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By Charles L. Kusik

As part of an effort to establish processes that could be exploited in case of adverse changes in international chromium production and trading patterns, this study was sponsored by the Federal Emergency Management Agency (formerly the Federal Preparedness Agency) through the Bureau of Mines, to experimentally determine the feasibility of recovering chromium from critical scrap metals containing significant quantities of this element. Based on a conceptual pyrometallurgical chromium recovery flowsheet developed at Arthur D. Little, Inc., the experimental program described in this report demonstrated key process steps for the recovery of chromium as ferrochromium in a batch process. The process involves oxidation of chromium into a slag phase, subsequent separation of the slag phase from the remaining metal, followed by reduction of chromium from the slag phase to produce ferrochromium.

Jan 1, 1981

By Robert E. Hershey

1. This investigation shows that the most important beds in Claiborne County, from the standpoint of present production and reserves, are the Coal Creek and Jellico. Together, they contain 69 percent of the known recoverable reserves in the county. Reserves in five other beds are tabulated in this report; in order of quantity of reserves, they are: Blue Gem, Lower Pioneer, Pewee, Big Mary, and Rex. 2. Known measured and indicated reserves in all beds, based on a minimum thickness of 14 inches and on 1,800 short tons per acre-foot of coal in place, are estimated to be 60 million tons, as of January 1, 1953. Of this total, 55 million tons is in beds 28 inches and more thick. Areas in each bed were omitted from the estimate because available data relative to the bed characteristics are too meager to permit making an estimate that conforms with the definitions of measured and indicated coal adopted for this study. Should future drilling or development prove reserves in these areas, such reserves should be added to the total estimated reserves.

Jan 1, 1956

By T. A. Sullivan

Research undertaken by the Bureau of Mines in 1938 has resulted in the development of titanium from a laboratory curiosity to a commercial metal. Along with processes for producing the metal, it was necessary for the Bureau to develop methods for analyzing the metal, raw materials, and intermediate products. Some of the methods developed have been published.3 4 5/ General Services Administration (GSA) was responsible for purchasing titanium metal under Defense Production Act contracts with commercial producers. GSA designated the Federal Bureau of Mines to analyze this metal and establish its compliance with Government specifications. A substantial quantity of tin was found in some of the samples analyzed, and in July 1957 tin was added to the list of impurity elements to be determined. The specifications limited the amount of tin in titanium sponge to a maximum of 0.10 percent. A program was immediately initiated to investigate methods and techniques for determining tin in the range of 0 to 1.0 percent. A method accurate at the 0.10 percent level was necessary, as this level was the critical range for acceptance or rejection of the metal.

Jan 1, 1960

By Phyllip Worley, Frank E. Chase, Christopher Mark

The Harris No. 1 Mine, located in Boone County, WV, has been longwalling the Eagle Coalbed for over 30 years. Harris has experienced numerous interactions associated with the extensive room-and-pillar and longwall mining operations which have been conducted in the overlying No. 2 Gas Coalbed. The problems have included roof falls, excessive rib sloughage, and gateroad and bleeder entry closure. A detailed evaluation of the multiple seam experiences at Harris No. 1 Mine was conducted as part of the National Institute for Occupational Safety and Health (NIOSH) nation-wide multiple seam mining case history data base. One observation from the Harris gateroad case histories was that smaller, critically loaded, upper seam pillars seemed to cause more severe ground conditions than did wider pillars. The LaModel program was used to investigate this supposition, and the results confirmed that “critical” sized pillars do transmit the highest amounts of stress to adjacent seams. In addition, the data suggest that the probability of a major multiple seam mining interaction increases when the depth of cover is 1,000 ft or greater and when the Eagle seam pillars have a Analysis of Longwall Pillar stability factor less than 1.50.

