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By Arnaldo Forgas Júnior

Three techniques for ferrite quantification were applied in a duplex stainless steel UNS S31803 solution treated at three different temperatures, 1000, 1100 and 1200°C, in order to verify their compliance with the results from ThermoCalc® prediction. It is verified that only austenite and ferrite phases are present in the samples and that an increasing in solution treatment temperature led to the increase of the volume fraction of ferrite. It is also observed that quantitative stereology technique shows absolute values closer to ThermoCalc® predictions. On the other hand, measurements by ferritoscope and XRD show significant deviations, probably due to texturing effect imposed by the rolling process.

Aug 16, 2017

By Jose M. Rodriguez-Ibabe, Beatriz Pereda, Beatriz Lopez, Felipe Bastos

The modeling of austenite evolution during the hot rolling of steels is covered in the literature for a wide range of chemical compositions, although mainly for carbon contents below 0.20%. In addition, most research on this topic is oriented for processes that are characteristic of flat products. Compared to those processes, the hot rolling of bars for structural applications presents considerable particularities concerning mainly deformation, rolling speed and rolling temperature profile. Those particularities result in considerable changes on process parameters that affect the austenite microstructure evolution, both in the softening and hardening mechanisms if microalloying elements such as Nb is present. The aim of this work was to develop a model to predict the evolution of austenite microstructure that is suitable for the hot rolling of structural reinforcing bars. Different torsion tests simulating industrial schedules particular from those type of processes were performed. The tests showed the need to investigate Nb strain-induced precipitation interaction with softening mechanisms that can occur during the deformation schedule. At the end, the new proposed kinetics and routines were introduced to a program, MicroSim-Bars®, that is able to model austenite evolution under structural bar hot rolling conditions.

Oct 1, 2019

By Francisco Morganti

This report gives in the first part the metallurgical basics for the production of AHSS grades in integrated steel plants starting at the melt shop and ending at the annealing lines of the cold mill. The corresponding process and plant technologies in each production step with its specifics and rules are explained. In the second part by way of example the practical requirements for TRIP 780 steel grade are highlighted like a recipe for process control in the steel plant, hot and cold rolling mill, annealing line and finally skin pass mill. Measuring of mechanical technological properties on samples shows that the specifications according to DIN EN 10268 are fulfilled.

Oct 30, 2017

By Dagoberto Brandão Santos, Marcus Vinícius Pereira Arruda, Fernando de Souza Costa, Túlio Magno Fuzessy de Melo

The development of advanced high strength steels (AHSS) is motivated by the automotive industry demands for higher strength steels with better formability and stretch-flangeability to avoid fractures during parts forming. In response to this, the new steel grades must have special microstructures in terms of constitution, morphology, distribution and hardness, which are strongly dependent on the chemical composition of the steel sheet and its processing, especially in the continuous annealing stage, in the case of cold rolled sheets. In this study the influence of the annealing heating rate and intercritical temperature (IT) on the microstructural evolution and the final hole expansion ratio of a cold rolled 980 MPa AHSS grade was evaluated. The annealing process was simulated using a Dilatometer and a Gleeble machine, and the microstructures were characterized using scanning electron microscopy, electron backscattered diffraction (EBSD) and nanohardness measurements. The increase of heating rate resulted in an overlap between ferrite recrystallization and austenite formation, changing the austenite morphology from a random to a fibrous distribution, while a higher IT resulted in more homogeneous microstructures and higher hole expansion ratios. This microestructural homogeneity, confirmed by nanohardness measurements, suggested that the difference in hardness between ferrite and the second phase affects the micro-void formation and crack propagation during the hole expansion test.

Oct 1, 2019

By Douglas Glenn Stalheim

The uniformity of the final cross sectional microstructure and subsequent final mechanical properties and shape of structural steels is dependent on the type or types of recrystallization behaviors that are created. There are three main recrystallization behaviors that are the foundation of the metallurgy created during production. Alloy design and subsequent processing design strategy drive how much of each recrystallization behavior is created through the cross section of the product. Carbon manganese steels create only one basic behavior while the addition of microalloys, in particular niobium, can add two additional behaviors. The behaviors are intertwined with each other and build upon each other. The three behaviors are Type I, static recrystallization, Type II, no-recrystallization, and Type III, metadynamic/dynamic recrystallization. How much of each behavior is generated through the cross section through the production influences the final transformed microstructure and corresponding mechanical properties and shape performance. This paper will discuss the three behaviors, how they are generated, how to identify which behavior is occurring through modeling or actual mill data. Actual examples from production will be discussed.

