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By J. W. Walkiewicz

One of the objectives of the Bureau of Mines is to develop substitution technology for scarce materials. In accordance with this goal, alloys containing lanthanum, cobalt, copper, and magnesium were investigated for fabrication of rare-earth-cobalt (RE-Co) permanent magnets. A complete substitution of lanthanum for samarium and a partial substitution of copper for cobalt was accomplished. Magnets of La-Co and La-Co-Cu-Mg alloys were fabricated by powder metallurgy techniques and evaluated. A maximum intrinsic coercivity of 23.2 kOe was obtained with a La-Co-Cu-Mg alloy. In comparison, maximum values of 9.3 kOe and 11.6 kOe were obtained with La-Co and La-Co-Cu alloys, respectively. The substitution of copper and magnesium for part of the cobalt resulted in a large increase of intrinsic coercivity, similar to the results of Bureau research with mischmetal-Co-Cu-Mg alloys. Unlike the mischmetal-Co-Cu-Mg magnets, the La-Co-Cu-Mg magnets showed signs of physical deterioration on exposure to air. The effects of fabrication parameters on the magnetic properties of the La-Co-Cu-Mg alloys were also determined.

Jan 1, 1982

By John C. Edwards

Several experimental programs were conducted at the Pittsburgh Research Center to investigate the level of mine fire detection and alarm capability possible using state-of-the-art technology. These programs involved comparison of the response and alarm time of optical and ionization type smoke sensors to smoldering and flaming coal combustion in a smoke chamber. Coal combustion experiments conducted in the smoke chamber demonstrated that a CO concentration of 5 ppm above ambient corresponded to an optical density of 0.022m1. For the four smoke sensors for which a continuous analog signal was available, a smoke sensor alarm was defined as the average background signal plus ten times the peak-to-peak noise. This alarm criterion resulted in the association of the alarm for three of the four sensors with a smoke optical density of 0.022m-1. and 0.033m-1 for the fourth smoke sensor. The smoke sensors used in the smoke chamber studies were incorporated into large scale diesel fuel fire experiments conducted under normal ventilation conditions in the Safety Research Coal Mine (SRCM) at the Pittsburgh Research Center. These experiments showed that a diffusion mode smoke sensor alarmed earlier than a diffusion mode CO sensor; and, based upon the measurement of the optical transmission at the location of a pump mode ionization type smoke sensor that a pump mode ionization smoke sensor alarmed at an average smoke optical density of 0.021m" for the twelve experiments conducted. A series of 30 and 330 kW diesel fuel fire intensity experiments were conducted under zero airflow conditions in the SRCM. It was determined that :(I) thermal sensors are inadequate at 30 m from a 300 kW fire;(2) a diffusion mode ionization smoke sensor can be more effective for mine fire detection than a diffusion mode CO sensor;(3) recommendations can be made for sensor spacing in a mine entry based upon the measured CO buoyancy induced spread rates along the mine roof and the time for a developing coal fire to ignite a conveyor belt.

By C. C. Shale

A semicommercia1, high-temperature electrostatic precipitator and adjunct equipment are described, and operating characteristics at 1,470° F and 80 psig are presented for both positive and negative polarity. Removal efficiency for negative corona waS about 91 to 96 percent while that for positive corona was only about 75 to 77 percent. Results are compared with those from bench-scale investigations, and equipment limitations are discussed. Theoretical aspects of the precipitation process are related to the operating characteristics.

Jan 1, 1969

By S. D. Hudock, C. M. Keran

A review of all upper extremity cumulative trauma disorder (UECTD) injuries was conducted by the U.S. Bureau of Mines for 1985 through 1989. This review was performed by analyzing each injury, as reported by law and maintained on the U.S. Mine Safety and Health Administration's accident data base. This analysis found that incidence rates in mining were lower than in private sector industry, although the number of reported UECTD injuries increased sevenfold and their percentage of all mining injuries increased fivefold from 1985 through 1989. Metal-nonmetal mines accounted for 80 pct of UECTD injuries, while coal mines accounted for 20 pct. Nearly 63 pct of UECTD injuries were accounted for by only four occupations-mechanics, laborers, boney (crusher) operators, and miners not elsewhere classified (NEC)-with an incidence rate well above the private sector industry rate.

