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By D. F. Walsh

A study of damping capacity was made on a number of magnesium-base alloys, commercial types and experimental compositions. Hardness and tensile properties were determined, and the microstructure of each alloy was examined. Alloys of low yield strength, in general, possessed high damping ability. A correlation was established between damping capacity and composition.

Jan 1, 1962

By G. L. Oldright, Virgil Miller

"ACKN0WLEDGMENTSThe data given in this paper were collected at the Bunker Hill smelter through the courtesy of Stanley A. Easton, the vice-president and general manager, Frank M. Smith, the smelter director, and with the assistance and cooperation of A. F. Beasley, the smelter superintendent, and his staff members.THE BLAST FURNACE AND PLANTThe general lay-out of the recently built (1917) Bunker Hill plant has been given in the technical press in articles that were cited in Report of Investigations 3088. In addition it may be noted that the description of an ideal smelter given by Riddell 5 a year later fits the Bunker Hill smelter very well, with some changes, such as the location of the stack, made necessary by topography. For purposes of this article on the blast furnace it may suffice to state that the plant is one of the ""side hill location"" type. The various successively lower benches may roughly be considered as made for (1) the stack, (2) Cottrells and bag houses, (3) Dwight and Lloyd sintering machines with the equipment or bins for handling or mixing the feed and storing the finished product, sinter, and (4) the blast furnace feed floor with a slightly rising gradient to the bottom of the bins for sinter, feed, and take. The lowest bench (5) might be considered that of the blast furnace tapping floor at which or at appropriately slightly lower elevations are located the units for softening, refining, and treating precious metals, and for casting and loading lead. A very careful study of grades was made in order to be able to handle the products easily. All units were left with at least one end open to permit expansion of the plant, it desired, and each unit was separated from the other, evidently so that the operators on one level would be annoyed as little as posssible with the products made on another."

Apr 1, 1931

By M. J. Reasor, M. DiMatteo, J. M. Antonini, K. Van Dyke, Z. Ye

"The inhalation of silica has been shown to produce a dramatic inflammatory and toxic response within the lungs of humans and laboratory animals. A variety of cellular and biochemical parameters are used to assess the silica-induced lung injury. The purpose of this paper is to introduce the use of luminok:Jependent chemiluminescence as a new method to study inflammation in both phagocytic cells and lung tissue recovered from silicaexposed animals. Chemiluminescence, or the emission of light, accompanies the release of reactive forms of oxygen when phagocytic cells are challenged. In this study, male Fischer 344 rats were intratracheally instilled with either silica (10 mg/100 g bw) or saline vehicle. One day after the instillations. a marked increase in the chemiluminescence was observed in the lung tissue and bronchoalveolar lavage cells recovered from the silica- treated animals when compared with the saline controls. The light reaction was markedly decreased by either superoxide dismutase or N-nitro-Larginine methyl ester hydrochloride. Superoxide dismutase is involved in the enzymatic breakdown of superoxide anion. while N-nitro-L-arginine methyl ester hydrocholoride, a nitric oxide synthase inhibitor, prevents the formation of nitric oxide. When superoxide anion and nitric oxide react. they form the highly oxidizing substance peroxynitrite. This study then implicates peroxynitrite as an agent that may be responsible for some of the oxidant lung injury that is associated with silica exposure. The use of luminol-dependent chemiluminescence may prove valuable as a method to measure the earliest events in the inflammatory process. and may be an adjunct in studying the mechanisms that produce inflammation. - Environ Health Perspect 102(Suppl 10):37-42 (1994) IntroductionResearch on inflammation has not produced a method that links the initial events of the process to the controlling events. Rather, a variety of parameters are measured that are the result of and not the basis of the inflammatory reaction. Parameters such as tissue weight, edema, blood flow, enzyme and protein release, or production of metabolites (prostaglandins, leukotrienes) have been used extensively. A method is needed that could be applied to cells of a particular type, groups of cells of different types, and even tissue, in an attempt to study the kinetics of the inflammation as well as being sensitive enough to monitor the early events of the process . Since inflammation is so complicated, the relationship between the control of the initial events and the oxidation process has never been explained nor studied in any derail."

