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By A. Dale Marcy, Pamela L. Drake

Workers who perform routine welding tasks are potentially exposed to fume that may contain manganese. Manganese may cause respiratory problems and is implicated in causing the occurrence of Parkinson-like symptoms. In this study, a field colorimetric method for extracting and measuring manganese in welding fume was developed. The method uses ultrasonic extraction with an acidic hydrogen peroxide solution to extract welding fume collected on polyvinyl chloride filters. Commercially available pre-packaged reagents are used to produce a colored solution, created by a reaction of manganese(II) with 1-(2-pyridylazo)-2-naphthol. Absorbance measurements are then made using a portable spectrophotometer. The method detection limit and limit of quantification (LOQ) were 5.2 mg filter-1 and 17 mg filter-1, respectively, with a dynamic range up to 400 mg filter-1. When the results are above the LOQ for the colorimetric method, the manganese masses are equivalent to those measured by the International Organization for Standardization Method 15202-2, which employs a strong acid digestion and analysis using inductively coupled plasma-optical emission spectrometry.

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

C. 4 Hoist Assemblies (not man-rated) A large number of manufacturers supply materials handling winches. These units are predominately electric powered while a limited number of vendors supply air powered equipment. Air powered units are currently used extensively for underground materials handling purposes. Suppliers of materials handling equipment normally include a disclaimer statement in their published literature which clearly states that the equipment "is not designed or suitable for lifting or lowering persons " This category of commercially available equipment can be adequate for emergency man hoisting provided that its' capacity is suitably derated and provided also that the necessary safety features are incorporated. Section C. 5 details the equipment which could be added to a commercial materials hoist to meet these needs. Four commercially available hoist assemblies, two electric and two pneumatic are discussed in the following paragraphs. This equipment is typical of what is commercially available and three of the units are currently used extensively in mining applications. Each hoist description includes a remarks paragraph which identifies the additional equipment each hoist would require for emergency hoist use.

Jan 1, 1976

By Harold W. Lipper

A NEW record was set for helium shipment in 1962 for the 13th successive year. For the first time since 1949, the production of helium from natural gas at Bureau of Mines plants was less than in the previous year. The Bureau shipped 599.5 million cubic feet, 9 percent more than the 1961 volume, and produced 680.9 million cubic feet-a decrease of 6 percent from the record set in 1961. The Bureau added 77.2 million cubic feet to the volume stored for future use. Of the total 524.6 million cubic feet in storage, 522.4 million cubic feet is accumulated excess production from Bureau of Mines plants. The remaining 2.2 million cubic feet was purchased during 1962 from industry under the helium conservation program. The first two of five private plants began production in December to recover helium for conservation storage and ultimate use. A 425-mile pipeline system to transport helium from the five private plants to the Cliffside field was constructed by the Bureau at a cost of about $8 million.

Jan 1, 1963

By W. H. Pailes, V. Castranova, D. Lewis, G. Goodman

We performed bronchoscopy with bronchoalveolar lavage (BAL) in 8 control subjects with no exposure to occupational dusts, 8 healthy power plant workers exposed to mixed dusts (primarily fly ash), 1 healthy coal miner and 1 rock driller with acute silicosis. All subjects were non-smoking males. We analyzed lavage effluents for total numbers of alveolar macrophages, lymphocytes and neutrophils and monitored chemiluminescence at rest (REST CL) and after stimulation with 3x10- M phorbol-12-myristate-13-acetate (PMA CL) or 2 mg/ml zymosan (ZYM CL). The data are as follows:

