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By T. O. Llewellyn

The Bureau of Mines, U.S. Department of the Interior, conducted studies to recover phosphate from four dolomitic southern Florida deposits not currently mined. The samples contained 5.8 to 10.2 percent P205 and 1.7 to 1.8 percent MgO. Chemical analyses of sized fractions indicated that no pebble concentrate (plus 1.2 mm) could be produced from these samples. A scheme was developed that consisted of desliming, grinding, scrubbing, and redesliming the ore to produce a flotation feed. Conventional one-step fatty acid-fuel oil batch flotation tests on the samples resulted in concentrates containing 29.0 to 31.3 percent P205 at flotation recoveries ranging from 72.4 to 96.1 percent of the flotation feed. The MgO content of the concentrates ranged from 0.47 to 1.36 percent. Continuous flotation of the Manatee No. 2 sample indicated that commercial-grade phosphate concentrates analyzing 31.3 percent P205 and 0.55 percent MgO could be produced with a flotation recovery of 89.9 percent. The MgO content of concentrates obtained from the Manatee No. I and Hardee samples was 1.20 to 1.36 percent, respectively. Leaching with aqueous SO2 reduced the MgO content of these phosphate concentrates to 0.5 and 0.8 percent, but with a concomitant loss in phosphate recovery.

Jan 1, 1983

By Victor Costa de Mello Vasconcelos

O objetivo desse projeto é a preparação nanofolhas de óxido de níquel por calcinação e a formação de híbridos com nanopartículas esféricas de ouro e paládio. O trabalho focou na síntese de materiais com forma e tamanho controlados por meio de metodologias simples e ambientalmente amigáveis e na preparação de estruturas híbridas com dispersão uniforme entre componentes. Foram obtidos hidróxidos, óxidos e híbridos, cujos parâmetros de síntese (como temperatura, tempo de reação, entre outros) foram estudados. Uma vez caracterizadas, empregaremos as estruturas do tipo M/NiO (M = Au, Pd) como catalisadores nas reações modelo de oxidação do álcool benzílico e de redução do 4-nitrofenol, com o intento de estudar a natureza da interação metal-suporte.

Oct 30, 2017

By Jon Pocock, Ashma Singh

The traditional approach for the beneficiation of South African siliceous sedimentary phosphate ores has been reverse cationic flotation. The robustness of this approach, however, has been a concern due to its sensitivity to parameters such as slimes content, headgrade ( P2O5 and SiO2 content), reagent dosages and conditioning times. The phosphate mineralisation for the ore body under investigation is predominantly carbonate fluorapatite composed of mainly quartz and apatite and minor amounts of chlorite, ilmenite and carbonates. Beneficiation of low grade sedimentary ores containing calcareous impurities, such as calcite and/or dolomite in addition to siliceous gangue, is required to meet the increasing demand; therefore, much research has been carried out to find an alternative technique to beneficiate this material. This paper investigates traditional flotation approaches versus the currently adopted ‘Crago Process’. Comparative results are presented in terms of upgrade potential for the production of concentrate rock for downstream applications. The novelty of the ‘Crago Process’ lies in its double stage approach, i.e. direct fatty acid flotation followed by reverse cationic amine flotation. The Crago process was able to achieve higher upgrades reporting at 32.1% P2O5 compared to conventional cationic flotation only achieving grades of 18.5% P2O5. Furthermore, the recovery gain was 3%.

May 13, 2023

By Robert P. Kennedy, Andrew H. Merritt, Edward J. Cording, Thomas R. Kipp

INTRODUCTION Measurement of certain data associated with nuclear testing necessitates the reception of waves at the instrument location which are unaffected by reflection off internal structures or tunnel surfaces. Therefore, in order to provide necessary facilities for the fielding of experiments in support of the underground nuclear testing program, the Defense Nuclear Agency (DNA) commissioned a cost and feasibility evaluation pertaining to the design and construction of large underground cavities in Rainier Mesa. The effort included research into past experience pertaining to the excavation and support of large underground caverns, assessment of the geological conditions which exist in Rainier Mesa, preliminary design of the chambers and their rock support systems based upon the geological setting, development of mining plans for the excavation of the caverns, and estimation of the cost and manpower schedule to complete construction. This paper summarizes the results of the feasibility evaluation. The investigation was limited to modified hemispherical configurations ranging in size from 24.4 to 91.4 m (80 to 300 ft) in diameter. Two cavity support systems were considered. The first employs internally installed rockbolts as the means of primary rock support while the second involves the use of annular tendon galleries located above the chambers from which primary support members are introduced prior to general excavation. The internal support configuration was considered for cavities with spans of 24.4, 36.6, 48.8, and 54.9 m (80, 120, 160, and 180 ft) while the external support configuration was considered for cavities with spans of 54.9, 73.2, and 91.4 m (180, 240 and 300 ft).

