Search Documents

By Fábio Dian Murari, Antônio Adel dos Santos

The effect of reheating temperature of slabs on the precipitates dissolution and mechanical properties of Ti-Nb microalloyed steel was investigated in pilot scale. It was verified, by means of transmission electron microscopy, a significant decrease in precipitates formed during the solidification of the steel as the reheating temperature increased from 1100°C to 1200°C. No significant changes in size and shape of the precipitates were observed with further temperature increase up to 1280°C. In line with the precipitates dissolution behavior, an increase in strength was observed with the elevation of the reheating temperature up to 1200°C, due in part to the reprecipitation of fine Nb-rich precipitates during the hot rolling. At 1200°C the presence of deformed ferrite on the microstructure contributed to the additional increase in strength. After reheating above 1200°C up to 1280°C, a decrease in strength of the rolled plates was noticed. This effect has been credited to the absence of deformed ferrite grains and also to a small increase in the low angle grain boundaries size. The results were in agreement with Thermo-Calc and Dictra simulations.

Oct 1, 2019

By Edo Engel

Whereas only a handful of decades ago, typical blast furnace working volumes were below 1000 m³, such furnaces are currently designated compact or even mini blast furnaces. For certain business cases, however, small furnace sizes remain an attractive option. Decades ago, this size blast furnace would have produced a maximum of 0.3 Mtpa with its 600 m³ working volume over a campaign of up to four years. The current state of technology and operational know–how will allow a similarly sized furnace to produce over 0.7 Mtpa while achieving the multiple decade campaigns that have become familiar to steel producers in full sized operations. This level of productivity, but especially the reliability and supply security associated with mature technology, allows for integration into minimills or taking a first step towards a full scale BF–BOF integrated mill. Steel producers considering such scenarios, which are typically attractive for emerging economies, are confronted with fundamental decisions, one of which is for the technological basis for the compact or mini blast furnace to be included in the plant. This article addresses some of these decisions from an operations–based perspective. A small number of case studies is included.

Aug 16, 2017

By Joachiim Lehner

The application of post-combustion (secondary oxygen) to avoid skull formation on BOF lances was tested in industrial trials. The main findings are that no negative impact on the metallurgical targets (i.e. carbon, temperature and phosphorus at end of blow as well as iron–oxide in the slag) could be observed. The technology is capable of avoiding the buildup of lance skull and consequently increasing the average life of lance tips. The application of post-combustion not only affects the skull formation, there are also interactions with the refractory lining, especially thermal wear, and the utilization of the process gases (CO Recovery) that have to be considered. Special attention has to be paid to the parameters determining the use of secondary oxygen because rather small changes can strongly affect the points mentioned above. Since August 2016, the PCD (Post-CombustionDistributor) lances are used on a daily basis in the steelplant LD3 in Linz.

Oct 30, 2017

By Douglas Glenn Stalheim

The demands for improved mechanical properties in hot rolled long products are increasing as the expectations of global Standards and construction designer’s increase. Cost constraints limit the excessive use of expensive alloys to meet these expectations. In addition, depending on the mill, equipment can limit what can be realized to meet the increasing expectations. The most effective way to meet the increasing expectations for improved mechanical properties of optimum strength and ductility is through producing steel with as fine as possible uniform cross sectional grain size in the “as-rolled” condition. The best solution to the development of this fine and uniform cross sectional grain size is to develop a cost effective alloy design coupled with proper metallurgical process control implemented into an existing mill’s equipment capability and layout. In other words, properly bringing together alloy, metallurgy, process control and existing equipment capabilities to develop an optimum product that can meet the increasing demands of the construction designer. This paper is designed to give a solid understanding of the production and metallurgical requirements to achieve a grain size in “as-rolled” long products that is as fine as possible within the limitations of the process and production parameters of the individual plant.

Jul 30, 2018

By Dagoberto Brandão Santos, Kairo de Barros Guimarães, Túlio Magno Füzessy de Melo

The effect of the cooling conditions on the microstructure and hardness of a Dual Phase hot-rolled steel 800 MPa strength was investigated. Simulations of the cooling conditions using a dilatometer were carried out from samples of a hot rolled coil with variations of the intermediary temperature from 620 to 740°C, isothermal holding time between 1 and 10 s and coiling temperature between 50 and 400°C. In addition, two CCT (Continuous Cooling Transformation) diagrams were developed to evaluate the effect of the isothermal holding time on the phase transformations of the remaining austenite. It was observed that the intermediary temperature has a strong influence on the kinetics of the phase transformation, as well as the isothermal holding time influences the amount of ferrite formed and, consequently, the final microstructure and hardness of the material. The coiling temperature did not cause significant changes in the amount and morphology of the ferrite, but a gradual replacement of martensite with bainite was observed, which, in addition to the self-tempering effect, contributed to the hardness reduction.