By J. J. Forbes

The investigation of major and minor coal-mine disasters has been a routine function of the Bureau of Mines since its inception in 1910, and the facts obtained during such investigations have been used as a basis for determining the precautions that the personnel of many mines are observing to prevent similar occurrences, The Bureau has conducted extensive research on roof-control problems, but a comprehensive study of fatal roof-fall accidents was not attempted until February 10, 1950, when the policy of investigating all coal-mine fatalities was approved by Bureau of Mines Director James Boyd. The investigations are being conducted by Federal coal-mine inspectors functioning under the provisions of the Coal Mine Inspection and Investigation Act of May 1941, Public Law 49, and reports covering the investigations are distributed to management, the State mine inspection agency, and representatives of the mine workers organization having jurisdiction at the mine. SCOPE AND PURPOSE OF STUDY This study covers the Federal investigation of 263 of the 315 fatalities from falls of roof, face, or rib that were charged to the bituminous-coal industry during the calender year 1950. The number of roof-fall fatalities investigated is recorded by States in table 1.

Jan 1, 1951

By E. M. Tignor

A research program to aid development of improved methods for increased production of petroleum from partly depleted reservoirs is a vital part of the Bureau of Mines effort to effect true conservation of that mineral resource. This report presents results of an investigation to identify the clay minerals within some Appalachian petroleum-reservoir sands, the effect of clay content on the fluid-flow behavior of those sands, and the use of brines in water-flooding operations. Permeability measurements using kerosine, calcium chloride brine, simulated oilfield brine, potassium chloride brine, sodium chloride brine, and distilled water were made on reservoir-rock cores. Clay fractions were separated from sand grains of disaggregated portions of each core sample, and the clay minerals were identified by the differential thermal analysis method. Relations of the permeability to various fluids were developed.

Jan 1, 1957

By Gary P. Sames

This report discusses some practical applications of a geotechnical investigation conducted by the U.S. Bureau of Mines that can help mine operators meet revised Federal regulations in their roof control plans. The investigation, designed to characterize roof conditions near the coalbed outcrop in drift coal mines in eastern Kentucky, revealed that weathered stress-relief joints near outcrop are crucial ground control factors in the region. The joints' origin and character were determined through underground mapping of many joints in coal mine roof and detailed observations and measurement of joint trends and physical characteristics in widely separated strip mine highwalls and roadcuts. This resulted in an understanding of stress-relief-joint patterns and the effect of various rock types on the intensity of weathering in the joints. That information is used in this report to show how stress-relief joints contribute to roof failure and how, through improved roof support and mine planning, safer roof support plans can be developed.

Jan 1, 1992

By David A. Benjamin

The USBM (U.S. Bureau of Mines) studied mines, prospects, and mineralized sites in the Roberts WSA (Wilderness Study Area) in 1984. The 15,090-acre WSA, located 35 miles northwest of Eureka, NV, is underlain by alluvial deposits of Quaternary age, extrusive and intrusive volcanic rocks of Oligocene through Miocene age, and metasedimentary rocks of Cambrian through Permian age. The Roberts Mountain Thrust fault cuts through the WSA, dividing the metasedimentary rocks into upper and lower plate rock units. One mine, the Kelley, which produced 397 tons of lead-zinc ore prior to 1940, and two prospects are within the WSA; no resources were identified. Exploration for precious metal deposits is presently being conducted in and adjacent to the WSA on large claim blocks. The study area contains six sites in and near these claim blocks that have anomalous gold and silver. Detailed exploration is needed to delineate resources. High purity silica rocks are present in the WSA. Barite, phosphate, oil shale, and vanadium occurrences just outside the WSA may extend into it, but no such occurrences were observed during the USBM study.