Aug 16, 2017

By Wenting Zhu, Liqing Chen, Junjun Cui, Zhenye Chen

In this presentation, a low carbon high strength steel microalloyed with Nb and Ti was processed by thermo-mechanical controlled process (TMCP) containing two stages of controlled rolling. The austenite with various grain sizes was obtained by austenitizing this hot-rolled steel at different temperatures. And the effect of austenite grain size on bainitic transformation was investigated in a dilatometer to reveal microstructural change. The results showed that the microstructure of the hot-rolled steel was mainly composed of granular bainite, lath-like bainite, and martenite/austenite constituents (M-A constituents). With increasing the austenitizing temperature, or increasing the austenite grain size, the microstructure was changed from granular bainite to lath bainite. When the steel was reheated to a lower temperature of 860 ºC, a relatively higher start temperature (Bs) was measured for bainitic transformation. This was mainly caused by the formation of solute-depleted region in the austenite and the promotion of the granular bainitic nucleation. The highest reaction rate occurred at austenitizing temperature of 1000 ºC with fine grain size, while the coarse austenite grain can lead to a sharp increase in the amount of bainite. An analysis was made on the kinetics of bainite transformation which was controlled by the volume diffusion of C atom.

Oct 1, 2019

By Vitor Orlando Ferreira

The efficiency of an apparatus which uses a forced lubrication system, as well as the useful life of its components, is strongly related to the degree of contamination of lubricating oil. The presence of contaminants and the degradation of the oil itself cause it to release substances that fouling of the wall of the pipes. The cleaning and dialysis of the oil pipes, besides prolonging the life of the lubricant reduces wear of the components. There are several methods of cleaning in pipes, the problem is that some have abrasive characteristics, which could damage some types pipes. Among the non-abrasive methods stand the Flushing and Air scouring. Flushing uses the lubricating oil which circulates in temperatures alternating and high speeds, for generating turbulence to perform washing. The Air scouring method uses oil and filtered compressed air, injected into pipe, to generating higher flow, causing the power supply unit with fluid can work with lower power consumption and higher speeds, removing fouling of the pipe. The objective of this research is to evaluate the Reynolds number to correlate with the efficiency of cleaning the pipe. The method applied was the Air scouring and it was verified that the qualitative effects may occur when compared to Flushing. After testing, it was found that the chosen method brings significant changes in flow, and this flow regime varies considerably increasing the Reynolds number.

Jul 31, 2018

By José Adilson de Castro

In the integrated steel industries the sintering process plays an important role furnishing raw material to the blast furnace. In this work, a computational simulation of the sinter process is developed that is able to predict the most important phenomena within the sintering bed. The model is based on the multi phase concept with multiple components described by conservation equations of each component coupled with the momentum, chemical reactions and heat transfer. The model validation was carried out comparing the model predictions with averaged industrial data and local temperature measurements within the sinter strand. The model predictions presented good agreement with the averaged values measured on the industrial sinter process.

Aug 2, 2018

By Antonio Adel dos Santos, Carmos Antonio Gandra, Fabricio Mazola da Silva Paiva, Vicente Tadeu Lopes Buono

Abstract Usiminas Steel Plant in Ipatinga installed an accelerated cooling device named CLC (Continuous On-Line Control) in 2010, enabling it to supply steels produced by TMCP (Thermo Mechanical Control Process) technology. This technology complements the TMCR (Thermo Mechanical Control Rolling), with the inclusion of the accelerated cooling process after controlled rolling. There are various gains in terms of quality and productivity associated to the application of such technology. However, the flatness control for API steel becomes crucial because large thermal stresses may be generated due to thermal heterogeneity during the fast cooling when the austenite phase decomposes mostly into ferrite and bainite. In literature, there is lack of knowledge regarding a full understanding of the relation among cooling conditions and plate flatness. Therefore, this work has focused on the effect of the cooling strategy for API steels, aiming at optimizing flatness and keeping the mechanical properties within the specified ranges. The starting point was dilatometer simulation, where cooling conditions such as start cooling temperature, SCT, finish rolling temperature, FRT, and cooling rate, CR, were changed in order to evaluate their effect on microstructure. Those laboratory conditions supposed to give the best results were transposed to industrial scale, so as to produce experimental lots of plates with five different cooling strategies. It was shown the possibility to find a cooling profile that guarantees the balance between mechanical properties and flatness requirements. The influence of cooling strategy on flatness was explained by the varied heat transfer regimes occurring from hot steel surface to the ambient