Jan 1, 1992

By Staff

The papers contained herein summarize results of various recent Bureau of Mines investigations in the area of mine power distribution systems. They are based on information from Bureau personnel, contractors and grantees, and Mining Enforcement and Safety Administration. Conclusions drawn from a series of parameter measurements on mine power systems, taken over a 3-year span, are presented. Personnel and equipment hazards due to faults on isolated, solidly grounded, and resistance grounded three-phase systems are discussed. Two papers cover dc applications of circuit breakers, including a novel protection scheme for trolley lines. The methods of suppressing induced arcing currents and voltages in a-c machines are evaluated. An evaluation program for ground monitors is described. Acceptance test procedures and the importance of various paparameters for trailing cable splice are covered. A number of techniques for locating faults in trailing cables are described.

Jan 1, 1975

By Travis Rhoden

Merriam Webster?s Collegiate Dictio­nary (1996) defines team as ?a number of persons associated together in work or activity? and teamwork as ?work done by several associates with each doing a part, but all subordinating personal prominence to the efficiency of the whole? (page 1209). According to Dr. Geller, author of Building Successful Safety Teams: Together Everyone Achieves More (1998), a team of people working together for industrial safety consists of as few as two people or as many as fifteen who have complementary skills, assignments, or abilities for completing a particular task. Effective teams have members who share a common mission and relevant goals, and they share specific methods to reach their goals and accomplish their mission. They also have an evaluation system in place for holding themselves mutually accountable for goal-directed responsibilities.

Nov 1, 1998

The head loss data for coal slurries over a range of concentrations and velocities and the laboratory screen analysis were selected as areas for investigation in the data analysis performed. The analysis resulted in the following: (1) Size distributions for the coal used in the horizontal pipeline tests were fitted to the Rosin - Rammler distribution function. Each of the fits was significant. Corresponding Rosin - Rammler parameters were obtained which were introduced into the regression analysis. (2) A regression equation was obtained which predicts the slurry head loss of 1-inch by 0 coal slurries ranging in volumetric concentration from 20 to 40 percent and line velocities from 1 to 14 feet per second as a function of the square of velocity. The addition of the term for concentration in the regression equation did not contribute significantly c head loss.

Jan 1, 1972

By David A. Monaghan, Kenneth R. Maser, Adi R. Gurdar, D. Randolph Berry

APPENDIX C SCALING RELATIONSHIPS 1. Scaling Law for Fly Ash Crater Formation The scaling law derived for predicting crater diameters at different scales is developed below by considering the equation of motion of individual fly ash particles. It is assumed that the air drag on each particle is characterized by Stokes flow, and at the borehole - passage intersection the air velocity and the fly ash particle velocity are the same. The equations of motion for a fly ash particle are the following, (see Figure C-1).

Jan 1, 1973

By R. Barany

The heats of the glass-crystal transformation of nepheline (Na0.7794K0.2206AlSiO4) and wollastonite (CaSiO3) and the heat of formation of nepheline at 298.15° K were determined by solution calorimetry. For the glass-crystal transformations, the heat values were -9.0 ± 0.3 kcal/mole for nepheline and -8.1 ± 0.2 kcal/mole for wollastonite. The heat of formation of nepheline was -34.8 ± 0.6 kcal/mole from the oxides and -501.0 ± 0.5 kcal/mole from the elements.

Jan 1, 1966

By Andrew B. Cecala, Edward D. Thimons

The Bureau of Mines has successfully tested a method to simulate methane (CH~) flows from face areas through the returns of noncoal mines. This technique' involves releasing a small quantity of tracer gas at a working area and sampling for that gas downstream in the re- turn airways. By measuring the dilution of the tracer gas, the dilution of any volume of CH4 released at the face can be calculated. This information is useful in selecting locations for CH4 monitors and in deciding the necessity for permissible equipment in the returns.

Jan 1, 1984

By R. D. Leitch

From time to time the Bureau of Mines has received requests from persons who wish to destroy unwanted explosives, and although the information that follows has been accumulated from sources considered reliable,4/ the. Bureau of Mines assumes no responsibility for accidents that may result from following the suggestions offered. Explosives to be destroyed may be fresh material from damaged packages, usable material for which there is no further need, or material that has deteriorated either from natural aging or from improper storage to the point where it is unfit for use.

Jan 1, 1945

By Robert King

Splicing portable trailing cables used in underground coal mines is usually less expensive in terms of capital outlay and production time lost than replacing them. However, handling trailing cables may result in electrical arcs, shocks , and burns. Also, destructive forces encountered during a mining operation may shorten the effective life of a cable splice. This report gives the results of an analysis of cable splice defects in an effort to establish cable splice performance criteria, determine testing standards for cable splices, establish guidelines for training programs in cable splicing, and indicate areas for improvement.