Oct 1, 2019

By Cleber Caetano Thomazi

Rotary kilns are continuous process equipment used on calcining of nickel ore. The chemical and physical reactions are created by means of heat up the material to predetermined temperatures. Tertiary air fans are attached to the kiln shell to maintain oxidizing/reduction conditions. Special ducts orientate the air flow inside the kiln. In the present work, two types of failure on distinct tertiary ducts mounted on the same kiln are reported. Chemical analysis, hardness test, metallographic and fractographic examinations were carried out. Fabrication related problems and creep were identified as the root causes of damages.

Oct 30, 2017

By Mirko Jurkovic, Thomas Hueper, Jens Kempken

The high competition scenario pushes the steel producers business. Zero defect requirements from customers force the operators for additional efforts in process control and quality management. PQA® has been developed as an advanced process and quality management assurance solution. It is focusing on the analysis of process data, equipment information, inline quality measurement devices and trend analysis. The paper describes the structure of the advanced process and quality management assurance solution PQA®; it gives insights on the expert know-how, process and quality evaluation and points out the benefits like cost reduction, improvement yield and customer satisfaction increase.

Oct 1, 2019

By Sebastien Flament

More and more Hot Strip Mills are facing defects on their products that lead to a rejection of complete product batches by their customers. Several of those defects are induced by excessive work roll degradation. This paper is focussed on the understanding of work roll corrosion and oxidation mechanisms in a hot strip mill. Several laboratory trials (Hot rolling simulator, cyclic oxidation) have highlighted important factors influencing corrosion of work rolls as well as helping the understandings of oxidation of a work roll in the roll bite and along the roll circumference in a stand. The attention is focussed on several elements present in water used in HSM for direct roll cooling (e.g. chloride, bactericides, sulphates, phosphates) and their effect on roll surface degradation. The second part of this paper is focused on the understanding of work roll oxidation along the roll circumference. The effects of roll composition, roll temperature, water composition and water temperature have been studied in order to understand the oxidation/corrosion mechanisms in a HSM.

Aug 16, 2017

By Wagner Viana Bielefeldt, Vinicius Cardoso da Rocha, Augusto Lachini Pereira, Antônio Cezar Faria Vilela

A minor change in the chemical composition and temperature affects the slag viscosity, which has a great extent of the physical properties in regarding refining slags. Optimizing those parameters may affect the steel cleanliness. The viscosity measurement process is considered expensive, so the cost-effectiveness does not favor the measures at high-temperatures. Alternatively, it is possible to apply mathematical models or thermodynamic softwares to obtain viscosities for a given range of chemical composition and temperature of slags. The present work contemplates a validation of the experimental data, collected in the literature, with a calculated data and proposes an accurate representation of iso-viscosity curves applied for secondary steelmaking slags, covering the composition ranges: 0–100 wt.% CaO, 0–80 wt.% SiO2, 0–77 wt.% Al2O3 and 0–15 wt.% MgO (CSAM) system at 1500ºC. The viscosity representation fields include fully liquid and a partially liquid slags in the CSAM system and the viscosities were calculated using the FactSage 7.2 (for Liquid Phase) and the Roscoe-Einstein equation (for Phase mixture) for a total of 5976 slags. The preliminary results indicated that there is a great convergence between the calculated and experimental viscosities data, promoting an efficient approximation of the iso-viscosity curves for the CSAM slag system in the high-temperatures.

Nov 1, 2019

By Alessandro Marques

Based on a short overview regarding steel defects in the final product, several refractory approaches to maintain or increase steel cleanliness are reviewed in this publication. By applying a ladle to mold approach, one potential to maintain cleanliness is to reduce the probability of air ingress by selection of a suitable slide gate system. Following this path, also the influence of a special configured impact pot is presented to maintain steel quality. Finally, higher productivity as well as cleanliness can be provided by selection of PROIL as a revolutionary product at the casting machine.