Dec 1, 1995

By J. J. Demeter

A tube-wall reactor with a Raney nickel catalyst deposited on the outer wall of the tube by flame spraying is effective in the practically complete conversion of 3H2+1CO synthesis gas to a high-Btu gas (methane) at an hourly space velocity of 7,000 volumes of gas (NTP) per hour per volume of annular volume. Partially reacted synthesis gas containing an appreciable amount of methane can also be treated in this reactor to increase the heating value to over 900 Btu per cubic foot. Excellent heat removal through the metal wall to a coolant and temperature control were obtained. The heat transfer co-efficient from the catalyst to the coolant was about 275 Btu per hour per square foot per ° F. Synthesis tests were conducted with tubes 1.2 inches in ad by 6 inches long, and 1.3 inches in od by 36 inches long. When operating at a synthesis gas rate of 100 to 120 scfh per square foot of catalyst-coated tube, catalyst life was long enough to realize a catalyst cost for the raw Raney nickel alloy of about 0.3 cent per 1,000 cubic feet of pipeline gas (900 to 950 Btu per scf). Gas recycling at ratios of 1:1 to 3:1 was effective in increasing conversion and in extending the life of the catalyst to about 16 weeks. In cost and in operating characteristics the tube-wall reactor compares favorably with the fluidized-bed and hot-gas-recycle reactor systems for the synthesis of high-Btu gas from H2+CO.

Jan 1, 1967

By D. Harrington

[Notwithstanding the fact that it is now fairly generally recognized that widespread explosions can be almost absolutely prevented in coal mines by efficient rock-dusting and that this rock-dusting can be done thoroughly at a cost which should seldom exceed 1 cent per ton of coal mined, a recent survey of the situation by the Safety Division of the U. S. Bureau of Mines, following a similar survey by the Bureau in the fall of 1925, shows that while some progress is being made by our coal-mining people, many entire mining communities are lamentably slow in taking advantage of one of the most effective safeguards available. Much of the information as to the extent of rock-dusting was obtained through the various State inspection departments. Table 1 shows that in the fall of 1925 about 92 coal companies in the United States were using rock-dust ad that in the summer of 1927 the number had increased to 239, or about 160 per cent increase. Similarly, from the fall of 1925 to the summer of 1927 the number of mines using rock-dust increased from 177 to 463, or about 160 per cent increase. This appears to be a decidedly healthy increase, but when it is considered that in 1926 (the last date for which figures are available) there were 7,141 bituminous mines operating and that there were only 463 or 61 par cent, which were even reported to Ice using rock-dust to any extent whatever, the forgoing figures as to progress are by no means impressive or even satisfactory.]

Jan 1, 1928

By H. J. Heinen

This report summarizes preliminary research studies by the Bureau of Mines in electrowinning molybdenum directly from pure or impure molybdenum trioxide (MoO3) by fused-bath electrolysis in an open graphite cell without need of a protective inert atmosphere. A formulated electrolyte of the tertiary system containing 41.6 percent sodium pyrophosphate, 16.7 percent sodium tetraborat, 33.3 percent sodium chloride, and 8,4 percent molybdenum trioxide, by weight, electrolyzed at 1,000° C,, gave excellent results. Current density studies were made over a range from 20 to 260 amperes per square decimeter. Current efficiencies of 80 to 90 percent were obtained over the entire range. Yields up to 500 grams of molybdenum per kilowatt-hour were obtained. Higher current densities, however, reduced yields and produced a finer grained metal. The two most important facets in electrowinning molybdenum from MoO3, in an open cell, are temperature and electrode spacing to minimize or eliminate the formation of the suboxide MoO2, the major source of oxygen contamination. At temperatures of 1,000° C. and higher, together with the proper spacing of the electrodes, formation of oxides are practically eliminated. Molybdenum metal electrowon from pure MoO3 was 99.9 percent pure and contained 0,056 percent oxygen and 0,007 percent carbon. This metal, when arc-melted, had a Vickers hardness number of 175 and contained 50 parts per million oxygen and less than 10 parts per million carbon. Molybdenum metal electrowon directly from an impure MoO3 containing 90 percent MoO3 resulted in a metal of 99.8 percent purity.