Oct 1, 2019

By Antônio Aldenor Pinheiro Neto, Matheus de Lima Vieira

In mid-2015 the steel industry faced a strong crisis due to the weak performance of the Brazilian economy and the persistent entry of Chinese steel into Brazilian territory. This situation demanded that Brazilian steelmakers seek to develop products to meet new export markets. within the volume of exports possible are the rebars, where its applications are in the construction industry. One of the largest importers is Peru which has a large percentage of this export volume. This market demands as a priority requirement the surface quality of blue condition (low oxidation index) and mechanical properties normative.in order to meet the items required by the customer at a competitive cost, a vanadium microalloyed steel was applied to the hot rolling process without heat treatment after the last rolling pass. Where the great challenge was to achieve a high level of stretching without compromising the minimum limits of tensile strength. Assuming that the steel used is the correct one interventions were made on rolling parameters such as set-point temperature, residence time of pieces in the furnace, linear mass and rolling speed. All the changes made were based on statistical tools and practical tests. Finally, with the execution of actions generated from the statistical analyzes and tests it was possible to reduce process losses by 96%.

Oct 1, 2019

By Anna Carolina Cerqueira Neves

Synthetic fibers have been gradually replaced by lignocellulosic fibers. Compared to the synthetic fiber, natural fiber showed economic and environmental advantages presenting interfacial characteristics with polymer matrices that favor the impact energy absorption by the composite structure. However, so far little has been reported about the hemp fiber embedded in polymer matrices, such as tensile properties. This study aims to evaluate the resistance in tensile tests of epoxies composites reinforced with different percentages of hemp fiber. Tensile tests were submitted with percentage of 0%, 10%, 20% and 30% incorporated hemp fiber in epoxy matrix. The tensile strength and deformation substantially increased the relative amount of hemp fibers incorporated into the polymeric matrix.

Aug 16, 2017

By Davide Onesti

Electrode regulation is the technology at the heart of the AC and DC Electric Arc Furnace. As such, in the last decade it underwent continuous improvement to maximize the EAF performances, in terms of process efficiency, machine utilization and operator safety. Given this background, Danieli Automation’s efforts in the field of electrode regulation have been focused on fast response to scrap cave-in, compensation of supply variations, automatic resonance detection, transformer protection, dynamic regulation of the electrical and chemical set-points, coordination and control of slagging and foaming agents, arc irradiance supervision. An extensive analysis of operator utilization and feedback was also carried out to develop an innovative system HMI. In this field, the choice of the variables shown to the user is the key aspect to allow a prompt process evaluation by the operator, who can refer to a condensed set of useful data. This paper will describe the innovative features and embedded models of the electrode regulation module (Q-REG+) and the supervision HMI, together with the effects of their application on EAF process efficiency and system usability.

Oct 30, 2017

By Renata Cristina Teixeira

The lubricant oil is a complex mixture of different basestocks and additives. Engine oils evolved from the use of pure mineral basestocks back in the early years of automotive industry to the advent of synthetic, fully formulated, low ash lubricants. This evolution was driven by a number of factors, such as new engine designs, extended durability needs, increased fuel economy needs, environmental concerns, feedstock prices and availability and legal issues. This paper uses technology prospecting on literature and patents databases to allow an investigation on the historical evolution of engine oils. Main basestocks (mineral, hydrotreated, polyalphaolefins, esters) and additives (antioxidants, antiwear, friction modifiers, detergents and dispersants) are characterized according to their research effort. Technology prospecting data is crosschecked against the evolution of engine oil classes, allowing an analysis of how the main drivers push the development of lubricant oil quality. A research effort was identified in late 1990’s until mid-2000’s and related to the adoption of chemical limits for lubricants. Different patterns for the articles and patents publication account for the high value technological knowledge has in this industry. Technology prospecting is seen as a useful methodology for the understanding and forecast of lubricant technology movements.