Jan 1, 1975

By John M. Devine

The oxygen bomb-is used extensively for determining sulphur in petroleum, although it has been suspected that the results obtained with this method are somewhat lower than the true varies. In this paper are compared the results given by the oxygen-bomb and Carius methods, the latter being generally accepted as the standard procedure for the determination of sulphur in organic compounds. The Carius determinations given hero were made in connection with a special study of this method.4 Only petroleum oils of the less-volatile type are covered in the present work. Summary and Conclusions. When used with oils containing 2.3 to 0.15 per cent of sulphur the oxygen-bomb method gives results that are consistenly if slightly lower than those obtained with the Carius method. This variation, for the oils used, amounts to 3.1 per cent (on tae basis of sulphur present) for the sample containing 2.47 per cent of sulphur, and gradually increases (as the percentage of sulphur in the oils decreases) to 7.3 per cent for the oil containing 0.15 per cent of sulphur. With the oils studied the presence of ammonium nitrate in the bomb does not influence the results materially.

Jan 1, 1928

By A. E. Wells

"When the United States entered the World War, the heavy requirements for sulphuric acid in the manufacture of explosives made necessary a definite knowledge of the sulphuric acid capacity of the country. The Bureau of Mines, under the authority conferred by the explosives regulation act, made a thorough survey of the sulphuric acid situation. In this work, which was personally directed by the writer, comprehensive data were collected on the situation and capacities of the various acid plants, sources of supply of raw materials (brimstone, pyrite, pyrrohotite, zinc ores and concentrates, waste sulphur dioxide gases from copper smelting, and spent oxide from gas works), the principal points in regard to manufacturing processes (chamber and contact) and the uses of the acid. The results of this investigaion have recently been published by the Bureau of Mines, as Bulletin 184, entitled ""The Manufacture of Sulphuric Acid in the United States"" by A. E. Wells and D. E. Fogg. The following paragraphs on the uses of sulphuric acid are abstracted from this bulletin.Sulphuric acid is one of the most important of all chemicals, not only because of the large quantities manufactured but also because of the wide use of the acid in many different industrial works. Sulphuric acid is to the chemical industry what iron is to metallurgy. The general public, however, does not realize this fact, for sulphuric acid does not appear in the finished product as does iron and steel, but is only a means to an end. It is essential in many industries, such for example as in the manufacture of phosphate fertilizers, explosives, dyes and petroleum products. In recent years in the United States, especially in the East, the demand for sulphuric acid for chemical and metallurgical industries has been an accurate and sensitive barometer of the general business conditions. This demand for acid responds much more quickly to a general slump or boom in the industrial world than does the demand for iron and steel."

Oct 1, 1920

Develop a safe, nonpolluting power source for underground mining equipment. Approach The Bureau of Mines and EIM-CO Mining Machinery International entered into a cost-shared project to develop and demonstrate a novel power source for mining. An underground mining utility truck was equipped with an ultra-low-emission hydrogen-fueled engine and a safe, metal hydride fuel storage system. How It Works The nonpolluting hydrogen engine and a "solid-state" (metal hyride) hydrogen fuel storage system were combined to power a utility mining vehicle. An 85 horsepower diesel engine was convened to burn hydrogen. The engine was converted by equipping it with a spark ignition, lowering the compression ratio, turbocharging, and adding an ahercooler and a parallel fuel induction system. Parallel induction provides two intake paths, one for hydrogen and one for air. It avoids intake-manifold backfiring by keeping the hydrogen and air separate until they enter the cylinder.

Jan 1, 1986

By Rudolf E. Greuer, Linneas W. Laage, Xinton Chang

INPUT FORMAT INSTRUCTION FILE FOR PROGRAM MFIRE GENERAL RULES FOR DATA INPUT: $THERE IS NO NEED TO DISTINGUISH INTERGER AND REAL NUMBERS. $ $ SYMBOLS FOR NUMERICAL INPUT INCLUDE THE FOLLOWING $ $ 1234567890 -+BLANK $ $ * FREE FORMAT IS ALLOWED. COMMA AND BLANK SPACE CAN BOTH BE $ $ DELIMITERS. SEQUENTIALLY DISTRIBUTED BLANK SPACES ACT AS ONE $ $ DELIMITER. BLANKS ADJACENT TO A COMMA HAVE NO DELIMITING EFFECT $ $ * A ZERO INPUT CAN BE OMITTED BUT NOT THE DELIMITERS EXCEPT WHEN $ $ THE ZERO INPUTS ARE THE LAST ONES ON A LINE. $ $ * A LINE WHOSE FIRST NON-BLANK SYMBOL IS "$ IS AN INSTRUCTION $ $ LINE WHICH WILL BE IGNORED IN A PROGRAM RUN. $ $ * A LINE WHOSE FIRST NON-BLANK SYMBOL IS NEITHER ONE USED IN THE $ $ ABOVE LIST FOR NUMERICAL INPUT NOR "$, OR WHICH CONTAINS MORE $ $ THAN 3 SYMBOLS OUTSIDE OF THE LIST, IS A COMMENT LINE WHICH WILL $ $ BE SHOWN IN THE OUTPUT FILE. $