Jan 1, 1986

By W. M. Dressel

A simple, reliable field test for beryllium in rocks has been developed by the Rolla Metallurgy Research Center of the Federal Bureau of Minas. A small portion of the pulverized rock is fused with a sodium carbonate-sodium hydroxide flux in a wire loop. The fused mass is dissolved in water, a few drops of quinizarin solution are added, and the solution is viewed under ultraviolet light. A pink-to-orange fluorescence reveals the presence of beryllium in a sample containing as little as 0.013 percent beryllium (0.26 percent beryl). INTRODUCTION New and potential uses for beryllium make necessary a more intensive search for this metal, which is so similar to aluminum in its chemical reactions that it is not separated from aluminum in ordinary chemical analyses. The principal ore mineral of beryllium is beryl, a beryllium-aluminum silicate, which contains only 5 percent beryllium. This mineral is so similar to quartz in appearance that it is not always possible to distinguish one from the other in the field. While the distinction may be made easily with a petrographic microscope, few prospectors have access to such an instrument, and fewer still know how to use it.

Jan 1, 1960

By M. R. Geer

The Bureau of Mines examined the washability data for 25 Appalachian coals requiring low-density washing to reduce sulfur content to 1 percent, using the distribution-curve method. The purpose was to estimate how closely theoretical sulfur values could be approached, what yields of washed coal could be expected, and the recovery efficiencies that might be achieved. Assuming that the run-of-mine coal would be crushed to 3/8 inch and cleaned in dense-medium cyclones, the calculations indicate that theoretical sulfur contents could be approached closely when cleaning at a specific gravity of separation as low as 1.30. With coals that have favorable specific gravity compositions the recovery efficiency anticipated for cleaning at 1.30 specific gravity is surprisingly high. Similar calculations for cleaning with concentrating tables at intermediate specific gravities indicated that theoretical sulfur contents at 1.50 specific gravity could be approached closely with some coals but not with others. The calculations suggest that operating a table at a specific gravity of separation much lower than about 1.50 probably would be unsatisfactory with most coals.

Jan 1, 1968

The National Institute for Occupational Safety and Health (NIOSH) recommends that occupational exposures to respirable coal mine dust and respirable crystalline silica* be controlled by complying with the provisions presented in this document. These recommendations are designed to protect the health and provide for the safety of workers exposed to respirable coal mine dust and respirable crystalline silica for up to 10 hr/day during a 40-hr workweek over a working lifetime. The information presented in this document demonstrates that underground and surface coal miners are at risk of developing simple coal workers' pneumoconiosis (CWP), progressive massive fibrosis (PMF), silicosis, and chronic obstructive pulmonary disease (COPD). Adherence to the recommendations in this document should prevent or greatly reduce the risk of adverse health effects in workers exposed to respirable coal mine dust and respirable crystalline silica. NIOSH recommends that preventive efforts be focused primarily on reducing worker exposures. Effective health and hazard surveillance and medical screening are also useful components of a comprehensive prevention effort.

Jan 1, 1997

By S. H. Brooks

"IntroductionThis preliminary report deals with the effect of oxygen pressure on the ignition temperature and combustibility of oils, it is the third of a series which will present the results of an investigation being made by the Bureau of Mines, on oxygen-oil explosions. The purpose of this research is to obtain technical data that will serve as a basis for safety precautions general outline of the problem has been given in the first report (Serial 2507).The present experiments have resulted in (1) a method for determining spontaneous ignition points of oils in an atmospheric of oxygen under pressure; and (2) the determination of these ignition temperatures for three typical oils, one being an animal oil (sperm), one a vegetable oil (linseed), and one a mineral oil (""Moiloil A"").These experiments on explosibility of oil were performed in order to discover the general nature of the phenomenon, especially the order of magnitude of the temperature necessary for spontaneous explosion (120°C. and upwards) and the effect of pressure variation (negligible as regards ignition temperature but important in relation to the violence of the explosion). A continuation oftests should provide a basis for selecting the safest lubricants for high pressure compression of gases particularly air and oxygen; and should be of value when devising new specifications for lubricants, both in the government departments and the compressed-gas manufacturing industry."