Jan 1, 1988

By E. P. Youngman

The mining laws referred to by those who furnished the reports mentioned in the preceding paragraph are : General Austrian Mining Law of 1854 and the Law of 1868 , which prescribes for Hungary (as well as for Transylvania ) the full text and decisions of the General Austrian Mining Law; Government Decree 18346 , 1859 ; Parliamentary Decree of 1861 ; the Law of 1871 ; the Commercial Code , Law 37 of 1875 ; the Industrial Lar of 1884 ; the Law of 1386 ; the Decree of the High Court of Justice , 5540 , of 1399 ; Laws 6 and 7 of 1911 ; Law of 1921 ; Laws 23 and 24 of 1922 ; Laws 5 and 21 of 1927 ; and Law 40 of 1928. ( Lev 21 of 1927 and Law 40 of 1928 are labor laws . ) A compilation of the mining laws of Hungary , " Magyar Banya Jog , " or the " Hungarian Mining Law, " was made use of in part . This volume is the second edition of a school textbook , which ras prepared by Dr. Bela Balkay and Dr. Imre Szeoke , and which was published by the Apollo Press ( V. , Sas -utca 13 , Budapest ) in 1909 .

Jun 1, 1931

By J. E. Chilton, C. R. Carpenter

The U.S. Bureau of Mines has developed an intrinsically safe carbon monoxide (CO) monitoring system for mines by coupling a fiber-optic data telemetry (FODT) system with a prototype electro- chemical CO monitor. The CO monitoring system can be used in a coal mine as one component of an early fire warning system. This system may be used in belt haulage entries when the entries are used for supplying ventilation air to working places. The FODT accepts a 0.1- to 1.1-V analog signal from the monitor and converts it to pulses (0 to 5 V) at frequencies from 1.1 to 11 kHz that drive a light- emitting diode (LED). An electrically nonconducting fiber-optic cable carries the LED signal to a remote receiver. The receiver analyzes the incoming light signal and displays the measured CO concentration in parts per million. This report discusses the performance of the FODT system and characteristics of the CO monitor such as response times, linearity, and temperature and pressure effects.

Jan 1, 1992

By David Hoadley, Kenneth R. Maser, Ashok B. Boghani, James E. Billar, D. Randolph Berry, Mackenzie Burnett, Robert H. Trent

APPENDIX F GOVERNMENT OFFICES CONTACTED DURING SURVEY 1. MESA Inspection Offices North Central District Duluth, Minnesota South Central District Dallas, Texas Rolla Subdistrict Rolla, Missouri Rocky Mountain District Lakewood, Colorado Salt Lake City Subdistrict Salt Lake City, Utah Spokane Field Office Spokane, Washington Osburn Field Office Osburn, Idaho Phoenix Subdistrict Phoenix, Arizona 2. MESA Research and Management Denver Technical Center Denver, Colorado Pittsburgh Technical Center Pittsburgh, Pennsylvania Metal and Non-Metal Office Washington, D C 3. State Offices (State plan States) Arizona State Mine Inspector Phoenix, Arizona New Mexico State Mine Inspector Albuquerque, New Mexico

Jan 1, 1976

By R. V. Holmes

The properties of the Colorado Copper Co. in Sinbad Valley, Mesa and Montrose Counties, Colo., were rehabilitated and sampled by the Bureau of Mines in October, November, and December 1942. The several deposits were reexamined in March and April 1945 to obtain information disclosed by company work after December 1942. The development program included surface trenching, rehabilitation of several edits, and channel sampling of the exposures. Assay determinations wore made on 204 samples from the surface and underground workings. The results are given in the appendix. Several copper deposits in the Sinbad Valley area are similar in origin. The host rocks are sedimentary and mice in age from Pennsylvanian to Cretaceous. The Colorado No. 3 deposit occurs in the Cutler formation, which consists of many small lenses of conglomerate, sandstone, and shale. Mineralization is closely associated with faulting. On the Pyramid group the enrichment occurs in a zone of fracturing and jointing end also spreads into the adjoining sandstone. The ore deposition on the Copper Rivet claim is associated with a fault zone and is confined to en area above the contact of the Dolores-Wingate formations. Mineral deposits on the Sinbad claims occur at intersections of faults with blue-gray Pennsylvania limestone. Copper enrichment occurs along faults and as replacement of the surrounding limestone. Metallurgical tests indicate that ores from the Colorado No. 3 and Pyramid claims can be treated successfully by leaching with sulfuric acid. This method cannot be applied to ores from the Copper Rivet or Sinbad deposits because of high calcite content. Flotation tests at Boulder City, Nev., showed a recovery of less than 60 percent with a 14.24 percent copper concentrate.