Jan 1, 1979

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Jan 1, 1980

By Leticia Costa Macêdo

Esse trabalho tem como objetivo analisar por meio da termodinâmica computacional a influência do K2O na dissolução das fases sólidas formadas durante o processo de dessulfuração de ferro gusa. Para isso, foi utilizada a cal como agente dessulfurante e a Sodalita (Fonólio) como fundente, realizando uma adição de K2O no fluxante de 1% a 10%, com uma temperatura de trabalho de 1400ºC. Por meio do uso de software de termodinâmica computacional FactSage, foi possível simular e avaliar as fases sólidas e líquidas formadas na temperatura determinada e comparar com os resultados obtidos com outras análises. Os resultados obtidos mostraram que o aumento gradativo de K2O levam a um aumento do potencial termodinâmico de dessulfuração e melhores condições cinéticas, sendo a mistura que apresentou os melhores resultados a que continha 10% de sodalita com adição de 10% de K2O na fonte.

Oct 30, 2017

The Rosebery and Hercules mines, situated in the Rosebery-Williamsford district in western Tasmania, have a history of production dating back to 1896-7, although full scale production did not commence until 1936, following the development of a satisfactory process of selective flotation (Hall, Cottle, Rosenhain and McGhie, 1953). The mineral composition of the Rosebery zinc-lead ores was first described in detail by Stillwell (1934). The Hercules ore is generally similar, but as yet no descriptions of it have beenpublished.Since Dr. Stillwell's paper appeared, the management of the Rosebery and Hercules mines has from time to time submitted a number of interesting mineral specimens to C.S.I.R.O. Mineragraphie Investigations. Examination of these specimens brought to light eight minerals, some relatively uncommon, not previously recognized in these ores.They are cassiterite, molybdenite, stannite, electrum, meneghinite, boulangerite, pyrargyrite and pyrrhotite. Some of the specimens are also rich in tetrahedrite and gold. In addition each of the other ore minerals described by Stillwell, viz. pyrite, sphalerite, galena, bournonite, chaleopyrite and arsenopyrite, was detected in one or more of the specimens examined during the present study. The principal gangue minerals were found to be quartz, manganiferous carbonate, sericite and barite, agreeing closely with the observations of Stillwell.The present study was based on the examination of the following eight specimens.

Jan 1, 1960

By Marcos Meyer

A pelotização é um processo de aglomeração com objetivo de agregar valor aos finos de minérios de ferro (pellet feed). A partir de 2010, a mina de Brucutu situada no Quadrilátero Ferriferro (QF) passa a ser a maior fornecedora de matéria prima para as plantas de Tubarão / Vitória-ES. O estudo avaliou a performance industrial de duas misturas com alta participação de minério de Brucutu, acima do padrão utilizado na usina de pelotização. Os minérios compostos nas misturas foram caracterizados por análise química, física, mineralógica e microestrutural. O desempenho operacional mostrou superior à mistura padrão utilizada para a produção de pelotas para redução direta, permanecendo com os parâmetros de qualidade consoantes com as especificações do produto final. O conhecimento das características geometalúrgicas destas misturas com minério de Brucutu em maior escala foi de suma importância para adequar o processo e custo das principais operações unitárias da planta envolvida (moagem e forno).

