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By C. I. Pierce

Knowledge of the water content of oil-bearing formations is important in petroleum-reservoir evaluation work. Electric logging provides a means for making reliable estimates of water content if resistivity-saturation relationships representative of the formations are available. Relationships can be determined in the laboratory by a number of methods. This report describes and presents results of a laboratory investigation conducted at the Bureau of Mines Appalachian Experiment Station, Morgantown, W. Va. (1) to evaluate an evaporation method of attaining water saturations in sandstone samples when determining resistivity-saturation relationships and (2) to compare saturation exponents derived from data obtained, using different methods of achieving water saturations. A series of tests was conducted to determine the effect of evaporation on salinity distribution within the core specimen. Results of these tests show that a zone of high salinity was set up at the surface of a sample during evaporation and that long periods were required for the sample to reach resistance equilibrium after evaporation had ceased. Equilibrium time ranged from several minutes to several days, depending on the sample size and the technique used. The high-salinity zone was removed from the sample by using auxiliary porous material in capillary contact with the sample surface during evaporation. Salinity determinations and resistance measurements indicate that, at saturations greater than the minimum interstitial values, the mechanism of flow during evaporation was one of moisture migration mainly as a liquid from the interior of the test specimens to their exterior surfaces. The concentration of the contained brine remained essentially unchanged, except for a narrow zone near the evaporating surfaces.

Jan 1, 1958

By D. J. Bauer, V. E. Shaw

Bastnasite concentrate was processed to recover total rare - earth content and obtain high - purity ceric nitrate . Reaction of the concentrate with 45 percent caustic soda for 1 hour at 180 ° C in stainless steel vessels resulted in 99 - percent conversion to rare - earth hydroxides . A drying step followed by solution in nitric acid produced a tetravalent cerium fraction amenable to extraction with TBP . Single- stage separatory funnel experiments resulted in 90 -percent recovery of ceric nitrate at a purity of 99.9 percent . Fractional extraction in pressure - bubbler columns resulted in 98.5 - percent recovery of 99.5 -percent - pure ceric nitrate .

Jan 1, 1964

By W. W. Adams

"The third annual safety contest for plants producing sand and gravel, which was conducted in 1911 by the United States Bureau of Mines in cooperation with the National Sand and Gravel Association, registered further progress in safety as compared with the two previous annual contests. Both the accident-frequency rate and the accident-severity rate were reduced.The period covered was the calendar year 1931; sixty plants participated, and 17 States were represented by the participating companies.The contest covered accidents and man-hours worked by all men at the participating plant who were employed by the same company; and it included work up to the point of delivery of the material directly to the consumer or to an independent agency of transportation--in other words, to the point of relinquishment of control of the material by the producer.The purpose of the yearly contests for producers of sand and gravel is to aid in the promotion of safety among the employees and in the reduction of accident costs to the companies. The contests develop friendly rivalry among the various plants and among the employees of individual plant in a concerted effort to prevent accidents.Two safety trophies are awarded annually, both of which are provided by Rock Products magazine. One of the trophies is for the host safety record among plants that were in operation the contest year 100,000 or more man-hours; the other trophy is for the best among plants that were in operation lees than 100,000 man-hours. Awards and the relative standing of the various plants are based upon statistical compilation by the Bureau of Mines of accident reports and employment reports furnished by the enrolled companies. are summarized at the close of each year, and the summaries are submitted to each company concerned for certification as to the accuracy of the summary and the completeness of the company's reports from which the summary was prepared. When the summery is returned signed by an official of the company, the records are considered to be a trustworthy basis for determining the relative standing of the various plants. The position of each plant is determined by its accident-severity rate; that is, the number of days of disability resulting from accidents for each 1,000 men-hours of work done by all employees at the plant."

Aug 1, 1932

Protect rescue workers fighting fires or mine personnel temporarily working in hot environments from heat stress. Approach A specially designed ice-cooled vest is worn while working in hot environments where cooling the mine air is not possible. How It Works The vest holds a total of 44 individual ice cells in packets that are firmly held near the wearer's skin. These ice cells remove heat from the wearer, reducing heat stress and increasing comfort. The locations of the ice cells and packets are shown in the diagram. The vest is constructed in three layers with the outer layer being aluminzed fiberglass cloth. Its aluminized surface reflects radiated heat, and its fiberglass cloth provides fire resistance and strength.

Jan 1, 1979

By C. H. Elder, Maurice Deul

Coal degasification boreholes drilled from the surface have been success - fully hydraulically stimulated to increase the flow of gas from the coal. This Bureau of Mines report describes the hydraulic stimulation procedure for a coalbed, the equipment required, and design criteria for the treatment. Three examples of stimulation treatment show from fivefold to twentyfold increases in gas production. The tests were conducted in the Pocahontas No. 3coalbed, Buchanan County, Va., the Pittsburgh coalbed, Washington County, Pa., and the Mary Lee coalbed, Jefferson County, Ala. Two sites where the coal was hydraulically stimulated and exposed by subsequent mining show no adverse effect on mining operations through the treated zones. The induced vertical partings were confined to the coalbed and did not in any way affect either roof or floor rock.