Dec 1, 1923

By Philip B. Lorenz

A Bureau of Mines feasibility study on the use of tracer pulses to assess the degree of fracturing in an underground formation consisted of three phases: 1. A laboratory study on sand packs and open tubes, which developed a correlation between dispersion of the pulse and size of the flow channels. 2. A test on a retort, 11 feet in diameter and 45 feet high, packed with shale rubble. Void volume was measured, but evaluation of channel size was not possible because of interference from the space unoccupied by the matrix. 3. A field test on an explosively fractured shale formation. Pressure, flow, and transit time led to qualitative estimates of fracture pattern, but quantitative detection of dispersion in the formation was overwhelmed by dispersion effects in the well.

Jan 1, 1973

By W. W. Adams

"The fifth annual National Safety Competition conducted by the United States Bureau of Mines to determine the best safety records at mines and quarries during the calendar year 1929 has been concluded, and the general results of the contest are presented herewith. To the winner in each of the five groups into which the contestants were divided there has been awarded the bronze trophy 'Sentinels of. Safety,' donated by the Explosives Engineer magazine. The trophy for bituminous coal mines was won by a mine in Alabama; that for metal mines by an iron-ore mine in Michigan; that for nonmetallic mineral mines by a salt mine in New York; that for quarries and open-cut mines went to a limestone quarry in Michigan;. the trophy provided for anthracite mines was, of course, won by a mine in Pennsylvania, as all of the anthracite mines participating in the contest are situated in that State.Winners of the trophies were selected by a committee of sward in accordance with rules governing the contest and on the basis of accident records furnished by the various companies to the Bureau of Mines. These records were summarized by the bureau and the results submitted to the committee. Members of the committee are W. H. Cameron, managing director of the National Safety Council. William Green, president of the American Federation of Labor; James F. Callbreath, secretary of the American Mining Congress; T. T. Read, Vinton professor of mining of Columbia University and editor of 'Mining and Metallurgy'; C. B. Huntress, executive secretary of the National Coal Association; A. J., Curtis, assistant to the general manager of the Portland Cement Association; A. T. Goldbeck, director of the engineering bureau of the National Crushed Stone Association.Thirty-four States were represented in the l29 contest. Among the plants which participated were 68 bituminous coal mines, 29 anthracite mines, 54 metal mines, 19 nonmetallic mineral mines, all of the foregoing being underground mines, and 141 quarries or open-cut mines. A total of 106,533,006 man-hours of work was reported by all of the companies. Accidents during the year numbered 7,008 and represented a period of disability equal to 986,306 man-days. Hence the accident-severity rate for all plants combined represented 9.3 man-days of disability for each thousand man-hours of exposure to hazard. Similarly, the combined accident-frequency rate for all plants showed that 66.3 accidents occurred for every million man-hours of exposure to hazard. Both of these rates indicated an improvement over the combined rates for all plants in the previous year's contest. The reduction in the accident-severity rate centered chiefly in the metal mine group, though all except the quarry and open-cut mine group shared in the reduction; the improvement in the accident-frequency rate was in all croups except anthracite and metal, the rate for the former having increased while that of the latter remained unchanged."

May 1, 1930

By H. E. Powell

The selective recovery of nickel and zinc from a waste phosphate solution by solvent extraction was investigated by the Bureau of Mines as part of a broad program to recover valuable metals and compounds from industrial wastes, and to reduce the associated land and water pollution caused by dumping these wastes. The waste, which resulted from the phosphation of automboile bodies, yielded 99 percent of both the nickel and the zinc by extraction with dinonyl naphthalene sulfonic acid (DNSA) and di-2-ethylhexyl phosphoric acid (EHPA), respectively. Dilute sulfuric acid was used to recover the metals and regenerate the solvents.