Aug 1, 2018

By J Nell, J Petersen, X C. Goso

The feasibility of increasing the deportment of titanium species and the stability of the pseudobrookite solid solution (M3O5) in a titaniferous slag was investigated, to facilitate the valourisation of titaniferous slags. Thermochemical simulations using FactSage™ software, ver 8.3 (by Thermofact/CRTC and GTT-Technologies), and equilibration-quench experiments were conducted using an appropriate synthetic titaniferous slag composition in an oxygen partial pressure (pO2) ranging from air to 10-16 atm under non-isothermal conditions. The temperature-pressure phase stability diagram for the synthetic slag containing 37.19 per cent TiO2, 19.69 per cent SiO2, 13.12 per cent Al2O3, 16.00 per cent CaO and 14.00 per cent MgO showed that the spinel solid solution (M3O4) was the primary phase until a pO2 of 10-10.5 atm, thereafter M3O5 was the primary phase until a pO2 10-13.2 atm. M3O4 again was the primary phase between a pO2 10-13.2 and 10-16 atm. The changeover of the primary phase coincided with an increase in the liquidus surface. When cooling the slag in a pO2 of 10-16 atm, M3O5 crystallised as a ternary phase that showed a rapid increase in mass while that of the primary M3O4 phase decreased and that of the secondary perovskite (CaTiO3) phase increased at a slower rate. At 1300°C under sub-liquidus conditions, the contents of M3O5, M3O4 and CaTiO3 were about 20 per cent, 15 per cent, and 11 per cent, respectively. Experimental results showed that the Ti3+/Ti4+ mass ratio in the M3O5 phase, ie a measure of the reduction of titanium species, is not considerably sensitive to equilibration temperature in the reviewed range. Slow cooling and minimum/no oxidation during cooling of titaniferous slag would increase the deportment of titanium species to, and the growth and stability of the M3O5 phase.

Jun 19, 2024

By A. E. Wells, H. O. Hofman, R. P. Reynolds

A Discussion of the Paper of H. O. Hofman, R. P. Reynolds and A. E. Wells, read by title at the London Meeting, July, 1906 ; presented at the New York Meeting, April, 1907, and printed in Bi-Monthly Bulletin, No. 13, January, 1907, pp. 37 to 52. GEORGE A. PACKARD, Boston, Mass. (communication to the Secretary*) :-The very interesting results obtained by Prof. Hofman and his assistants came to my attention when I had temporarily assumed charge of the metallurgical department of the Missouri School of Mines, and had found it, pending the completion of a new building, lacking a furnace in which to roast ore preparatory to the customary lead blast-furnace run. An attempt at lime-roasting had been already determined upon, but the use of a charge which would make a slag of definite composition was a new idea. The results following were obtained by Messrs. Aubrey Fellows, J. C. Long, E. R. Wash, and Dr. T. C. Tseung, under my supervision. It is regretted that the data are not more complete; but the work was done simply incidentally to securing the desired ore for the blast-furnace, with no idea of obtaining any results of especial interest. It is submitted because of the metallic lead obtained, no notice of which has been seen elsewhere. The ore was an aggregate of several lots of concentrates, apparently from Missouri ores. The analysis follows, with that of the limestone and sandstone used, as far as made:. Ore, SiO2, 3.04; Fe, 0.77; CaO, 2.53; Pb, 68.74; Zn, 5.77; S, 13.9 per cent.; limestone, SiO2, 1.0 ; CaO, 54.35 per cent.; sandstone, SiO2, 99.8 per cent. The converter was made in the shops from a sheet of No. 14 iron riveted in the shape of a truncated cone, 20 in. in diameter at the top, 15 in. at the bottom and 22 in. high. A grate of No. 8 iron, 17 in. in diameter, with 130 s-in. holes placed at about 1.25-in. centers, was held in place by the shape of the

Jul 1, 1907

By Luiz Alberto dos Santos

Neste trabalho foram usinados CDPs da liga com composição de 50,9 % at de Ni e, em seguida, as amostras foram envelhecidas em temperaturas entre 350-550 ºC, tensões aplicadas de 60 MPa e tempos de 45 e 180 minutos. Além disso, foram realizados também envelhecimento sem aplicação de carga nas mesmas condições de temperatura e tempos para comparação das propriedades, porém acrescentando uma amostra solubilizada a 850ºC durante 1 hora. Posteriormente as amostras foram caracterizadas por DSC para determinação das temperaturas de transformação de fases. Observa-se neste trabalho que o DSC de algumas amostras apresentou tanto no aquecimento quanto no resfriamento dois picos de transformação que pode estar relacionado ao aparecimento da fase R. Além disso, pode ter ocorrido a formação da fase Ni3Ti4, pois ligas com teores acima de 50,6 %at. de Ni são caracterizados pela formação de precipitados ricos em Ni, que pode acarreta na diminuição da concentração de Ni na matriz e aumento da temperatura de transformação. Este trabalho é importante, pois há poucos estudos relacionados com o efeito do envelhecimento sob carga nas propriedades de efeito de memória de forma e superelasticidade da liga NiTi.