Jan 1, 1952

By S. C. Termes, P. E. Richardson, R. L. Wilfong

"The Bureau of Mines conducted research on the flocculation of various minerals with insoluble cross-linked starch xanthate (ISX) to determine its potential as a beneficiation technique for low-grade, highly disseminated ores and for selective desliming. Covellite, chalcocite, pyrite, pyrrhotite, chalcopyrite, bornite, sphalerite, galena, and molybdenite fines flocculate with ISX. Floc formation, floc size, and settling rate are dependent on pH, with the pH dependence differing for each mineral. Quartz is not flocculated by ISX. Experiments to obtain selective flocculation of sulfides from quartz were attempted. Good selectivity was only obtained for the bornite-quartz system. Post flocculation separations resulted in flocculated bornite in grades as high as 92 pct. Evidence is presented that the flocculation of many of the sulfide minerals with ISX may involve covalent bonding of the xanthate group to lattice metal site(s). INTRODUCTIONBecause of the increasing interest in selective flocculation as a beneficiation technique for low-grade, highly disseminated ores and for selective desliming, the Bureau of Mines has been investigating the flocculation behavior of several cross-linked starch derivatives containing chelating groups. This report dis cusses the flocculation of sulfide mineral fines by insoluble cross-linked starch xanthate (ISX).Polymeric materials such as ISX, which contain a chelating group of known re¬activity towards specific mineral surfaces, were first proposed by Slater, Clark, and Kitchener (1), 3 Kitchener (2), and Attia and Kitchener (3) as selective flocculants for mineral fines with particle aggregation possible through a bridging mechanism. ISX appeared to be attractive as a sulfide mineral flocculant because (1) alkyl xanthates are known to react selectively with sulfide minerals"

Jan 1, 1983

By D. B. Dow

The study of oil production methods with reference to the amount of oil originally pressent in the oil-bearing, formations has developed the fact that-ordinary methods-of production remove only a part of the oil actually present. In fact, it is generally realized that when a field is abandoned more oil remains in the sand than has ever been removed. As a consequence of this realization, the petroleum engineer has devoted considerable tine in recent years in devising methods for increasing the percentage of recovery. His studies have indicated that in most cases the total production of a field is dependent upon the available gas rather than upon the available oil. Mien the gas in the sand is exhausted, oil production ceases even though there may be enormous quantities of oil remaining unrecovered. Consequently, any method of conserving the gas or increasing the supply of gas will increase the ultimate recovery from a field. The practice of producing oil under vacuum increases the effectiveness of the gas remaining in the sand, as well as furnishing more gas by evaporating the light fractions of the crude. Pumping ' compressed gas or air down selected wells of a lease has been found to increase the production of oil from the surrounding wells. Studies of oil and gas ratios have indicated that much of the available gas has been wasted as far as its effectiveness on oil production is concerned. his has led to the development of "stop cocking"3 and the practice of producing under back pressure3, which methods aim, to obtain more effective work from the gas with reference to the amount of oil delivered to the well.

Jan 1, 1926

By M. H. Stanczyk

The Bureau of Mines made bench-scale laboratory tests on a sample of typical Florida phosphate slime to determine alumina and phosphate extractions obtainable by agitation leaching, by baking and curing, and by a leach-electrolysis scheme. Recovery of mineral values from leached slime pulps by resin-in-pulp ion exchange contact and the reaction of the leached pulps to filtration, flocculation, and settling were also investigated. The best extractions of alumina and phosphate were obtained by (l) agitation leaching with sulfuric, hydrochloric, or nitric acid at an elevated temperature or (2) curing or baking the slime with sulfuric acid. Alumina extractions ranged from 80.8 to 90.0 percent and phosphate extractions ranged from 93.3 to 98.4 percent when the slime was leached at 90° C with sulfuric, hydrochloric, or nitric acids. Baking the slime with sulfuric acid at 200° C for 4 hours yielded an alumina extraction of 92.3 percent and a phosphate extraction of 97.0 percent, whereas curing with sulfuric acid at 100° C for 24 hours gave slightly higher alumina and phosphate extractions. Flocculation and settling properties of the slime were virtually unaffected in all cases. Filter area requirements, although somewhat improved as compared to untreated slime, remained relatively high. The lowest filter area requirement obtained was 44 square feet per ton of dry solids treated per day. Contacting leached slime pulps with ion exchange resins depleted the leach pulps of solubilized values; however, the filtration and settling properties of the barren pulps were unaffected. A leach-electrolysis scheme resulted in some concentration of solubilized phosphorus, but the method showed little promise of being commercially feasible.