Jan 1, 1970

By J. W. Faul

[The Bureau of Mines initiated an extensive research on coal-mine ventilation factors in 1922, large- scale tests being conducted in its experimental nine near Bruceton, Pa., over a period of two years. A comprehensive report an this work is in course of preparation, but in order to place the practical results before the mining fraternity immediately and in condenses form, the more important features will be presented in a number of short papers. The present report is the first of a series dealing with the resistance of coal-mine entries to the flow of air and considers only entries in which there are no obstructions other than the natural roughness of the ribs, roof, and floor.]

Jan 1, 1924

By F. C. Gibson

An electrical method for the continuous determination of propagation velocities in opaque, confined explosives, and propellants is described. A resistance element imbedded in the reactive material generates electrical signals that are displayed oscillographically and indicate the position and progress of a reactive zone associated with progress of a reactive zone associated with burning or detonation. The method is applicable to both solids and liquids.

Jan 1, 1963

By C. A. Kumke

The Korean crisis and the cessation of Russian manganese-ore shipments to the United States in 1950 reemphasized the almost total dependence of the domestic steel industry on foreign supplies for metallurgical-grade manganese ore. In this emergency, Congress authorized the Bureau of Mines to undertake experimental mine and process development work on the known large reserves of low-grade manganese ore in the Artillery Mountains region in Mohave County, Ariz. The objective of the work was to obtain the basic mining and metallurgical data needed to make specific plans for initiating exploitation of the deposits within 3 years if high-grade foreign ore could not be obtained during the emergency. The manganese deposits of the Artillery Mountains region are in an area of about 25 square miles on the north side of the Bill Williams River in southern Mohave County. Lasky, of the Federal Geological Survey, has estimated reserves at 175 million tons of manganiferous material assaying 3.5 to 4 percent Mn. Although the man¬ganese occurs in various Tertiary and Quaternary formations as both bedded and fissure vein deposits, the more important syngenetic deposits are found in upper and lower manganiferous zones in the sedimentary beds of playa and alluvial fan origin that constitute the Chapin Wash formation.

Jan 1, 1957

By Jack E. Fraley

In this Bureau of Mines study, sealants containing mineral wool, cement, etc, were sprayed through dry-process equipment that propels dry material pneumatically to the water-adding nozzle. Advantages over slurry applications include no mixing, no extensive cleanup, and freedom from hardened cement in equipment should power be lost. Sealants with large mineral wool nodules (>l-inch) were sprayable at rates to 900 square feet per hour for 1/2-inch thickness with little dust and smooth material flow through equipment, but they were weak for mine use, Materials containing small wool nodules (1/4-inch) were stronger but tended to plug lines because the nodules were inadequately separated in the shredder. Increasing the dedusting oil also increased line plugging by holding the nodules together in larger lumps. Best results were obtained using a 3/4-inch-nodule wool with cement binder, which provided both smooth flow through the machine and adequate strength.

Jan 1, 1977

By K. J. Miller

Electrophoretic mobility measurements of coal and pyrite particles in distilled water revealed a difference between the migration speeds of the two materials toward the anode in a dc electric field. This information led to the development of a laboratory electrophoresis column for separating fine pyrite from coal by utilizing the electrokinetic and the specific gravity differences between coal and pyrite. The study demonstrated on a laboratory scale that pyrite and other impurities can be separated from fine coal by electrophoresis using a stage separation technique. In a cost analysis, electrical power for electrophoresis was extrapolated to about $1 per ton of clean coal product. But, since the only successful tests ever made were in the laboratory with prewashed samples of minus 100-plus 325-mesh coal in distilled water, the cost figure derived is not representative of conditions prevalent in commercial coal cleaning operations. True conditions would reflect costs many times as great. In the course of the work, several scale-up techniques were considered but their feasibility became academic in view of the physical and economic problems associated with electrophoretic separation of pyrite from coal. Although the process and apparatus were finally deemed impractical for commercial coal preparation, the electrophoresis column may have some application as a laboratory device.

Jan 1, 1974