Jan 1, 1975

By Daniel Edelstein

In 1985, ASARCO Incorporated terminated copper smelting operations and associated byproduct arsenic trioxide recovery at Tacoma, WA, although shipments of arsenic trioxide from stocks and limited production from cleanup operations continued. Imports of arsenic trioxide increased markedly as a result of increased demand for arsenical wood preservatives and the decline in domestic shipments of trioxide. Expanded world capacity more than met the increased demand for arsenic and its compounds, and prices remained unchanged throughout the year. Domestic Data Coverage.-Arsenic trioxide was produced by one U.S. company, which voluntarily reported its production to the Bureau of Mines.

Jan 1, 1987

By J. D. Dixon

The Bureau of Mines has developed structural design data for unreinforced concrete tunnel linings in the form of stress and deflection coefficients from which bending, axial, shear, and boundary stresses, moments, thrusts, and shear forces, and structural deflections can be determined at any point on the lining. Results were obtained by structural analyses of nine concrete-lined tunnel configurations subjected to 22 biaxial load conditions. The tunnel configurations include three basic shapes, circular, rectangular, and horse-shoe, with dimensions based on designs evolved by the mining industry. These analyses were made by the direct stiffness matrix method, a computer-oriented procedure. Numerical results agree closely with those obtained experimentally.

Jan 1, 1969

By G. G. Morgis, J. J. Forbes

"INTRODUCTION The greatly diversified and increased uses of beryllium and its con& pounds in recent years have focused attention on the health hazards incident thereto. The Bureau of Mines has a fundamental interest in safety and the elimination or reduction of health hazards in the mineral and allied industries, and it recognizes that serious hazards are inherent in the production and use of beryllium and its compounds. This circular presents a review of the literature pertaining to such health hazards but does not describe original research by Bureau personnel. Most of the bibliography has boon either quoted in part or abstracted in an effort to present information in a comprehensive and readable form.In reviewing the literature, differences of opinions wore recognized in the writings of the respective authors, but no attempt was made to evaluate such differences. This presentation was devoted strictly to reporting without editorial comment.SUMMARYAlthough beryllium was known to industry for about 150 years, its toxicity did not present any serious problems in the United States until the advent of World War II, when the increased use of this element and its compounds brought to light several toxicologic reactions occurring primarily in the lungs and skin of workers handling it. The pulmonary effects, characterized as acute pnoumonitis and chronic pulmonary granulomatosis in beryllium workers, are far more serious than the dermatological manifestations.The addition of beryllium to the list of toxic industrial metals has boon so recent that there is still some confusion in the clinical picture. Data on magnitudes of exposure likely to be responsible for the production of disease are not yet adequate. There appears to be no relation between the severity of exposure and the development of cases some of those having had severe exposure have not developed a reaction, whereas those having a slight exposure in some instances have developed a response."

Jul 1, 1950

By Motohisa Kanda

The time and amplitude statistics necessary to adequately describe electromagnetic (EM) noise in mines are illustrated through computer software techniques. They are 1) Allan Variance Analyses (AVA), 2) Interpulse Spacing Distributions (ISD), 3) Pulse Duration Distributions (PDD), 4) Average Crossing Rates (ACR) , and 5) Amplitude Probability Distributions (APD) . These statistics are illustrated using data taken from a rather large store of raw analog data recorded in operational mines. The curves generated for the illustrations characterize the noise environment in the mines from which the corresponding data were taken, and should aid in the design of reliable communication systems for such mines.

By M. E. Kundick, W. E. Dieter, L. Cohen

The major details of design and maintenance of a seamless stainless steel fume hood system , developed by the Bureau of Mines , are described and illustrated . Operating and housekeeping routines are outlined .

Jan 1, 1964

By A. A. Sonnek

A simple, portable helium analyzer was developed primarily for field use. Its utility lies in making preliminary surveys before exact analyses are required. The analyzer is based upon chromatographic principles; that is, separation of gas mixtures resulting from variable retention times of the components with respect to a separation medium (column-packing material). It uses thermistors for sensing detectors, a dry battery as source of power, and a micro-ammeter for indicating helium concentration. The absolute accuracy of the instrument depends upon the recency and care with which the instrument is calibrated with a standard gas. The unknown gas should be analyzed immediately after calibration, and another calibration should be made before another unknown sample is analyzed. The instrument is simple to operate, requiring approximately 15 minutes, after calibration, to determine the helium content of a natural gas sample. Although developed primarily for helium determination, the analyzer possibly can be used for other analyses that can be performed at ambient temperatures.

Jan 1, 1965

By B. T. Brady

Results of a study are presented of the effect of low radial reinforcement pressure on the postfailure characteristics of two types of granite, a sandstone, and marble. The low radial reinforcement pressure is applied to the rock surface by a gooch rubber sleeve. The gooch rubber sleeve provides a radial pressure of less than 1 psi pressure to the rock surface. This method of support gives an average strength increase of approximately 8 percent to the fractured rock sample.

