the small crystals which are formed are so entangled in each other that a very hard mass results."" Later, he observed that the dehydration of gypsum occurs in two stages: three-fourths of the combined water is much more easily driven out than the last fourth. LeChatalier first determined the temperature decomposition accurately, his method was as follows: Pulverized gypsum was placed in a glass tube in the middle of a paraffin bath, the temperature of which was raised in a progressive and regular manner. A thermometer gave at each instant the temperature the salt, and the passage of the mercury column past each division of —co. was cared by a registering chronograph. The rise in temperature was except at 128°C. and 168°C. where breaks occurred."

Nov 1, 1924

By G. R. Hopkins

"A new record in fuel efficiency at petroleum refineries was achieved in 1935, when an average of only 615,000 B. t. u. was needed to refine a barrel of crude oil, compared with an average of 638,000 B. t. u. in 1934 and 829,000 B. t. u. In 1925. (See fig. 1.)Refiners have made almost uninterrupted progress in firing efficiency during the last decade although much of this gain was brought about by improved technique and greater use of heat exchangers and pipe stills, the determining factor was the trend in crude runs to stills. Most plants can increase their crude throughput materially with but small increase in fuel consumption. Consequently, in years in which crude runs have increased substantially, average requirements have declined; but in years in which crude runs have decreased, the average has tended upward. This conclusion is confirmed by figure 1, which shows that there has been but one minor exception to this rule in the last 10 years.Technical progress in fuel efficiency may be illustrated by comparing crude runs and total B. t, u. consumed. Between 1925 and 1935 crude runs to stills increased 31 percent, but the total quantity of heat required did not increase; in fact, it declined slightly.The trend of modern still construction is from shell stills, in which a large body of oil is heated, to tube stills, in which the heat comes into much closer contact with the oil. In 1935 the total capacity of operating pipe stills increased about 4 percent; this increase, though small, probably was related to the gain in average efficiency.The Increased use of heat exchangers and their role as fuel savers have been discussed in previous reports of this series. It is sufficient to say that refiners with insufficient exchange capacity added as much in 1935 as their budgets would permit."

Jan 1, 1937

By C. C. Merrill

Columbium, tantalum, titanium, and zirconium are present in solid waste products generated by the chlorination of rutile used for production of titanium tetrachloride (TiC14). The columbium and tantalum were separated from titanium and zirconium by liquid-liquid extraction techniques using a secondary amine. Salts of these elements are in a leach liquor produced by water leaching of mineral waste from the chlorination of rutile. This waste, produced at the rate of approximately 50,000 tons per year, is about 40 wt pct water soluble. Leach liquors, separated by filtration, were further separated into a solid fraction and a liquid fraction by pressure hydrolysis, The solid fraction containing Cb, Ta, Ti, and Zr was dissolved in HC1-HF and used as a feed solution. Columbium and tantalum were removed from the organic extractant with 1 [N] HC1. A miniature 10-stage reactor showed that the columbium and tantalum present in solution could be separated with a continuous flow.

Jan 1, 1972

By E. D. Gardner

"A fire hazard exists in nearly all mines. Progressive mining companies recognize this danger and take all possible precautions to prevent any conflagrations, but in spite of such safety measures, mine fires do occasionally occur and endanger life and property. In order to be prepared for such an emergency, miners are trained in the use of self-contained breathing apparatus and the necessary fire-fighting equipment is kept on hand. Men trained to wear breathing apparatus can penetrate workings full of poisonous fumes, but in order to successfully combat fumes or to rescue miners, the rescue crews must be trained in fire-fighting operations and know how to proceed with a minimum loss of time when they get to the scene of action.In order to perfect fire-fighting plans and to train men of the Globe-Miami district under conditions approximating those found at an actual mine fire, mine-reseue maneuvers were held at Globe, Arizona, on October 17-20, inclusive. The work was done under the direction of Orr Woodburn, director, and his associates of the Globe-Miami District Mine Rescue and First Aid Association. He was assisted by Albert Tallon, safety engineer, and Herbert Finnegan of the Old Dominion Co.; Herbert Hodson, safety engineer for the Inspiration Consolidated Copper Co.; A. 3. Martinson and J. M. Harrington of Car One, and F. D. Gardner of the Southwest Station, Bureau of Mines. Invitations were issued to mining men likely to be interested and representatives of mining companies from other districts were present and observed the work.The Globe-Miami District Mine Rescue and First Aid Association is maintained by the mining companies in the district and each company contributes to the organization's support in proportion to the total number of men on the pay roll. A central station*, between Globe and Miami, has been established and a truck with 10 sets of 2-hour self-contained breathing apparatus and the necessary accessories is always in readiness to respond to a call to any of the mines in the district. Besides being in readiness for emergency work, the station employees train men in the use of mine-rescue apparatus and in first-aid to the injured at the mines of the association. The Globe-Miami Mine Rescue organization has been developed to high point of, efficiency under Mr. Woodburn's direction and is one of the best in the country. The three largest mines of the district such maintain a crew of 15 men trained in the use of breathing apparatus, and other mines keep crews of 5 men each."

May 1, 1923

By P. M. Gruzensky

In view of some of the outstanding properties of chromium, considerable effort has been made in recent years to prepare the high-purity metal in ductile form. The object of this investigation was to obtain such metal by electrolysis of chromic acid solutions and to determine the conditions that yield optimum results. The apparatus is described, as well as the parameters that received consideration. Ion-exchange resins were employed to remove cation impurities from the electrolyte. Tensile specimens prepared from the electrodeposits by arc melting, press forging, swaging, and drawing, were ductile at room temperature. INTRODUCTION Metallic chromium displays an exceptionally high resistance to corrosion, oxidation, and wear at elevated temperatures. Although these properties are utilized to some extent when chromium is alloyed with other metals, such as in stainless steels, high-chromium alloys and pure chromium are not employed as engineering materials because of a serious lack of ductility and impact resistance at room temperature. Because high-chromium alloys appear promising as refractory metals for applications such as in gas turbines, much interest has been shown recently in the preparation of uniformly ductile chromium and in determining which factors contribute to its brittleness.

Jan 1, 1957