The Batch Phase Disengagement Test

In the batch phase disengagement test, an organic and an aqueous phase are mixed together for a known period to produce a dispersion which may be either organic continuous (aqueous phase droplets) or aqueous continuous (organic phase droplets). The continuity of the dis- persion will depend upon the method of init- iating the dispersion, the conditions under which the system is operating, such as temper- ature and impeller speed, and the properties of the liquids, such as viscosity, inter- facial tension and solute content. Once the dispersion has been agitated for the required period, the agitator is turned off and the position of the coalescence interface and the sedimentation interface recorded as a function of time. This will produce a plot similar to Figure 1, where the overall dir- ection of travel of the droplets of dispersed phase is away from the sedimentation inter- face and towards the coalescence interface where the droplets coalesce with the homophase.