Jul 31, 2018

By Samuel Filgueiras Rodrigues, Clodualdo Aranas Jr., Gedeon Silva Reis, Eden Santos Silva, Fulvio Siciliano

When austenite is deformed above the Ae3 temperature, partial amount of it transforms dynamically into ferrite by a displacive mechanism. After unloading, it retransforms back into the stable austenite by a diffusional process. This influences the rolling load which decreases under isothermal condition or does not increase with decreasing temperature as rapidly as expected under cooling. Plate rolling simulations under isothermal and continuous cooling conditions were carried out on a 0.09 wt.% Nb X-70 steel. Pass strains of 0.2 were employed together with interpass times of 10 s, and 30 s for the cooling conditions and 0.3 with interval of 10 s at 900 °C for the isothermal experiments; strain rate of 1 s-1 was used during the simulations. The mean-flow-stress (MFS`s) behavior of both conditions indicates that dynamic transformation and dynamic recrystallization were taking place during straining. The critical strains for the initiation of dynamic transformation fell around 0.06 while the critical strain for DRX was 0.12. It has been shown that ferrite is formed due to the applied deformation of roughing passes and increases its volume fraction throughout the finishing rolling stage. Under cooling conditions, the ferrite formation is also favored as the temperature approaches the Ae3 line. Such ferrite forms when the driving force for dynamic transformation is higher than the total free energy barrier preventing its formation. This obstacle consists of the free energy difference between austenite and ferrite as well as the lattice dilatation work and shear accommodation work. The addition of Nb retards the retransformation of the ferrite into austenite. Moreover, holding times after rolling increases the amount of austenite available for microstructure control on subsequent stages. The dynamic transformation (DT) mechanism can be used to design improved rolling schedules

Oct 1, 2019

By Armando Vazquez

Steel Dynamics Inc. (SDI) and Tenova Goodfellow Inc. (TGI) have successfully commissioned the first hybrid extractive/laser system for continuous and full spectrum analysis (CO, CO2, O2, H2 and H2O vapor) on two twin shell furnaces at Butler, Indiana. NextGen® technology using off-gas analysis as a main tool for EAF practice optimization is a proven effective method for improving plant productivity. Significant benefits attributed to the NextGen® system are operational cost reductions through the use of real-time dynamic control of chemical energy and improved environmental conditions through reduced GHG emissions. Additionally, the implementation of Tenova’s Water Leak Detection Technology® has shown results as an effective tool for operators to identify in real-time the presence of water during both reducing and oxidizing conditions. This paper will include project details, trials and results and will also outline the latest hardware developments and multipoint capabilities

Oct 30, 2017

By Antônio Augusto Gorni, Fabio Adriano da Silva, Emanuelle Garcia Reis, Afrânio Márcio Costa

Gerdau Ouro Branco´s plate mill started the operation in 2016 with high level technology. Stands out the capacity to produce different thicknesses in a same plate, therefore allowing special service for sectors such as building structures, bridges, shipbuilding and mechanical applications. The purpose of this study is to present the first results obtained in this innovative product in Brazil. Some slabs of EN10025-2 S355JR+AR steel were rolled and were evaluated the dimensional tolerances, mechanical properties uniformity, grain size, surface and internal qualities. In addition, a correlation was observed between slab and plate thickness reduction and internal plate quality. The results show that this technology can be used with adequate performance for these steel grades in the current market.