Jan 1, 1961

By J. M. Mutmansky, S. Padmanabhan

"The subject of quartz occurrences in respirable coal mine dusts has been of increasing concern in recent years. The primary impetus for this concern has been provided by better measurement technology that has detected an increased number of mines with high quartz content in their respirable dusts. This paper presents the results of statistical analyses of quartz levels in multi-stage impactor samples from eighteen different coal mining sections located in Pennsylvania, West Virginia, Ohio, Illinois, Kentucky, Colorado and Ucah. The quartz and kaolinite determinations were then determined by combining impactor stage loadings to provide larger dust masses and applying the infrared spectrometry procedure outlined in Bureau of Mines/MSHA Method P7.The results will be presented using two categories of data collected during two separate phases of the research:(l) quartz concentration data from mines where quartz was known to be present in relatively high concentrations, and(2) quartz concentration data from mines chosen at random.The aspects of the occurrence of quartz in coal mine airborne dusts that will be reported include the size dependence of the quartz content, quartz variations with location in the mining section, and variations due to mining region. The results of the study show a strong pattern of size dependence of the quartz content in mines for which high quartz concentrations exist. A similar, though less pronounced, pattern exists in mines chosen at random. Quartz levels appear to have a varying relationship to section location and strong geographical patterns do not appear to exist in the data collected. Kaolinite content was found to be similar to that of quartz with patterns that are somewhat more consistent."

Jan 1, 1989

By G. R. Peterson

The Bureau of Mines evaluated the potential supply of cobalt from known domestic resources, both as a primary product from some deposits and as a byproduct from others, and found that U.S. production could play an important role in meeting U.S. cobalt needs by the mid-1980's. This production would be of a relatively short duration, however, with production declining significantly before the year 2000. As part of the study, a tonnage-price relationship was developed indicating the quantity of cobalt that could be produced from known cobalt-bearing deposits at various primary commodity prices and at a 15-percent rate of return on the required capital investment. All capital and operating costs are calculated in August 1980 dollars, and commodity prices are based on August 1980 prices. Known U.S. cobalt-bearing deposits which represent the current U.S. cobalt reserve base contain some 310,800 metric tons of cobalt in slightly over 1 billion metric tons of demonstrated mineralized material. Approximately 37 percent of the cobalt contained in the reserve base is considered recoverable using existing technology. Of this quantity, some 87,000 metric tons of cobalt is economically recoverable assuming a cobalt price of $25 per pound, a copper price of $1 per pound, and a lead price of $0.40 per pound. Assuming that the cobalt price decreases to $15 per pound, keeping copper and lead prices constant, the quantity that is considered economically recoverable declines to some 45,700 metric tons. Domestic cobalt consumption in 1979 was 7,900 metric tons (17.4 million pounds). Currently, no primary cobalt is produced from domestic resources, and none has been produced since 1971.

Jan 1, 1981

By an Slo, J. J. Forbes

"INTRODUCTION This is the first of a series of information circulars dealing with the control of roof and the prevention of accidents from falls of rock and coal. These circulars are being published to focus attention of the coal-mining industry on this most prevalent source of fatalities and injuries and to present factual information that should be helpful in reducing loss from these causes.Records of fatal accidents in the coal mines of the United States, from all causes, have been kept since 1906; during this period approximately 30,000 men have been killed by falls of rock and coal in the bituminous-coal mines, and more than 7,000 men have lost their lives in the Pennsylvania anthracite mines from the same causes. From 1906 to 1930, about 900 men were killed annually by falls of rock and coal in bituminous-coal mines, and about 200 men were killed annually in anthracite mines during the same 25-year period. From 1931 to the present time, the number killed annually from falls of rock and coal has averaged more than 500 men in bituminous-coal mines and about 125 men in Pennsylvania anthracite mines.Numerically the record of accidents from falls of rock and coal shows improvement, but on a percentage basis and on a million-man-hours-of-exposure basis little, if any, improvement has been made during the past 40 years. The cold fact is that, year after year, about 50 percent of all those killed in coal mines in the United States lose their lives from falls of rock and coal."