Oct 30, 2017

By Carolina Arriel Pedroso Dias

Neste trabalho, tiras de aço inoxidável duplex UNS S32205 foram laminadas a morno a 600°C com 60% e 80% de redução e, em seguida, foram recozidas a 1050°C durante 300 s. A tira como fornecida (laminada a quente industrialmente e recozida) também foi recozida para efeito de comparação. Avaliou-se o comportamento mecânico das amostras como fornecida, 60% e 80% por meio de ensaios de tração e microdureza Vickers, obtendo-se 779 MPa, 730 MPa e 807 MPa de limite de resistência a tração e 265 HV, 244 HV e 256 HV de microdureza Vickers para as três condições descritas, respectivamente. Outros ensaios de microdureza foram realizados ao longo da superfície do corpo de prova fraturado em tração, indicando um aumento da dureza nas regiões mais próximas da fratura. O aumento da dureza na região de estricção indicou o aparecimento da martensita induzida por deformação para as amostras laminadas a morno. Usando a derivada da curva tensão verdadeira em função da deformação verdadeira, (ds/de), avaliou-se o comportamento de encruamento do aço para as três condições. Juntamente com os exames por microscopia eletrônica de alta resolução e difração de raios X, buscou-se uma interpretação dos mecanismos de deformação plástica envolvidos no processo de encruamento. Em determinados estágios, observou-se uma mudança da inclinação para um regime estável, indicando a ocorrência de outros mecanismos de deformação plástica, diferentes do escorregamento de deslocações. A martensita induzida por deformação foi considerada responsável pelo aumento da taxa de encruamento do aço, i.e., por ser obstáculo à movimentação das deslocações e por postergar a formação da estricção.

Oct 30, 2017

By Rob van Opbergen, Edo Engel

The highly dynamic economic climate of recent years has tightened the operating envelope for steel producers world-wide. Steel producers continue to experience immense pressure to respond quickly to changing circumstances and the focus has shifted towards efficiency improvement and maximizing flexibility in operations. The ability to safely stop, restart and ramp-up production facilities has become essential. Establishing this level of flexibility, without sacrificing efficiency, requires sound process control, fit-for-purpose process management practices and solid know-how and experience regarding special situations in blast furnace ironmaking operations. The same business environment that demands this increased flexibility has made it increasingly difficult for steel producers to sustain sufficient knowledge about these situations. While many experienced, senior operational staff have retired, a new generation of ironmaking specialists has acquired its hands-on experience over more recent decades, during which these process situations have been much less frequent than before. Over the past 10-15 years, the requirement in the industry for external operational support during e.g. blast furnace blow–downs, salamander tapping and restarts after planned and especially unplanned stops, has become increasingly frequent. This article presents a number of these cases from a process management perspective as well as with regard to project organization and optimized cooperation between internal and external teams of experts.

Oct 1, 2019

By Stefan Thelen

In November 2013 Salzgitter restarted their tandem mill after two weeks of shutdown, during which the existing mill entry equipment has been removed and replaced by new entry area equipment including pay-off reels, welding machine and a vertical entry looper for continuous feeding of the 5-stand tandem mill. It turned out to be beneficial to both product quality and production capacity.

Aug 16, 2017

By Ronaldo Esteves Ribeiro, Jefferson Felipe Faria Clemente, Carlos Victor Francisco dos Santos, José Herbert Dolabela da Silveira

n recent years, the market for thick plates has been highly competitive, in this scenario the plates quality is a critical success factor. In this process, the quality of the cut in thick plates is one of the important requirements for the customers, by the visual aspect as well as the technical aspect of the plate application. In the shear line, the cutting is done by shearing to trim tips, subdivide plates, trim side edges, remove samples, eliminate defects, etc. The cut is obtained by the penetration of the upper knife in the plate, causing plastic deformation in a certain region and hardening. If the clearance between the knives is adequate, the cracks will be close to the centre of the plate thickness and will result in a good cut quality. This work will present the theory of cutting of thick plates, the types of shearing, the quality of the edge in the cut, the types and the main characteristics of the knives.