Aug 16, 2017

By M. C. Amiri

The plant produces 130 kg slag per tonne of crude steel, to add to the basic oxygen steel-making converter slag stockpile of around 2 500 000 t. The slags contain 1.81% V2O5, which can be rendered water-soluble by salt roasting with NaCl and an alkali such as Na2CO3. Preliminary tests gave less than 3% V recovery from slag under optimum roasting conditions when NaCl, NaCO3 or Na2SO4 was used, but showed that sodium phosphate could make all the V water-soluble when roasted with slag in a ratio of 3:1 at 1 100-1 200 degrees C. Almost complete leaching was obtained within 2 h with water at boiling point. Sodium vanadate was precipitated by acidifying the leach liquor with HCl to a pH of about 2.2

Jun 21, 1905

By Graham Holmes, John Starkey

"The Kinross Kubaka Project is a gold mine located in the Russian Far East. The grinding circuit, comprised of a 6.1 m diameter x 2.74 m long SAG mill and a 4.1 m diameter x 5.5 m long secondary ball mill in closed circuit with cyclones, was built using SAG Power Index and Bond Ball Mill Work Index testing to determine the grinding energy requirements. Extremely cold climatic conditions and the need to keep heated space and capital costs to a minimum, dictated a grinding circuit with no in-circuit crusher and no conveyors external to the mill. High energy requirements for both the SAG mill and the ball mill were correctly predicted and have allowed grinding production tonnage forecasts to be met. Design test data and production results are given.INTRODUCTIONIn 1995 Davy International Canada, now Kvaerner Metals E & C, was commissioned as the Engineer and Project Manager for the Omolon Gold Mining Company, to design and construct a gold extraction plant for the Kubaka gold deposit, located in the Russian Far East. This deposit had been studied extensively in Russia during the exploration phase and a Feasibility Study was completed in 1993 by Kilborn who visited the site twice during that year to inspect facilities and to take metallurgical test samples. More samples were taken in 1995 to check ore hardness variability, as part of the final design program by Davy.The client’s objective in designing the Kubaka grinding circuit was to achieve design tonnage at all times, even when milling the hardest ore zones in the deposit. Since the samples taken in 1993 were taken as composite samples, it was necessary to take additional samples in 1995 to determine the extent of the variability. Six samples were sent to Canada for SAG Power Index (SPI) testing. Five of these were combined as a composite open pit sample, while the sixth sample was taken from the site adits as a composite sample to represent undergound ore. These two composite samples were tested to determine the MacPherson Autogenous Work Index for comparison with the SPI values."

Jan 1, 2001

By D. R. Lentz, S. H. Mcclenaghan, J. A. Walker

"Abstract - The Orvan Brook deposit is one of several (Zn+Pb>>Cu)-rich sulfide deposits hosted by the Spruce Lake Formation (California Lake Group) in the northwestern part of the Bathurst Mining Camp. This parautochthonous deposit is hosted by a narrow band of highly deformed, locally graphitic shale that appears to conformably overlie felsic volcanic rocks of the Spruce Lake Formation, and is in tectonic contact with overlying mafic volcanic and related sedimentary rocks of the Canoe Landing Lake Formation. The Spruce Lake Formation is dominated by felsic volcanic rocks and subordinate fine-grained sedimentary rocks, and mafic volcanic rocks (Canoe Landing Lake member). The felsic volcanic rocks can be divided into aphyric and feldspar-phyric rock types. The feldspar-phyric rocks and a few of the aphyric varieties have a Zr/TiO2 ratio of 0.06, and fall into the California Lake Group field on a Y/TiO2 versus Zr/TiO2 diagram. In contrast, the aphyric felsic volcanic rocks have Zr/TiO2 ˜ 0.09 and are marked by high Zr and Th, which is consistent with highly fractionated felsic magma of Spruce Lake affinity. Major and trace element analyses of host rocks suggest that weak to moderate hydrothermal alteration developed on the south side (stratigraphic footwall) of the deposit, which is consistent with a north-younging succession. The sulfide lens strikes east-west for approximately 2.3 km, extends down-dip for at least 500 m locally, and has an average thickness of between 0.75 and 1 m, but is locally up to 5.5 m thick. The contacts of the massive sulfide lens with its host rocks are invariably sharp. Host rocks show evidence of intense ductile deformation as well as later brittle deformation. Compositional layering and sulfide breccia textures in the sulfide body are interpreted to result from deformation or tectonic enhancement of original primary layering. The deposit contains an estimated resource of 2.69 Mt grading 1.73% Pb, 5.95% Zn, 0.37% Cu, 72 g/t Ag, and 0.9 g/t Au. Similarities in bulk d34S between the Orvan Brook (+8.6‰) and the nearby Cu-rich McMaster deposit (+8.2‰) suggest a common depositional setting."