Apr 1, 1948

By R. H. Storch

This report describes work done as part of a Bureau of Mines program to appraise the titanium-mineral resources of Idaho. The work included both field reconnaissance and a spot churn-drilling program. Much general information was available, as a result of earlier work done under the Western Radioactive Minerals Exploration Program conducted between 1950 and 1954 by the Bureau of Mines for the United States Atomic Energy Commission. This particular exploration provided data as to the quantity of ilmenite (TiFe03) and accessory black-sand mineral concentrates in a number of placer deposits; however, at that time no tests were made to ascertain if the ilmenite was of marketable grade. The spot churn drilling was begun in the Gold Fork area of Long Valley, Valley County, Idaho (fig. 1), in August 1956 and was completed during October of the same year. Eleven holes (designated as the GF series on fig. 2) 35 to 45 feet in depth, aggregating 425 feet, were completed during this period. Data from other exploration drilling in 1951 was used in this report. The 13 holes in the G series shown in figure 2 were drilled by the Bureau of Mines for the United States Atomic Energy Commission; the 7 holes of the DH series were drilled by the Bureau of Reclamation. The 20 holes, ranging from 16 to 140 feet in depth, totaled 1,625 feet. The combined number of all samples recovered was 422. Those taken in 1956 were composited for each drill hole and sent to the Bureau of Mines laboratory in Albany, Oreg., for analyses.

Jan 1, 1958

By Maria I. De Rosa

Table 37 and figure 13 show the number of fires and fire injuries for surface stone mines by state during 1990-2001. Table 37 also shows the injury risk rates, employees' working hours, and lost workdays. In all, 96 fires occurred in 31 states and 1 fire occurred in Puerto Rico. Sixty-eight of the fires caused 67 injuries and 1 fatality (including 6 fires and 5 injuries involving contractors). The yearly average was eight fires and 5.6 injuries. The Ewhr value was 689 x 106 hr (Irr = 0.02), and the LWD value was 7,399. Indiana had the most fires (eight fires and four injuries), followed by Georgia (seven fires and seven injuries) and Pennsylvania (seven fires and five injuries). Of these states, Georgia had the highest injury risk rate value (Irr = 0.058). Table 38, partly illustrated in figure 14, shows the number of fires, fire injuries, fire fatalities, risk rates, employees' working hours, and lost workdays by time period. The number of fires and fire injuries show an increase during the second period followed by a decrease during most of the remaining periods. Employees' working hours increased during most of the periods. The In values follow patterns similar to those shown by the injury values. Tables 39-44 show the number of fires by ignition source, method of detection and suppression, equipment involved, location, and burning material by time period. Figure 15 shows the major variables related to fires for 1990-2001. Table 45 shows the number of fire injuries per number of fires causing injuries and total fires by year, ignition source, equipment involved, and location.

Jan 1, 2004

By Harry E. Tuff

"This paper is based data obtained by the Bureau of Mines from some of the principal mine operators in Pennsylvania, in the course of a study conducted in cooperation with the U. S. Forest Service, with regard to economies that might be effected in the selection storage, and preparations of timber particularly treatment with preservative to prolong its life.The Pennsylvania anthracite region, considered as a single mining district is by far the largest user of mine timber of any mining district, either coal or metal, in the United States, and the bituminous districts of Pennsylvania rank second. The present annual consumption of mine timber by the coal-mining industry of Pennsylvania probably exceeds 100,000,000 cubic feet annually.In 1919, Pennsylvania produced, in round figures, 145,300,000 tons of bituminous coal, 86,200,000 tons of anthracite, and 5,400,000 tons of iron ores. If it be assumed that the bituminous coal mines required 0.33 cubic feet, anthracite mines 0.7, and iron mines 0.9 cubic feet per ton mined the timber requirements were bituminous. 47,950,000; anthracite, 60,340,000; iron mines, 4,860,000 or a total of over 113,000,000 cubic feet.The average cost of round mine timber in the anthracite region in 1905, was, according to the U. S. Forest Service, 6.6 cents per cubic foot, and $15.00 per 1000 board feet for sawed timber. The present cost Las advanced to 27.5 cents per cubic foot for round timber, delivered to the mine, of which cost 57.4, represents freight charges."