Jan 1, 1966

By B. W. Gandrud

This is the first report published by the Bureau of Mines on washability characteristics of coal from beds in Tennessee. It is based principally upon screen-sizing and float-and-sink tests of raw coal from a bed on the Cumberland Plateau. Stripping operations were undertaken recently on this bed by the Cumberland Collieries, Inc., near Chalybeate,Van Buren County, Tenn. The bed has not been definitely correlated, but it may be an extension of the Sewanee bed, which has been mined extensively in the Tracy City district to the south-vest and at points near Dunlap and Pikeville to the southeast and east. It was spoken of by officials of the Cumberland Collieries as the Sewanee bed at the time of sampling for this study. In a letter dated October 16, 1948, W. D. Hardeman, geologist of the Department of Conservation, Nashville, Tenn., states: "The stripping operations of the Cumberland Collieries near the old postoffice at Chalybeate are, I am fairly certain, in the upper part of the Whitwell shale, which carries the Sewanee coal. This coal may be a stray seam, but it probably can be correlated with the Sewanee coal, which is mined farther east. "There are no detailed geologic maps or reports covering the area, and this opinion is based on what was observed in visiting the strip mines in that general vicinity." The laboratory work upon which this report is based was done at the Southern Experiment Station of the Bureau of Mines, United States Department of the Interior, in cooperation with the University of Alabama and the Cumberland Collieries, Inc.

Jan 1, 1949

By By Staff

"This publication summarizes, for potential contractors and all other interested parties, the research, development, and demonstration of in-house and contract projects programmed by the Bureau of Mines for fiscal year 1982(October 1, 1981-September 30, 1982) under its Minerals Health and Safety Technology program. The objective of these projects is to provide an ordered and sequenced series of advance toward the Bureau's overall goal of providing the systems technology required to create a more healthful and safer working environment for the Nation's mining and minerals processing workersINTRODUCTION The Bureau of Mines conducts a balanced, continuing in-house research and development program to accelerate systematic improvements in health and safety conditions in U.S. mines. Part I of this report outlines the Bureau's present in-house effort to all interested parties; in particular, potential contractors can refer to it when submitting USP's (unsolicited proposals), thus avoiding proposing research that duplicates work being performed by the Bureau.It is the policy of the Bureau of Mines to utilize as fully as possible the capabilities of the private sector in minerals research, and to that endPart II of this report outlines the Bureau's current projected contract research needs.The projects presented were planned at the beginning of the fiscal year and are subject to change based on emerging priorities and availability of funds. Contingencies may require that a significant portion of the program be deferred into fiscal year 1983 (FY 83) or beyond. It is important to realize that since this is a summary document, the project descriptions related to a design, fabrications, and demonstration effort do not necessarily imply total package procurement."

Jan 1, 1982

"INTRODUCTION These safety standards for anthracite mines have been prepared for use as a guide for Federal inspectors. They are a revision of ""Tentative Inspection Standards for Anthracite Mines,"" published as Bureau of Mines Information Circular 7282 issued in May 1944 and used as a guide in Federal inspections. No provision made in these safety standards should be construed or operate to nullify any existing State statutes; they are intended to supplement the State statutes in the interest of increased mine safety. Mines are inspected in accordance with the Federal Coal-Mine Inspection and Investigation Act of 1941, Public Law 49, 77th Congress, H. R. 2082. Any unusual hazard noted by an inspector and not covered by these standards will be discussed in the inspection report, and suitable remedial procedure will be recommended.ARTICLE I. - SURFACE STRUCTURESSection 1. Breaker and cleaning plant.Electric switches and controls in breakers and cleaning plants should be enclosed.Where coal is dumped at or near air-intake openings, reasonable provisions should be made to prevent the dust from entering the mine.Section 2. Lamp houseNaphtha or other flammable liquids in lamp houses should be kept in approved containers or other suitable dispensers.Flame safety lamps should be permissible and maintained in permissible condition.Flame safety lamps should be properly cleaned, examined, and assembled by a qualified lamp attendant or other competent person before each period of use. Lamp assembly should again be checked by the person using it immediately before he enters the mine.When not in service, methane indicators, flame safety lamps, and electric cap lamps should be in the custody of competent persons responsible for maintenance and testing."