Jan 1, 2006

By Adelson Goncalves

No processo de extração mineral, a perfuração de rocha é uma atividade essencial. Por isso, a redução de custo com materiais de desgaste é sempre um desafio para todos no campo da mineração. A partir desse desafio, o grupo de melhoria contínua Perfuração desenvolveu um projeto que visa redução de custo com hastes para perfuratrizes de grande porte. A metodologia aplicada para elaboração do projeto foi o PDCA, onde foi desenvolvido uma forma de reaproveitar o corpo da haste, que evita o descarte precoce da peça, otimizando a vida útil e consequentemente reduzindo o custo com materiais de desgaste de perfuração.

Aug 17, 2017

By Albert L. Toenges, Frank A. Jones

"INTRODUCTION The introduction of mechanized pining in coal mines, which has speeded loading, has emphasized the importance of efficient underground transportation systems. The purpose of this investigation is to study and analyze various systems now in use, and to derive conclusions therefrom. This report may be helpful to operators who are planning new systems of transportation or who are revising present systems to increase their efficiency. This paper is the first of a series on this subject and describes some systems of transportation utilizing rail haulage.ACKNOWLEDGMENTThe information used in preparing this report was obtained through the courtesy and cooperation of the officials of the companies whose mines wore studied. The descriptions of the transportation systems at the mines included herein have been checked for accuracy, and publication of the data has been approved by the executives of the several operating companies."

Jun 1, 1940

By Raelly Laurinda Araujo da Silva

As ligas de alumínio são utilizadas mundialmente em inúmeras atividades. Com o aumento da competitividade, existe a necessidade de melhoria constante no processo produtivo. Essas melhorias têm como objetivo reduzir custos e melhorar o desempenho dos componentes e têm sido realizadas pela aplicação de novas técnicas e pelo desenvolvimento de novas ligas/composições. O processo squeeze casting é um processo inovador dentro dos processos de fundição, no qual o metal vazado no estado liquido é solidificado sob pressão dentro de uma coquilha metálica fechada por um punção. Neste contexto, o presente trabalho buscou analisar a influência da aplicação de diferentes pressões no processo de squeeze casting na modificação estrutural da liga de alumínio do tipo AlSi1Mg0.5Mn. Os resultados indicam que o aumento da pressão na liga gera uma taxa de transferência de calor mais elevada que reduziu o tempo de solidificação modificando a microestrutura.

Oct 30, 2017

By Mauro Vivaldino Fernandes

Os desafios para o aprimoramento do desempenho operacional dos altos-fornos constituem um campo aberto para o desenvolvimento e aplicação de métodos de controle que promovam a otimização da operação do reator, aliada ao prolongamento da sua vida útil. O Alto-Forno 3 da Usiminas - Ipatinga, nesta sua 4ª campanha, foi projetado para 15 anos de operação, com uma produção estimada de 41 milhões de toneladas de gusa. Os resultados da campanha atual, em termos de produção e de duração da campanha, superam os dados projetados. Neste contexto, são apresentadas as principais características do Alto-Forno 3 na sua atual campanha, a evolução do seu desempenho em termos de produtividade e tempo de operação, além das principais ações direcionadas para a preservação e estabilidade do sistema de refrigeração e do cadinho, contribuindo para o prolongamento da sua vida útil. Como resultado destes esforços, a vida útil estimada do Alto-Forno 3 é de 22 anos, superando em 7 anos a duração prevista.