Nov 1, 1923

By B. W. Jong

As part of the Bureau of Mines program to develop substitute or improved performance refractory materials for metallurgical applications, the Tuscaloosa Research Center has evaluated the effect of additives on sintering and strength properties of aialon (silicon aluminum oxynitride) compositions fabricated by a conventional powder metallurgy technique. Additions of Y203, Gd203, CeO2, MgO, ZrO2, ZrSiO4, and MgA12O4 to a sialon composition containing 70 pct ß-Si3N4 + 30 pct a-A1203 increased sintered densities by as much as 50 pct over densities of undoped material. The studies also indicated that sintered densities reached a maximum between 20 and 30 mole-pct a-A1203 when a series of sialon compositions of a-Si3N4, having 6.7 to 57.9 pet a-Al203, were doped with Y203, Gd2O3, and MgO. In studies to establish the effect of the crystalline phase of the silicon nitride and alumina used, tests were made using a- and ß-Si3N4 and a- and ?-A12 03 as starting materials. The tests indicated that when using an addition of 5 wt-pct Y203, best results were obtained with a sialon composed of 74.4 mole-pct a-Si304 and 25.6 mole-pct ?-A1203. In other tests made with this sialon composition MOR values of 28,120 and 29,500 psi at 25° C, and 23,520 and 16,850 psi at 1,400° C, were obtained when doping with 5 wt-pct ZrSiO4 and ZrO2, respectively.

Jan 1, 1980

By W. L. O'Brien, E. A. Rowe

Electrorefined vanadium with additions of up to 5 percent by weight of yttrium, cerium , lanthanum , praseodymium, neodymium, and samarium was melted to ingots in a nonconsumable electrode arc in a helium atmosphere . The ingots were rolled into strips and evaluated for the effect of the alloying elements on hardness , tensile strength , ductility , recrystallization temperature , and microstructure . Except for samarium , average additions of alloying elements of 1 to 2 weight - percent resulted in the retention of 0.12 to 1.05 weight - percent in the alloys and reduced the ultimate tensile strength from about 48,000 to approximately 30,600 psi . The corresponding yield stress (0.2 percent offset ) was reduced from about 40,700 to approximately 20 , 200 psi . Diamond pyramid hardness (DPH) was reduced from 117 to an average of 62 kg /mm² . Increased malleability at room temperature resulted with yttrium and all rare - earth- metal additions , except samarium , particularly with more than 0.25 weight - percent additions . Decreasing oxygen contents corresponded with the changes noted in the mechanical properties of the alloys . The recrystallization temperature of electrorefined vanadium was reduced from approximately 950 ° to 800 ° C. Yttrium or a rare- earth metal content , except samarium , in excess of 0.1 weight - percent in vanadium produced a second phase suggestive of an eutectic which indicated a possible maximum solubility of less than 0.1 weight - percent for both room and elevated temperatures .

Jan 1, 1964

By John W. Buch

"INTRODUCTION The Ruhr coal basin is estimated to cover an area of more than 1,000 square miles. Here, the total thickness of the coal bearing formation (Carboniferous) is 10,500 feet, and drilling-hole have revealed 92 coal beds with a total thickness of 262 feet. 6/ Beds pitch from 0 to 90 degrees and about 70 percent of the wartime production came from beds that pitched less than 30 decrees. 5/For example at the Minisiter Stein mine, there are 24 minable coal beds ranging from 80 centimeters. (2 ft., 7 1/2 in.) to 250 centimeters (8 2 1/2 in.). The vertical thickness of the measures is 1,000 meters (3,200 ft.), and at this mine the deposits are covered with 150 meters (500 ft.) of surface wash. The cross section (fig, 1) at Fritz mine; Hoesch, A.G., Essen, Ruhr, is characteristic, The mines have been developed and worked to vertical depths of 2,000 to 2,500 feet by vertical shafts; main-level intervals are 500 to 700 feet apart. Haulage roads are straight, driven in rock, and centered as nearly as practical between property boundaries. Levels are sectionalized by driving crosscuts at right angles to the main haulage road on 800- to 900-foot centers. The roads are the main transportation arteries for the use of trolley or Diesel locomotives. A plan of the sixth main level (fig. 2) at the Bruchstrasse mine; Gelsenkirchener A.G., Bochum, illustrates main-level development and,sectionalizing with crosscuts. The cross section in figure 3 is that of the fourth crosscut west at the same mine."