Oct 1, 2019

By Hongshuang Di, Tianyu Zhang, Huiqiang Huang

A CMnSiAl transformation induced plasticity (TRIP) steel was used to study the effect of retained austenite on room-temperature mechanical properties. The steel plates with retained austenite were obtained by hot rolling, cold rolling and subsequent continuous annealing. The starting and finishing temperature of hot rolling are between Ac1 and Ac3. Reduction ratio of cold rolling is 75%. The continuous annealing is carried out at different intercritical temperatures. The relationship between work hardening exponent and retained austenite was discussed. The results show that, the Ac1 and Ac3 were much high because of the alloy elements, and the temperature range between them was wide. Due to the high hot rolling temperature, the grains was hereditarily refined as a result of dynamic recrystallization. Annealing at intercritical temperature of 930 ºC, retained austenite with relatively high stability reached a maximum volume fraction of 25%, a maximum total elongation of 30.2% and a best ultimate tensile strength × total elongation of 20.1 GPa·%. Instantaneous work hardening exponent reflects strengthening mechanisms at different strain stages. The TRIP effect of retained austenite is the main mechanism during deformation. With retained austenite of sufficient amount and high stability, continuous work hardening was observed in the tensile specimen of 930 ºC.

Oct 1, 2019

By Xihuai Gong, Hongshuang Di, Jianping Li, Ning Yan

In this work, we investigated the effect of the rolling process (warm-rolled or cold-rolled) on microstructure evolution and mechanical properties of 9Mn steel. After intercritical annealing at 670°C for 10min, both cold-rolled and warm-rolled microstructures are composed of ultra-fined austenite and intercritical ferrite. The austenite in warm-rolled sample includes two types of morphology, namely equiaxed and lamellar, which exhibits a wide distribution of grain-size. The incomplete recrystallization or recovery behavior of ferrite in warm-rolled and annealed sample results in higher yield strength and shorter yield point elongation. Moreover, the warm-rolled and annealed sample extends the TRIP-related work hardening over a broad strain range, resulting in a better combination of ultimate tensile strength and total elongation.

Oct 1, 2019

By Rodrigo Ribeiro de Andrade, Túlio César Nogueira, Ed Juarez Mendes Taiss, Nilton José Lucinda de Oliveira

The objective of this study was to determine the effects of an eventual slab central macro-segregation in microalloyed steels with low Mn content (0.80%) and high Nb content (0.08 to 0.10%) on the kinetics of recrystallization of austenite during its rolling, on its critical temperatures, that is, of non-recrystallization (Tnr), start Ar3 and finish Ar1 of ferrite transformation and its response to a simulated industrial thermomechanical processing. The determination of the austenite recrystallization kinetics was made through isothermal double compression tests using a dilatometer, while the critical temperatures were determined through hot torsion tests in a Gleeble® 3800. It was found that austenite recrystallization kinetics, Ar3 and Ar1 temperatures did not present significant changes for the samples extracted both at ¼ of the thickness and at the core of the plate, indicating that, as expected, the central segregation in this type of steel was not intense to the point of affecting this phenomenon. The Tnr values determined for the samples extracted in the core of the plate were, on average, 30°C lower than those obtained from specimens extracted at ¼ thickness, which suggests that a significant portion of the carbonitrides present in the core of the slab are eutectic and coarse, not having completely dissolved during the reheating of the specimens. This occurred despite the fact that the austenitization temperature adopted in this treatment theoretically leads to the total dissolution of Nb, as seems to have occurred in the case of specimens extracted at ¼ of thickness, where carbonitrides have a finer size.

Oct 1, 2019

By Edmar de Souza Silva, Antonio Augusto Gorni, Emanuelle Garcia Reis, Daniel Bojikian Matsubara

Controlled rolling followed by accelerated cooling, known worldwide as TMCP, aims to increase mechanical properties without toughness deterioration. The process principle is to promote the plate cooling with water jets along the range of the austenite transformation temperatures. The accelerated cooling process is only fully effective when controlled in an integrated manner, as it alone cannot ensure significant improvements in the final properties of steels. Plate surface quality depends on some parameters that must be controlled before the start of the plate accelerated cooling. Good flatness is essential to avoid irregular water accumulations during cooling. After the reheating process, the slab should have uniform temperature, uniform austenitic grain size and easily removable scale. The slab thermal and microstructural heterogeneities are inherited by the rolled plate and tend to increase further during the accelerated cooling. This results in flatness problems, high level of internal stresses and mechanical property variations. The descaling strategy is an extremely important factor and must be determined with great caution. It is important that scale thickness and distribution is uniform to ensure homogeneous cooling over the entire plate surface. Otherwise, there will be an uneven temperature distribution, which can cause serious problems of flatness, surface quality and mechanical properties.

Oct 1, 2019