Feb 1, 1948

By J. L. Shultz

The investigation of organic compounds in respiratory coal dust by high-resolution mass spectrometry has shown that the organic components differ (1) with particle size, (2) with rank of coal, (3) in coals of same rank from different coal seams, and (4) in respirable mine dust and respirable coal dust (prepared) from the same mine. The eight respirable mine dusts studied are from coal seams in the Appalachian region where the incidence of coal workers' pnumoconiosis is relatively high. The molecular weights of the major organic components vary greatly among these respirable mine dusts; three show strong concentrations of polynuclear aromatic hydrocarbons.

Jan 1, 1972

This paper on. the physical and chemical properties of crude oils from California fields is one of a series of reports on the oil-producing districts of the United States., The paper includes a short discussion of results, tabular data, and individual analyses of eight California crudes. Analyses of other crude oils from California have been published in Reports, of Investigations 2595,3/ 2608,4/ and 28465/. The samples were obtained by members of the San Francisco office of the Bureau of Mines. The collecting samples was facilitated by the courtesy of representatives of oil companies in California.

Jan 1, 1931

By L. J. Kane

Applications are described of various methods for determining the weight concentration and physical properties of solid and liquid impurities of gases in connection with problems encountered in synthesis-gas production. Of special interest among these methods may be listed: 1. A method developed for determining, the weight concentration of solid and liquid impurities in. hot, crude synthesis gas containing a high concentration of moisture. 2. A method developed for the same purpose but for highly purified synthesis gas or atmospheric air. 3. A method for obtaining a uniform dispersion of dry duet or, a microscope slide for particle-size determination or other purposes.

Jan 1, 1954

1. Domestic Production and Use: In 1979, 12 companies operated 32 primary aluminum reduction plants, with 3 firms accounting for 64% of production. Washington, Oregon and Montana accounted for 32% of the total production; Gulf Coast States 20%; other Northern States 32%; and other Southern States 16%. Based on published producer prices output of primary metal in 1979 was valued at over $6 billion. Aluminum consumption by 25,000 firms was centered in the East Central United States. Of aluminum consuming industries in 1979, building accounted for about 24%; packaging 23%; transportation 22%; electrical 11%; consumer durables 8%; and other uses, 12%.

Jan 1, 1980

By G. H. Wigton

This paper, describing the concentrator practice of the Chief Consolidated Co., is one of a series being prepared by the United States Bureau of Mines. The concentrator adjoins the town of Eureka, Utah, in the Tintic mining district. The Chief Consolidated, Eureka Lilly, Plutus, and Grand Central mines, all of which are owned or controlled by the Chief Consolidated Mining Co., are the principal sources of milling ore. The ore is transported from mines to mill by railroad. Although all the mines are within 3 miles of the mill, the railroad distance varies from 1 mile to 12 miles.

Jan 1, 1930

By T. J. Ballard

The Tallapoosa Copper mine in Haralson County, Ga., has been operated, or under development at various times since before the Civil War. The geology of the deposit is similar to that of many of the pyrite deposits occurring in the belt of ancient crystalline and metamorphic rocks that extends diagonally northeast-southwest across the State. The Bureau of Mines, in its program of investigation of, strategic mineral deposits, diamond-drilled four holes totaling 1,570.3 feet at the deposit during the period June to September 1947 to verify the old drill records and the continuation of the deposit at depth.

Jan 1, 1948