Oct 1, 2019

By José Adilson de Castro

In this paper a new technology for a compact iron ore sintering machine is analyzed. The compact sintering process is based on the massive injection of gaseous fuels and the solid fuel is only agglomerated fine charcoal obtained by biomass. The solid fuel used in this study is obtained by agglomeration of fine charcoal produced from elephant glass which has very short period for production and CO2 capture(less than 6 months in tropical climate). To overcome the lower heat supply into the combustion front of the sintering process the simultaneous injection of oxygen and gaseous fuel is proposed. The proposed methodology is to combine the solid fuel (agglomerated fines charcoal) and steelworks gases in a compact machine to enhance heat and mass transfer with high productivity (about 5 times the conventional large machine). A multiphase mathematical model based on transport equations of momentum, energy and chemical species coupled with chemical reaction rates and phase transformations is used to analyze the inner process parameters. A base case representing a possible actual industrial operation of the sintering machine is used in order to compare different scenarios of practicable operations which represents advanced operations techniques. The model was used to predict six cases of combined operation with biomass and fuel gas utilization with oxygen support.

Aug 2, 2018

By Mario González Ramírez

The safe transport of sour gas requires steels with enhanced hydrogen induced cracking (HIC) resistance. Centerline segregation bands of high hardness microconstituents and non-metallic inclusions are the heterogeneities usually linked to HIC failures in pipeline steels. Full-scale production heats of a new low Mn, Nb microalloyed steel were produced by different steel mills aiming at the application in sour gas environments. The new alloy design provides both effective strengthening and control of sulphide inclusions. Coil microstructure consisted of fine grained ferrite with a small volume fraction of uniformly dispersed eutectoid aggregates. Most importantly the microstructure was uniform in both the longitudinal and transverse directions and exhibited exceptional consistency. Samples from this steel were submitted to HIC testing according to NACE standards TM0284-2003 without any sign of cracking. The results, so far, confirm that this new alloy design provides the unique opportunity to economically produce a high strength pipe steel grade with improved sour service resistance for the linepipe industry.

Aug 8, 2018

By Nathanael Wagner Sales Morais

Os aços maraging tem grande importância tecnológica devido sua aplicação nas industrias aeroespacial e nuclear. Uma das aplicações para esse material é a fabricação de cilindros de alta resistência pelo processo de estampagem profunda, logo o conhecimento da textura cristalográfica torna-se fundamental. Este trabalho investigou o efeito da laminação à frio seguida por um recozimento sobre a microestrutura, textura e anisotropia plástica no aço maraging 350. A anisotropia foi medida pelo cálculo dos coeficientes de Lankford e dos coeficientes de anisotropia normal (Rm) e planar (?R). Os resultados mostraram o aumento na deformação a frio gera um aumento na intensidade da fibra acompanhada de um aumento no valor de Rm. As análises metalográficas mostram que maiores reduções induzem à um precipitação intermetálica após o recozimento.

Aug 8, 2018

By André De Araujo Abilio

Geopolímero é um material inorgânico formado por ativação alcalina durante a qual processos de polimerização de alumino-silicatos formam a cadeia polimérica que consiste em tetraedros de Si-O e Al-O. Com o intuito de encontrar subprodutos para serem usados como uma alternativa de aglomerante na formulação do geopolímero, um subproduto oriundo do processamento de rochas ornamentais foi utilizado. O presente estudo consiste na caracterização da capacidade de flexão do material geopolimérico resultante da adição do granito como aglomerante alternativo. Estudos foram elaborados de modo a avaliar ambos o efeito e a viabilidade de seu uso em formulações futuras do geopolímero.

Aug 16, 2017

By Fabio Da Costa Garcia Filho

O uso de resíduos de vidro como aditivo mineral finamente moído, em substituição parcial de cimento e agregados é uma direção promissora para a reciclagem. Este trabalho teve como objetivo analisar a influência de resíduos do processo de corte de vidro em argamassa adesiva, como substituição parcial de cimento e agregado miúdo. O vidro em pó foi utilizado em percentuais de 10, 15 e 20% em peso em substituição ao cimento Portland e, em outro momento, em substituição ao miúdo agregado. Verificou-se que a substituição refletiu positivamente sobre a resistência à adesão da argamassa, com o aumento da temperatura de cura.

Oct 30, 2017

By Shanti Arangala

Several improvements were made to the single strand rod mill at Laverton to increase production, reduce maintenance and improve several aspects of product quality. With changes to the water cooling line and control system, cobbles could be significantly reduced, more consistent properties obtained and yield improved. An upgrade of the laying head enabled vibrations to be reduced and thus allowed for higher speeds on small sizes. With potential for dramatically increased pipe life, a new pipe support and laying pipe system provided for improved laying pattern on small sizes and thus more uniform cooling on the conveyor and better coil package. This paper discusses details of these equipment and control system upgrades and the resulting benefits that have been realized from the project.

Aug 16, 2017