Oct 30, 2017

By P. K. Koh, H. A. Lewis, H. F. Graff

New data on the distribution of silicon between slag and carbon-saturated iron at 1600Oand 1700OC are presented which, in combination with previously published data, permit the determination of silica activities over a broad range of compositions in the CaO-Al2O3-SiO2 system. The distribution of silicon between graphite-saturated Fe-Si-C alloys and blast furnace-type slags in equilibrium with CO has been described in previous publications.1"3 In this past work the silica-silicon relation was established at temperatures of 1425" to 1'700°C for slags containing up to 20 pct A12O3. This paper presents the results of additional studies at 1600" and 1700° C which extend the silicon distribution data at these temperatures for CaO-A12O3-SiO, slags over a range from zero pct Al2O3 to saturation with Al2O3, or CaO.2Al2O3. The upper limit of SiO2 is set by the occurrence of Sic as a stable phase when the metal contains 23.0 or 23.7 pct Si at 1600" or 1700°C, respectively. The activity of silica over the expanded range is determined directly from the distribution data.3 Recently4-7 other investigators have studied the activities of SiO, and CaO, principally in the binary system, using different methods and obtaining somewhat different results. EXPERIMENTAL STUDY The experimental apparatus and procedure have been fully described in previous publications.1, 3 Six new series of experimental heats have been made, four at 1600° and two at 1700°C. Master slags of several fixed CaO/Al203 ratios were pre-melted in graphite crucibles, and these were used with additions of silica to prepare the initial slag for each experiment. Slag and metal were stirred at 100 rpm and CO was passed through the furnace at 150 cc per min. The initial sample was taken 1 hr after addition of slag at 1600°C or 1/2 hr after addition at 1700°C. The run was normally continued for 8 hr at 1600°C or 7 hr at 1700°C, and the final sample was taken at the end of this period. Changes in Si and SiO2 content indicate the direction of approach to equilibrium, and in a series of runs where the approach is from both sides this permits approximate location of the equilibrium line. Fig. 1 shows the results of such a series of 15 runs at 1600°C for slags of CaO/Al,O3 = 1.50 by weight. Figs. 2 and 3 record other series at 1600°C and Fig. 5 a series at 1700°C with fixed CaO/Al0 ratios. The results of the experiments at 162003°C have been reported in part in a preliminary note.3 In the experiments recorded in Figs. 4 and 6, the slags were saturated with A12O3 (or with CaO.2A12O3 within its field of stability) by suspending a pure alumina tube in the melt during the course of the run. The final slag analyses were used to establish the liquidus boundaries8 in the stability fields of CaO.2Al2O3 and of Al20,. ACTIVITY OF SILICA The free-energy change in the reaction has been calculated by Fulton and chipman2 from recent and trustworthy data including heats of formation, entropies, and heat capacities. The more recent determination by Olette of the high-temperature enthalpy of liquid silicon is in satisfactory agreement with the values used and therefore requires no revision of the result which is expressed in the equation: SiO2 (crist) + 2C (graph) = Si + 2CO(g.) [1] &F° = + 161,500 - 87.4T The standard state for silica is taken as pure cristobalite and that of Si as the pure liquid metal. Since the melts were made under 1 atm of CO and were graphite-saturated, the equilibrium constant for Eq. [I] reduces to K1 = asi /asio2. The value of this constant is 1.77 at 1600°C and 16.2 at 1700°C. Through K1, the activity of silica in the slag is directly related to the activity of silicon in the equilibrium metal.

Jan 1, 1960

By Marcos Paulo Kohler Caldas

O desenvolvendo da indústria de eletroeletrônicos associada ao barateamento dos produtos tem reduzido a vida útil de equipamentos levando a uma geração elevada de resíduos de equipamentos eletroeletrônicos (REEE). Um componente desse resíduo são as placas de circuito impresso, que possuem em sua composição altos teores de metais, que podem ser recuperados através de processos de reciclagem. O presente trabalho busca caracterizar placas mãe de computador, determinando sua quantidade de material orgânico, cerâmico e metálico. As placas foram direcionadas para cominuição, que foi realizada em moinho de facas com grelha de 9mm, seguida por um moinho de martelos, atingindo uma granulometria menor que 2mm. A amostra foi então quarteada, para uma maior homogeneização e passou por ensaio de digestão em água régia. O licor resultante foi diluído para determinação do teor dos metais Ag, Al, Au, Ba, Ca, Cu, Fe, Ni, Pb, Sn, e Zn utilizando espectrometria de emissão óptica por indução de plasma (ICP-OES). O sólido filtrado, também resultante da digestão em água régia, passou por um ensaio de perda ao fogo a 800°C por uma hora, para determinar o teor de material orgânico. Os resultados indicaram que o Cu é o metal de maior concentração com 22,5% na placa de circuito impresso e que a mesma possui 43,7% de metais, 31,9% de polímeros e 24,4% de cerâmicas. A prata representa 0,04% dos metais e sua obtenção será realizada na forma de nanopartículas a partir de rotas hidrometalúrgicas.

Aug 8, 2018