Oct 1, 1946

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

7. Hoisting Systems Hoists used solely for emergency escape use should above all, be simple and dependable. The hoist systems' motive power should be independent of all other mine equipment so that only an emergency in the immediate vicinity of the hoist will render it inoperative. The hoist should receive the same high level of inspection as is normal with any other man hoisting system. It should be operated at regular intervals, and must include sufficient safety devices to ensure safe operation when hoisting men. Of equal importance, however, safety devices must be included to safeguard the hoist system from in¬advertant damage due to inspection, maintenance or operator error In an emergency situation the hoist operator will be under considerable stress and the system must be simple and foolproof to operate. Under normal circumstances the hoist will only be operated during the regular inspection cycle. Because of this very low operational use rate, certain requirements, normally associated with man hoisting, can be relaxed. In particular the wire rope installation requirements, in terms of drum and sheave diameter and fleet angles, can be reduced provided that rope inspection during the system life is maintained at a high level. The following section includes recommended guidelines for emergency hoist system design, installation, operation, maintenance and inspection A summary of available hoisting equipment and components is included in Appendix C. Emergency Hoist Guidelines All hoists designated as part of a mine emergency escape system shall meet the requirements of the Emergency Hoist Guidelines. Where these hoists are also utilized for hoisting other than emergency hoisting, the requirements of Title 30, Code of

Jan 1, 1976

By E. C. Lane

For a number of years the Bureau of Mines has been studying crude petroleum from the producing fields of the United States, During the past year 10 crude-oil samples have been collected and analyzed from the producing fields of Pennsylvania and New York. This report gives the results of these analyses and for the purpose of comparison also analyses of samples of crude oils taken previously from some of these fields. This survey includes samples from normal producing properties as well as from properties using stimulative production methods such as water flooding and rapressuring. The outstanding feature of the survey is that the crude oils from tike various fields throughout this general area are similar in character and uniform in quality although they were produced from different sands and by various methods. Samples from fields in Venango County, Pa., however, appear to have a lower gasoline content than the others. This report includes two analyses reprinted from Bureau of Mines Bulletin 291.4/

Jan 1, 1938

By E. C. Lane

For a number of years the Bureau of Mines has been studying crude petroleum from the producing fields of the United States. During the past year 10 crude-oil samples have been collected and analyzed from the producing fields of Pennsylvania and New York. This report gives the results of these analyses and for the purpose of comparison also analyses of samples of crude oils taken previously from some of these fields. This survey includes samples from normal producing properties as well as from properties using stimulative production methods such as water flooding and repressuring. The outstanding feature of the survey is that the crude oils from tine various fields throughout this general area are similar in character and uniform in quality although they were produced from different sands and by various methods. Samples from fields in Venango County, Pa., however, appear to have a lower gasoline content than the others. This report includes two analyses reprinted from Bureau of Mines Bulletin 291.4/

Jan 1, 1938

By O. C. Blade

This report on the properties of motor fuels sold through service stations-in the United States was made in accordance with a cooperative agreement between the American Petroleum Institute and the Bureau of Mines of the United States Deparment of the Interior. It presents analytical data for 4,397 samples, representing the products of 130 companies. The samples were collected during December 1952 and January and February 1953. As in previous surveys, the gasolines covered by this survey include those from both large and small suppliers. The data were obtained by laboratories of various refiners, motor manufacturers, and chemical companies and submitted to the Bureau of Mines for compilation. A list of the National Motor-Gasoline Survey reports published during the past ten years is given on page 5.

Jan 1, 1953

By Robert W. Freedman, Robert L. Craft, William G. Humphrey

As part of a continuing effort to reduce the weight and bulk of equipment that mining personnel must carry underground, the Bureau of Mines and the Mining Enforcement and Safety Administration (MESA) investigated accurate and convenient gas samplers for use by mine inspectors in sampling mine atmospheres. The samplers are septum-stoppered glass vials commonly used for routine blood sampling. These lightweight, compact samplers yield results comparable with those obtained with conventional bottle samplers of 250-ml nominal capacity.

Jan 1, 1975