Jan 1, 1973

By Wilbur Duvall

For the past few years the Applied Physics Branch has been investigating, experimentally, the generation and propagation of strain waves in rock. The strain waves are produced by the detonation of a high-velocity explosive placed in a small cavity in the rock. Strain gages mounted in the solid rock surrounding the cavity record the strain pulses propagated away from the source. Numerous strain-wave pulses have been recorded in different rock types for charges of various sizes and at various distances from the charge. Analysis of these records has shown, among other things, that there is associated with the strain wave a characteristic pulse width. This pulse width is dependent on the rock type and the distance from the shot point to the gage, but is apparently independent of the charge size or cavity size. Recent published literature on the generation and propagation of seismic waves indicates that the characteristic frequency of an elastic wave generated by an explosion should be a function of the rock type and the size of the cavity created by the explosion. Also, internal friction in the rock would produce absorption of high-frequency components, which would cause continual change in the shape of the pulse propagated. As the experimental data did not verify the expected change in pulse shape with cavity size, a theoretical investigation of the vibrations associated with a spherical cavity in an elastic medium was undertaken.

Jan 1, 1950

By G. W. Grove, O. V. SIMPSON

During the years 1945, 1946 , 1947 , and up to July 1, 1948, only one death was caused by mine fires in bituminous - coal mines of the United States . The one fatality occurred in an Illinois mine in December 1945, and , therefore, there had been a period of 2-1/2 years in which no deaths occurred as the result of mine fires . Moreover, 1946 was the first year since 1930 in which no deaths occurred from mine fires . This record is markedly better than that of 1944 , when 89 fatalities and great property damage were caused by mine fires in bituminous - coal mines and 16 additional men were killed by an explosion that occurred while they were attempting to seal a mine fire .

Apr 1, 1949

By Robert L. Lagace, Alfred G. Emslie

This report presents a mathematical model for the propagation of UHF radio waves in the large cross-section tunnels of a room and pillar limestone mine, and describes the analysis of a small amount of propagation data obtained in a limestone mine. The model and analysis is based on the waveguide mode theory developed earlier for the transmission of UHF waves in coal mine tunnels, with allowance for propagation losses due to refraction into the tunnel walls, to scattering by wall roughness, and to long range random tilt of the walls. Propagation around corners and through pillars is also examined based on a ray theory approach, together with the beneficial effects of placing reflectors at intersections to significantly reduce corner losses. The theory is found to be in fair agreement with the data; however, additional in-mine measurements are needed to provide a more conclusive test of the model.

Jan 1, 1979

By David R. Forshey

This Bureau of Mines report presents a quantitative theoretical analysis of a coupled gasdynamics-heat release system involving the kinetics of water condensation in and behind the rarefaction wave in a shock tube using the method of characteristics. The merger of characteristics to form a shock wave is included.

Jan 1, 1977

By J. F. Barkley

The following questions and answers were prepared principally to supply information in answer to general inquiries received by the Bureau from those contemplating the use of propane and butane fuels . Primary or basic information only is covered; this usually gives enough guidance for most inquirers . To those who wish information of the treatise type , the handbook , Butane- Propane Gases , published by the Jenkins Publications , Inc. , 1709 West 8th Street , Los Angeles 14, Calif . , is suggested .

May 1, 1949

By T. A. Henrie, E. K. Kleespies

Carbon reduction of rutile and ilmenite in nitrogen and ammonia atmospheres was studied as a method of preparing titanium nitride . Ammonia was a better nitriding agent than nitrogen . The contact between the solid reactants , carbon and rutile , was a prime factor in nitrogen atmospheres and was of lesser import in dissociated ammonia . The reduction process for conversion of rutile to the nitride required carbon . The nitriding of ilmenite- carbon mixtures produced titanium nitride and elemental iron .

Jan 1, 1964

By J. Hanslovan, R. H. King

An investigation of the feasibility of shielding low-voltage trailing cables in underground coal mines is described. Both laboratory and under¬ground installation results are presented. The main objective of shielding is to reduce the electrical shock hazard; however, several problems will be encountered by mine operators who install shielded cables. Parameters related to such items as purchasing, splicing, troubleshooting, safety, and reliability are discussed. Some of these problems can be minimized by changes in cable constructions and shuttle-car reeling-device components. Both SH-C and SH-D constructions are considered.

Jan 1, 1979

By Bill M. Stewart, Philip W. Patton, Curtis C. Clark

Handling materials in underground mines continues to be a major safety problem. To help reduce materials-handling injuries, researchers at the Spokane Research Laboratory of the National Institute for Occupational Safety and Health are investigating those materials-handling tasks in underground mines that appear to generate a high number of injuries. Data from the Mine Safety and Health Administration for the years 1989-1999 were studied to find out if there were any trends in materials-handling accidents and if so, to determine what tasks were involved and the sources of injuries. Several underground coal and metal mines we revisited to document innovative materials-handling technologies. Considerations for safety training and mechanization needs for continued reduction in materials-handling injuries are described.