Jan 1, 1990

By M. M. Jones

A procedure for the spectrophotometric determination of uranium has been developed in support of minerals research being conducted by the Bureau of Mines. Uranium is separated from the sample by tributylphosphate extraction from acid solution containing added aluminum nitrate and (ethylene dinitrilo)-tetraacetic acid solutions. The colored uranium-dibenzoy1methane complex is developed in the organic phase by adding an ethanol solution of dibenzoylmethane buffered with triethanolamine. Absorbance is measured at 410 nanometers, and the response is linear up to at least 100 micrograms U30S in the aqueous aliquot taken for analysis. Aliquots containing as little as 8 micrograms U30S may be analyzed with relative errors no greater than ±5 percent. For aliquots containing at least 35 micrograms U308, relative standard deviation at the 95-percent confidence level is about ±2.2 percent. Appropriate procedures are given for analyzing a wide variety of samples.

Jan 1, 1980

Provide the National Park Service (NPS) with guidelines for closing abandoned mine openings such as shafts and adits. Approach The NPS needed alternative methods of closing a variety of abandoned mine openings on National Park lands. Because the U.S. Bureau of Mines (USBM) has a long history of mining-related experience, the NPS requested that the Bureau provide them with technical mine closure information. USBM engineers compiled information on various types of mine closures and prepared technical illustrations of those closure techniques. Multiple closure options, by type of opening, were prepared as one-page field guides to assist NPS field personnel in determining the most appropriate closure method for a given situation and detailing the construction of the closure method. Results Guidelines provided to the NPS included a description of the method, use applications, construction techniques, technical illustrations, and technical support information. The following provides a brief description of 11 mine closure techniques identified for use by NPS personnel. Most of the closure methods, except the backfill methods, allow for construction that can provide access to the mine. However, providing access makes the closure susceptible to vandalism. Most closure methods require periodic monitoring for subsidence and corrosion or deterioration of construction materials.

Jan 1, 1994

By B. W. Jong

The U.S. Bureau of Mines investigated anhydrous chlorination and caustic-acid leaching processes to recover Ni, Co, Mo, and W from waste hydroprocessing catalysts. In batch laboratory-scale equipment, the chlorination process extracted 61 to 99 pet of the metals. Final recovery was 65 to 99 pct. The caustic-acid leaching process extracted 81 to 98 pct of the metals. Final recovery was 36 to 99 pct. Chlorination processing included roasting, chlorination, hydrolysis of metal chlorides for recovering Mo or W, water leaching of Ni or Co from the spent charge, purification, and solvent extraction or precipitation of Ni or Co from the purified solutions. Caustic-acid leach processing included NaOH leaching, solvent extraction of Mo or W from the NaOH leach liquor, H2S04 leaching of the NaOH leach residue, purification, and solvent extraction or precipitation of Ni or Co from the purified solution. The estimated fixed capital cost for a commercial-scale plant processing 39,000 Ibid of waste Ni-Mo-AI catalyst was $8 million for the chlorination process and $9.6 million for the caustic-acid leaching process. The estimated operating cost was about $0.20 and $0.40 per pound of the waste catalyst, respectively, for the two processes.

Jan 1, 1989

By Charles L. Kimbell

For 1991, the aggregate value of world international export trade in mineral commodities was roughly estimated at $685 billion in current 1991 dollars. The estimated level was about 6 % higher than that for 1990, but still more than 3 % below the record high set in 1980, and the year was the fifth in a row in which the value of exported minerals advanced. Table 8 provides a data series for the estimated value of world export trade in all mineral commodities from 1979 through 1991, as well as a breakdown of this total into fuel and non fuel commodities. The data shown are based on the historically more traditional and realistic (from the viewpoint of data availability) practice of reporting trade values for the year before the year of review. Despite the considerable increase in the dollar value of mineral commodity exports, their share of total export merchandise trade declined to 19.1 % in 1990 from 19.7% in 1989. At 19.1 %, this share was very near the recent year record low of 19.0% reached in 1988. Comparable 1991 figures were not available in time for inclusion here, but it is expected that the mineral commodity share of the total will be little altered from that of 1990.

Jan 1, 1993